公开(公告)号：US6054302A

公开(公告)日：2000-04-25

申请号：US643719

申请日：1996-05-06

申请人： Yong-Cheng Shi ,  James L. Eden ,  James J. Kasica ,  Roger Jeffcoat

发明人： Yong-Cheng Shi ,  James L. Eden ,  James J. Kasica ,  Roger Jeffcoat

IPC分类号： A23L1/0522 ,  C08B30/00 ,  C08B30/12 ,  C08L3/00 ,  C08L23/08 ,  C09J103/00 ,  C09J103/02 ,  C09J131/04 ,  C12P19/14 ,  C12P19/16 ,  C12P19/20 ,  C12P19/22 ,  D21H19/10

CPC分类号： C12P19/14 ,  C08B30/12 ,  C09J103/00 ,  C09J131/04 ,  C08L23/08 ,  C08L3/00

摘要： A high solids, enzyme conversion process for preparing an enzyme-converted starch is carried out by adding to a modified or unmodified starch, preferably a granular starch, water and an enzyme in an amount sufficient to produce a single phase powdered mixture without a visible free water phase. The enzyme is activated by heating while maintaining a substantially constant moisture content in the mixture. The enzyme converted starch is recovered as a syrup, a granular converted starch, or mixtures thereof, or as a powder obtained by drying the syrup.

摘要翻译： 用于制备酶转化的淀粉的高固体，酶转化方法是通过向修饰或未改性的淀粉，优选颗粒淀粉，水和酶中加入足以产生单相粉末混合物而没有可见的自由基 水相。 通过加热活化酶，同时保持混合物中基本上恒定的水分含量。 将酶转化的淀粉作为糖浆，粒状转化淀粉或其混合物回收，或作为通过干燥糖浆获得的粉末回收。

公开(公告)号：US06096524A

公开(公告)日：2000-08-01

申请号：US78766

申请日：1998-05-14

申请人： Yong-Cheng Shi ,  James L. Eden ,  James J. Kasica

发明人： Yong-Cheng Shi ,  James L. Eden ,  James J. Kasica

IPC分类号： C08B31/04 ,  C08B31/12 ,  C09J103/02 ,  C09J103/06 ,  C12P19/14

CPC分类号： C08B31/04 ,  C08B31/12 ,  C09J103/02 ,  C09J103/06 ,  C12P19/14

摘要： High solids maltodextrin syrups, some of which are useful as the base for remoistenable adhesives, are prepared by a high solids alpha amylase enzyme conversion process. They are characterized by their high solids content (at least 55 wt. %) and light color. A granular chemically derivatized, optionally converted, starch having a degree of substitution of greater than about 0.01 and less than about 0.5 is used as the starting material. The maltodextrins have a reducing sugar content of about 5-19 dextrose equivalent and a distinct polymodal molecular weight distribution. When a granular highly esterified starch (D.S. of 0.5-1.8) is used as the starting material in the high solids process, the resulting enzyme-converted, esterified maltodextrins are characterized by their improved water dispersibility.

摘要翻译： 高固体麦芽糖糊精糖浆，其中一些可用作可再次接合的粘合剂的基质，通过高固体含量的α淀粉酶转化方法制备。 它们的特征在于其高固体含量（至少55重量％）和浅色。 使用具有大于约0.01且小于约0.5的取代度的粒状化学衍生的，任选转化的淀粉作为起始原料。 麦芽糖糊精具有约5-19葡萄糖当量的还原糖含量和不同的多模态分子量分布。 当高固含量的淀粉（D.S.为0.5-1.8）被用作起始原料时，所得酶转化的酯化麦芽糊精的特征在于它们的水分散性提高。

公开(公告)号：US5795397A

公开(公告)日：1998-08-18

申请号：US643644

申请日：1996-05-06

申请人： Yong-Cheng Shi ,  James L. Eden ,  James J. Kasica

发明人： Yong-Cheng Shi ,  James L. Eden ,  James J. Kasica

IPC分类号： C08B31/04 ,  C08B31/12 ,  C09J103/02 ,  C09J103/06 ,  C12P19/14 ,  C08B31/00 ,  C08B30/18 ,  C08B31/02 ,  C08B31/08

