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公开(公告)号：US20050009451A1
公开(公告)日：2005-01-13
申请号：US10793817
申请日：2004-03-08
CPC分类号： B24C3/28 , C23C14/028
摘要： A process for treating surfaces of rare earth metal-based permanent magnets, comprising removing an oxide layer formed on a surface of each of the permanent magnets using a blasting apparatus. The apparatus comprises a tubular barrel formed of a mesh net for accommodation of work pieces and supported circumferentially outside a center axis of a support member rotatable about the center axis, and an injection nozzle disposed to inject a blast material against the work pieces from the outside of the tubular barrel, wherein at least one of the tubular barrel and the support member is detachably mounted. The process further comprises removing the tubular barrel or the support member from the blasting apparatus and attaching the tubular barrel or the support member to a vapor deposited film forming apparatus, where a metal film is formed on the surface of each of the permanent magnets by a vapor deposition process.
摘要翻译： 一种用于处理稀土金属基永磁体的表面的方法，包括使用喷砂装置除去形成在每个永磁体的表面上的氧化物层。 该装置包括由网状物形成的管状筒体，用于容纳工件，并且围绕中心轴线可围绕支撑构件的中心轴线周向地支撑;以及喷嘴，其设置成将喷射材料从外部喷射到工件上 其中管状筒和支撑构件中的至少一个可拆卸地安装。 该方法还包括从喷砂设备中取出管状筒体或支撑构件，并将管状筒体或支撑构件附接到蒸镀膜形成设备，其中通过一个永磁体的表面上形成金属膜 气相沉积工艺。
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公开(公告)号：US06743082B2
公开(公告)日：2004-06-01
申请号：US09819765
申请日：2001-03-29
IPC分类号： B24C326
CPC分类号： B24C3/28 , C23C14/028
摘要： With the blasting apparatus in which the injection nozzle is disposed to inject the blast material against the work pieces from the outside of the tubular barrel formed of the mesh net for accommodation of the work pieces and rotatable about the center axis, the work pieces can be stirred homogenously and efficiently without excessive occurrence of the collision of the work pieces against one another and without occurrence of the collision of the work pieces against one another and with a strong shock force. Therefore, the treating efficiency is enhanced and, it is possible to inhibit the occurrence of the cracking and breaking of the work pieces. Further, with the blasting apparatus in which the tubular barrel is supported circumferentially outside the center axis of the support member rotatable about the center axis, it is possible to more inhibit the occurrence of the cracking and breaking of the work pieces.
摘要翻译： 通过设置注射喷嘴的喷射装置，将喷砂材料从由网状物形成的管状筒体的外部喷射到工件上，用于容纳工件并可围绕中心轴线旋转，工件可以是 搅拌均匀且有效，而不会过度地发生工件相互碰撞而不会发生工件相互碰撞并且具有很强的冲击力。 因此，提高了处理效率，并且可以抑制工件的破裂和断裂的发生。 此外，通过其中管状筒周向地支撑在支撑构件的中心轴线外侧的爆破装置可以围绕中心轴线旋转，可以更有效地抑制工件的破裂和破裂的发生。
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公开(公告)号：US07086934B2
公开(公告)日：2006-08-08
申请号：US10793817
申请日：2004-03-08
IPC分类号： B24C1/10
CPC分类号： B24C3/28 , C23C14/028
摘要： A process for treating surfaces of rare earth metal-based permanent magnets, comprising removing an oxide layer formed on a surface of each of the permanent magnets using a blasting apparatus. The apparatus comprises a tubular barrel formed of a mesh net for accommodation of work pieces and supported circumferentially outside a center axis of a support member rotatable about the center axis, and an injection nozzle disposed to inject a blast material against the work pieces from the outside of the tubular barrel, wherein at least one of the tubular barrel and the support member is detachably mounted. The process further comprises removing the tubular barrel or the support member from the blasting apparatus and attaching the tubular barrel or the support member to a vapor deposited film forming apparatus, where a metal film is formed on the surface of each of the permanent magnets by a vapor deposition process.