CPC分类号： C08B31/04 ,  C08B31/12 ,  C09J103/02 ,  C09J103/06 ,  C12P19/14

摘要： High solids maltodextrin syrups, some of which are useful as the base for remoistenable adhesives, are prepared by a high solids alpha amylase enzyme conversion process. They are characterized by their high solids content (at least 55 wt. %) and light color. A granular chemically derivatized, optionally converted, starch having a degree of substitution of greater than about 0.01 and less than about 0.5 is used as the starting material. The maltodextrins have a reducing sugar content of about 5-19 dextrose equivalent and a distinct polymodal molecular weight distribution. When a granular highly esterified starch (D.S. of 0.5-1.8) is used as the starting material in the high solids process, the resulting enzyme-converted, esterified maltodextrins are characterized by their improved water dispersibility.

摘要翻译： 高固体麦芽糖糊精糖浆，其中一些可用作可再次接合的粘合剂的基质，通过高固体含量的α淀粉酶转化方法制备。 它们的特征在于其高固体含量（至少55重量％）和浅色。 使用具有大于约0.01且小于约0.5的取代度的粒状化学衍生的，任选转化的淀粉作为起始原料。 麦芽糖糊精具有约5-19葡萄糖当量的还原糖含量和不同的多模态分子量分布。 当高固含量的淀粉（D.S.为0.5-1.8）被用作起始原料时，所得酶转化的酯化麦芽糖糊精的特征在于其水分散性提高。

公开(公告)号：US5318635A

公开(公告)日：1994-06-07

申请号：US919673

申请日：1992-07-27

申请人： James J. Kasica ,  James L. Eden

发明人： James J. Kasica ,  James L. Eden

IPC分类号： C08B30/12 ,  C08B30/14 ,  C08B30/16 ,  C08B30/20 ,  C08B37/00 ,  C08J3/12 ,  C08B30/00 ,  C08F8/00 ,  C08F16/06

CPC分类号： C08J3/122 ,  C08B30/14 ,  C08B37/0087 ,  C08J2300/10

摘要： A continuous coupled jet-cooking/spray-drying process for processing inherently water-dispersible or water-soluble crystalline polymers, such as starches, polygalactomannan gums, and fully hydrolyzed polyvinyl alcohols, is disclosed. It involves the steps of: (a) forming a slurry or paste of the polymer and water, (b) jet-cooking the slurry or paste with steam at a temperature sufficient to fully disperse or solubilize the polymer, (c) immediately conveying and introducing under elevated temperature and pressure the jet-cooked dispersion or solution into a nozzle of a spray-dryer chamber, (d) atomizing the jet-cooked dispersion or solution through the nozzle, (e) drying the atomized mist within the spray-dryer chamber at a temperature sufficient to dry the polymer; and (f) recovering the dried polymer as a water-dispersible or water-soluble powder. High amylose starches (above about 40% amylose) prepared by this process are characterized in that the starch is substantially non-crystalline and substantially non-degraded. Starch mixtures, mixtures of high amylose starches and other starches, gums, or polyvinyl alcohols can be co-processed.

摘要翻译： 公开了用于处理固有的水分散性或水溶性结晶聚合物如淀粉，聚半乳甘露聚糖胶和完全水解的聚乙烯醇的连续联合喷射蒸煮/喷雾干燥方法。 它包括以下步骤：（a）形成聚合物和水的浆料或浆料，（b）在足以使聚合物完全分散或溶解的温度下用蒸汽喷射蒸煮浆料或糊料，（c）立即输送和 在高温和高压下将喷射蒸煮的分散体或溶液引入喷雾干燥器室的喷嘴中，（d）通过喷嘴雾化喷射蒸煮的分散体或溶液，（e）干燥喷雾干燥器内的雾化雾 室在足以干燥聚合物的温度下进行; 和（f）将干燥的聚合物作为水分散性或水溶性粉末回收。 通过该方法制备的高直链淀粉（高于约40％的直链淀粉）的特征在于淀粉基本上是非结晶的并且基本上不降解。 淀粉混合物，高直链淀粉和其它淀粉的混合物，树胶或聚乙烯醇可以被共同加工。

公开(公告)号：US5188674A

公开(公告)日：1993-02-23

申请号：US697659

申请日：1991-05-08

申请人： James J. Kasica ,  James L. Eden

发明人： James J. Kasica ,  James L. Eden

IPC分类号： C08B30/14 ,  C08B37/00 ,  C08J3/12

CPC分类号： C08J3/122 ,  C08B30/14 ,  C08B37/0087 ,  C08J2300/10

摘要： A continuous coupled jet-cooking/spray-drying process for processing inherently water-dispersible or water-soluble crystalline polymers, such as starches, polygalactomannan gums, and fully hydrolyzed polyvinyl alcohols, is disclosed. It involves the steps of: (a) forming a slurry or paste of the polymer and water, (b) jet-cooking the slurry or paste with steam at a temperature sufficient to fully disperse or solubilize the polymer, (c) immediately conveying and introducing under elevated temperature and pressure the jet-cooked dispersion or solution into a nozzle of a spray-dryer chamber, (d) atomizing the jet-cooked dispersion or solution through the nozzle, (e) drying the atomized mist within the spray-dryer chamber at a temperature sufficient to dry the polymer; and (f) recovering the dried polymer as a water-dispersible or water-soluble powder.High amylose starches (above about 40% amylose) prepared by this process are characterized in that the starch is substantially non-crystalline and substantially non-degraded. Starch mixtures, mixtures of high amylose starches and other starches, gums, or polyvinyl alcohols can be co-processed.

摘要翻译： 公开了用于处理固有的水分散性或水溶性结晶聚合物如淀粉，聚半乳甘露聚糖胶和完全水解的聚乙烯醇的连续联合喷射蒸煮/喷雾干燥方法。 其包括以下步骤：（a）形成聚合物和水的浆料或浆料，（b）在足以使聚合物充分分散或溶解的温度下用蒸汽喷射蒸煮浆料或糊料，（c）立即输送和 在高温和高压下将喷射蒸煮的分散体或溶液引入喷雾干燥器室的喷嘴中，（d）通过喷嘴雾化喷射蒸煮的分散体或溶液，（e）干燥喷雾干燥器内的雾化雾 室在足以干燥聚合物的温度下进行; 和（f）将干燥的聚合物作为水分散性或水溶性粉末回收。 通过该方法制备的高直链淀粉（高于约40％的直链淀粉）的特征在于淀粉基本上是非结晶的并且基本上不降解。 淀粉混合物，高直链淀粉和其它淀粉的混合物，树胶或聚乙烯醇可以被共同加工。

公开(公告)号：US5571552A

公开(公告)日：1996-11-05

申请号：US417545

申请日：1995-04-06

申请人： James J. Kasica ,  James L. Eden

发明人： James J. Kasica ,  James L. Eden

IPC分类号： C08B30/14 ,  C08B37/00 ,  C08J3/12 ,  A23L1/05 ,  A23L1/0522 ,  A23L1/0532 ,  A23L1/0562

CPC分类号： C08J3/122 ,  C08B30/14 ,  C08B37/0087 ,  C08J2300/10

摘要： A continuous coupled jet-cooking/spray-drying process for processing or co-processing inherently water-dispersible or water-soluble crystalline polymers, such as starches, starch mixtures, gums (e.g., locust bean gum, carrageenan, agar), viscosifying proteins (e.g., gelatin), starch-gum mixtures, and fully hydrolyzed polyvinyl alcohols, is disclosed. The process involves the steps of: (a) forming a slurry or paste of the polymer and water, (b) jet-cooking the slurry or paste with steam at a temperature sufficient to fully disperse or solubilize the polymer, (c) immediately conveying and introducing, under elevated temperature and pressure, the jet-cooked dispersion or solution into a nozzle of a spray-dryer chamber, (d) atomizing the jet-cooked dispersion or solution through the nozzle, (e) drying the atomized mist within the spray-dryer chamber at a temperature sufficient to dry the polymer; and (f) recovering the dried polymer as a water-dispersible or water-soluble powder.