摘要翻译： 一种用于处理稀土金属基永磁体的表面的方法，包括使用喷砂装置除去形成在每个永磁体的表面上的氧化物层。 该装置包括由网状物形成的管状筒体，用于容纳工件，并且围绕中心轴线可围绕支撑构件的中心轴线周向地支撑;以及喷嘴，其设置成将喷射材料从外部喷射到工件上 其中管状筒和支撑构件中的至少一个可拆卸地安装。 该方法还包括从喷砂设备中取出管状筒体或支撑构件，并将管状筒体或支撑构件附接到蒸镀膜形成设备，其中通过一个永磁体的表面上形成金属膜 气相沉积工艺。
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公开(公告)号：US07056197B2
公开(公告)日：2006-06-06
申请号：US09901044
申请日：2001-07-10
IPC分类号： B24B31/00
CPC分类号： C23C14/223 , B24C3/26 , C23C14/24 , C23C14/505
摘要： A dry surface treating apparatus of the present invention comprises, within a treating chamber, a surface-treating material supply section and a tubular barrel having a porous peripheral surface for accommodating a work piece, to treat a surface of the work piece while rotating the tubular barrel horizontally arranged about a horizontal rotational axis, wherein the tubular barrel has a slide stop for stopping a slide of the accommodated work piece along an inner peripheral surface of the tubular barrel due to rotation of the tubular barrel.According to the dry surface treating apparatus of the invention, because the work piece is inverted of surfaces within the tubular barrel, the time the work piece at each surface faces the surface-treating material supply section is made equivalent. Consequently, it is possible to provide even deposited-film formation or surface treatment to the opposite surfaces of a work piece, particularly, a rare earth metal-based permanent magnet in a plate or bow form.
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公开(公告)号：US20110273252A1
公开(公告)日：2011-11-10
申请号：US13056387
申请日：2009-07-30
CPC分类号： H01F41/026 , B22F3/24 , B22F2003/242 , B22F2998/00 , B32B15/012 , C22C33/0278 , C22C38/005 , C22C38/10 , C22C2202/02 , H01F1/0577 , H01F7/0221
摘要： An object of the present invention is to provide an R—Fe—B based sintered magnet that exhibits excellent corrosion resistance and maintains excellent adhesion strength to an adherend even under severe conditions, and a method for producing the same. A corrosion-resistant magnet of the present invention as a means for achieving the object is characterized by comprising a chemical conversion film containing at least Zr, V, Al, fluorine, and oxygen as constituent elements and not containing phosphorus over a surface of an R—Fe—B based sintered magnet with a film made of Al or an alloy thereof therebetween.
摘要翻译： 本发明的目的在于提供即使在苛刻条件下也能显示出优良的耐腐蚀性和对被粘物的粘合强度优异的R-Fe-B系烧结磁铁及其制造方法。 作为实现该目的的手段的本发明的耐腐蚀磁体的特征在于，包括至少含有Zr，V，Al，氟和氧作为构成元素并且在R表面上不含磷的化学转化膜 -Fe-B系烧结磁体，其中由Al制成的膜或它们之间的合金。
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公开(公告)号：US09275794B2
公开(公告)日：2016-03-01
申请号：US13056387
申请日：2009-07-30
CPC分类号： H01F41/026 , B22F3/24 , B22F2003/242 , B22F2998/00 , B32B15/012 , C22C33/0278 , C22C38/005 , C22C38/10 , C22C2202/02 , H01F1/0577 , H01F7/0221
摘要： An object of the present invention is to provide an R—Fe—B based sintered magnet that exhibits excellent corrosion resistance and maintains excellent adhesion strength to an adherend even under severe conditions, and a method for producing the same. A corrosion-resistant magnet of the present invention as a means for achieving the object is characterized by comprising a chemical conversion film containing at least Zr, V, Al, fluorine, and oxygen as constituent elements and not containing phosphorus over a surface of an R—Fe—B based sintered magnet with a film made of Al or an alloy thereof therebetween.
摘要翻译： 本发明的目的在于提供即使在苛刻条件下也能显示出优良的耐腐蚀性和对被粘物的粘合强度优异的R-Fe-B系烧结磁铁及其制造方法。 作为实现该目的的手段的本发明的耐腐蚀磁体的特征在于，包括至少含有Zr，V，Al，氟和氧作为构成元素并且在R表面上不含磷的化学转化膜 -Fe-B系烧结磁体，其中由Al制成的膜或它们之间的合金。
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7.发明授权R-Fe-B based sintered magnet having on the surface thereof vapor deposited film of aluminum or alloy thereof, and method for producing the same 有权在其表面具有铝或其合金的蒸镀膜的R-Fe-B系烧结磁体及其制造方法公开(公告)号：US08163106B2
公开(公告)日：2012-04-24
申请号：US12599145
申请日：2008-05-09
IPC分类号： H01F1/057
CPC分类号： C23C14/226 , C23C14/14 , C23C14/246 , C23C14/505 , H01F1/0577 , H01F7/0221 , H01F41/026 , Y10T428/32 , Y10T428/325
摘要： An R—Fe—B sinlered magnet having on the surface thereof a vapor deposited film of aluminum or an alloy thereof and a method for producing the same. The vapor deposited film of aluminum or an alloy thereof comprises a columnar crystalline structure grown broader from the surface of the R—Fe—B sintered magnet body outward to the outer surface, which has a part within a region defined in the thickness direction of the film as taken from the surface of the R—Fe—B sintered magnet to ⅓ of the film thickness, 5 to 30 intercrystalline gaps of 0.01 μm to 1 μm in width as counted per 10 μm length in the lateral direction of the film. The method comprises controlling the average film formation rate such that it is slower up to a predetermined point and then is speeded up later thereon.
摘要翻译： 在其表面上具有铝或其合金的气相沉积膜的R-Fe-B带状磁体及其制造方法。 铝或其合金的气相沉积膜包括从R-Fe-B烧结磁体的表面向外扩展到外表面的柱状晶体结构，该柱状晶体结构在沿着厚度方向限定的区域内具有一部分 从R-Fe-B烧结磁体的表面取得的薄膜为薄膜厚度的1/3，膜的横向方向每10μm长度计数为5〜30个晶间间隙，宽度为0.01〜1μm。 该方法包括控制平均成膜速率，使得其延迟到预定点，然后在其上加速。
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8.发明申请R-FE-B BASED SINTERED MAGNET HAVING ON THE SURFACE THEREOF VAPOR DEPOSITED FILM OF ALUMINUM OR ALLOY THEREOF, AND METHOD FOR PRODUCING THE SAME 有权R-FE-B基于其表面的烧结磁体，其铝或其合金的蒸气沉积膜及其制造方法公开(公告)号：US20100295644A1
公开(公告)日：2010-11-25
申请号：US12599145
申请日：2008-05-09
CPC分类号： C23C14/226 , C23C14/14 , C23C14/246 , C23C14/505 , H01F1/0577 , H01F7/0221 , H01F41/026 , Y10T428/32 , Y10T428/325
摘要： An objective of the present invention is to provide an R—Fe—B based sintered magnet having on the surface thereof a vapor deposited film of aluminum or an alloy thereof, which maintains excellent adhesion strength with the adhered object even after subjecting it to a severe heat cycle test, and a method for producing the same. As a means for solving the problems, an R—Fe—B based sintered magnet having on the surface thereof a vapor deposited film of aluminum or an alloy thereof of the present invention is characterized in that the vapor deposited film of aluminum or an alloy thereof comprises a columnar crystalline structure grown broader from the surface of the bulk magnet body outward to the outer surface, which has a part within a region defined in the thickness direction of the film as taken from the surface of the bulk magnet body to ⅓ of the film thickness, 5 to 30 intercrystalline gaps of 0.01 μm to 1 μm in width as counted per 10 μm length in the lateral direction of the film are existing at the part. The method for producing the same is characterized by, on forming the vapor deposited film of aluminum or an alloy thereof on the surface of the R—Fe—B based sintered magnet, individually controlling the average film formation rate in the initial stage and in the later stage of the film formation as such that it is slower up to a predetermined point, and that it is speeded up later thereon.