摘要翻译： 用于加工或共处理固有的水分散性或水溶性结晶聚合物如淀粉，淀粉混合物，树胶（例如刺槐豆胶，角叉菜胶，琼脂），粘性蛋白质的连续联合喷射蒸煮/喷雾干燥方法 （例如明胶），淀粉 - 胶混合物和完全水解的聚乙烯醇。 该方法包括以下步骤：（a）形成聚合物和水的浆料或浆料，（b）在足以使聚合物完全分散或溶解的温度下用蒸汽喷射蒸煮浆料或糊料，（c）立即输送 并在升高的温度和压力下将喷射蒸煮的分散体或溶液引入喷雾干燥器室的喷嘴中，（d）通过喷嘴雾化喷射的分散体或溶液，（e）将雾化的雾气在 喷雾干燥器室，其温度足以干燥聚合物; 和（f）将干燥的聚合物作为水分散性或水溶性粉末回收。

公开(公告)号：US4874628A

公开(公告)日：1989-10-17

申请号：US242852

申请日：1988-09-12

申请人： James L. Eden ,  James J. Kasica ,  James P. Zallie

发明人： James L. Eden ,  James J. Kasica ,  James P. Zallie

IPC分类号： A23G3/34 ,  A23G3/00 ,  A23G3/02 ,  A23G3/04 ,  A23G3/42 ,  A23G3/48

CPC分类号： A23G3/48 ,  A23G3/0205 ,  A23G3/0252 ,  A23G3/04 ,  A23G3/42

摘要： Pregelatinized high amylose starches are useful in processing cast jelly gum confectionaries. The starch has an amylose content of at least 40% and it may be used alone or in combination with a converted starch. The starch is pregelatinized by spray-drying using a novel continuous coupled jet-cooking/sray-drying process or simultaneous atomization/spray-drying process or by drum-drying after fully dispersing the starch. The confectionary can be cooked at a lower temperature than was possible using prior art starches and still provide confectionaries with desirable characteristics.

公开(公告)号：US5435851A

公开(公告)日：1995-07-25

申请号：US239650

申请日：1994-05-09

申请人： James J. Kasica ,  James L. Eden

发明人： James J. Kasica ,  James L. Eden

IPC分类号： C08B30/14 ,  C08B37/00 ,  C08J3/12 ,  C08B30/00

CPC分类号： C08J3/122 ,  C08B30/14 ,  C08B37/0087 ,  C08J2300/10

摘要： A continuous coupled jet-cooking/spray-drying process for processing or co-processing inherently water-dispersible or water-soluble crystalline polymers, such as starches, starch mixtures, gums (e.g., locust bean gum, carrageenan, agar), viscosifying proteins (e.g., gelatin), starch-gum mixtures, and fully hydrolyzed polyvinyl alcohols, is disclosed. The process involves the steps of: (a) forming a slurry or paste of the polymer and water, (b) jet-cooking the slurry or paste with steam at a temperature sufficient to fully disperse or solubilize the polymer, (c) immediately conveying and introducing, under elevated temperature and pressure, the jet-cooked dispersion or solution into a nozzle of a spray-dryer chamber, (d) atomizing the jet-cooked dispersion or solution through the nozzle, (e) drying the atomized mist within the spray-dryer chamber at a temperature sufficient to dry the polymer; and (f) recovering the dried polymer as a water-dispersible or water-soluble powder.High amylose starches (above about 40% amylose) prepared by this process are characterized in that the starch is substantially non-crystalline and substantially non-degraded. Non-high amylose prepared by this process are characterized in that they are substantially non-crystalline and have bulk densities higher than the bulk densities of the same base starches pregelatinized by jet-cooking and spray-drying in two separate steps.

摘要翻译： 用于加工或共处理固有的水分散性或水溶性结晶聚合物如淀粉，淀粉混合物，树胶（例如刺槐豆胶，角叉菜胶，琼脂），粘性蛋白质的连续联合喷射蒸煮/喷雾干燥方法 （例如明胶），淀粉 - 胶混合物和完全水解的聚乙烯醇。 该方法包括以下步骤：（a）形成聚合物和水的浆料或浆料，（b）在足以使聚合物完全分散或溶解的温度下用蒸汽喷射蒸煮浆料或糊料，（c）立即输送 并在升高的温度和压力下将喷射蒸煮的分散体或溶液引入喷雾干燥器室的喷嘴中，（d）通过喷嘴雾化喷射的分散体或溶液，（e）将雾化的雾气在 喷雾干燥器室，其温度足以干燥聚合物; 和（f）将干燥的聚合物作为水分散性或水溶性粉末回收。 通过该方法制备的高直链淀粉（高于约40％的直链淀粉）的特征在于淀粉基本上是非结晶的并且基本上不降解。 通过该方法制备的非高直链淀粉的特征在于它们基本上是非结晶的，并且具有高于通过喷射蒸煮和喷雾干燥在两个单独步骤中预胶化的相同基础淀粉的堆积密度的堆积密度。

公开(公告)号：US5131953A

公开(公告)日：1992-07-21

申请号：US242657

申请日：1988-09-12

申请人： James J. Kasica ,  James L. Eden

发明人： James J. Kasica ,  James L. Eden

IPC分类号： C08B30/12 ,  C08B30/14 ,  C08B30/16 ,  C08B30/20 ,  C08B37/00 ,  C08J3/12

CPC分类号： C08J3/122 ,  C08B30/14 ,  C08B37/0087 ,  C08J2300/10

摘要： A continuous coupled jet-cooking/spray-drying process for processing inherently water-dispersible or water-soluble crystalline polymers, such as starches, polygalactomannan gums, and fully hydrolyzed polyvinyl alcohols, is disclosed. it involves the steps of: (a) forming a slurry or paste of the polymer and water, (b) jet-cooking the slurry or paste with steam at a temperature sufficient to fully disperse or solubilize the polymer, (c) immediately conveying and introducing under elevated temperature and pressure the jet-cooked dispersion or solution into a nozzle of a spray-dryer chamber, (d) atomizing the jet-cooked dispersion or solution through the nozzle, (e) drying the atomized mist within the spray-dryer chamber at a temperature sufficient to dry the polymer; and (f) recovering the dried polymer as a water-dispersible or water-insoluble powder.High amylose starches (above about 40% amylose) prepared by this process are characterized in that the starch is substantially non-crystalline and substantially non-degraded. Starch mixtures, mixtures of high amylose starches and other starches, gums, or polyvinyl alcohols can be co-processed.

公开(公告)号：US06428836B1

公开(公告)日：2002-08-06

申请号：US09633832

申请日：2000-08-07

申请人： Wolfgang Bindzus ,  Paul A. Altieri ,  James J. Kasica ,  Peter T. Trzasko

发明人： Wolfgang Bindzus ,  Paul A. Altieri ,  James J. Kasica ,  Peter T. Trzasko

IPC分类号： A23L105

CPC分类号： A23C19/093 ,  A23C20/00 ,  A23L13/426 ,  A23L13/72 ,  A23L17/70 ,  A23L29/219 ,  C08B31/066

摘要： The present invention is directed to a process of preparing starch phosphate monoesters, optionally in the presence of oligosaccharides, having improved reaction efficiency and reduced side reactions. The invention also includes the improved starch phosphate monoester products, characterized by high viscosity and low level of residual salts, their use in food and the enhanced food compositions prepared from them.

摘要翻译： 本发明涉及一种制备淀粉磷酸酯单酯的方法，任选地在寡糖存在下，具有改善的反应效率和降低的副反应。 本发明还包括改进的淀粉磷酸酯单酯产品，其特征在于高粘度和低水平的残留盐，它们在食品中的用途以及由它们制备的增强的食品组合物。