摘要翻译： 本发明的目的是提供一种R-Fe-B系烧结磁体，其表面上具有铝或其合金的气相沉积膜，即使经受严重的粘合，也能与粘合物保持优异的粘合强度 热循环试验及其制造方法。 作为解决问题的手段，在本发明的表面具有铝或其合金的蒸镀膜的R-Fe-B系烧结磁体的特征在于，铝或其合金的蒸镀膜 包括从本体磁体的表面向外延伸到外表面的柱状晶体结构，其具有在从体磁体的表面取出的膜的厚度方向上限定的区域内的1/3 在该部分存在薄膜厚度，在膜的横向上每10μm长度计数为0.01μm至1μm的宽度为5至30个晶间间隙。 其制造方法的特征在于，在R-Fe-B系烧结磁体的表面上形成铝蒸气沉积膜或其合金时，分别控制初始阶段的平均成膜速率和 胶片形成的后期使得其延迟到预定点，并且其稍后加速。
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公开(公告)号：US06960368B2
公开(公告)日：2005-11-01
申请号：US11049961
申请日：2005-02-04
CPC分类号： C23C14/505 , H01F1/0556 , H01F41/026
摘要： With the deposited-film forming apparatus according to the first embodiment of the present invention, the distance between the tubular barrel and the evaporating section can be varied, unlike the prior art deposited-film forming apparatus and hence, the efficient formation of the deposited film on the surface of each of the work pieces accommodated in the tubular barrel and the inhibition of the softening of the formed film can be achieved simultaneously. Therefore, it is possible to inhibit the damaging of the deposited film formed on the surface of each of the work pieces and the production of projections on the deposited film, and to form a deposited film at a high quality in respect of a corrosion resistance and the like and at low cost.With the deposited-film forming apparatus according to the second embodiment of the present invention, the distance between the accommodating section defined in the tubular barrel and the evaporating section can be varied and hence, this deposited-film forming apparatus also exhibits an effect similar to that in the deposited-film forming apparatus according to the first embodiment of the present invention.
摘要翻译： 利用根据本发明第一实施例的沉积膜形成装置，可以改变管状筒和蒸发部之间的距离，这与现有技术的沉积膜形成装置不同，因此有效地形成沉积膜 在容纳在管状筒体中的每个工件的表面上，可以同时实现对形成的膜的软化的抑制。 因此，可以抑制在每个工件的表面上形成的沉积膜的破坏和沉积膜上的突起的产生，并且在耐腐蚀性方面形成高质量的沉积膜， 喜欢和低成本。 利用根据本发明第二实施例的沉积膜形成装置，可以改变限定在管状筒体中的容纳部分与蒸发部分之间的距离，因此该沉积膜形成装置也具有类似于 在根据本发明的第一实施例的沉积膜形成装置中。
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公开(公告)号：US20050126495A1
公开(公告)日：2005-06-16
申请号：US11049961
申请日：2005-02-04
CPC分类号： C23C14/505 , H01F1/0556 , H01F41/026
摘要： With the deposited-film forming apparatus according to the first embodiment of the present invention, the distance between the tubular barrel and the evaporating section can be varied, unlike the prior art deposited-film forming apparatus and hence, the efficient formation of the deposited film on the surface of each of the work pieces accommodated in the tubular barrel and the inhibition of the softening of the formed film can be achieved simultaneously. Therefore, it is possible to inhibit the damaging of the deposited film formed on the surface of each of the work pieces and the production of projections on the deposited film, and to form a deposited film at a high quality in respect of a corrosion resistance and the like and at low cost. With the deposited-film forming apparatus according to the second embodiment of the present invention, the distance between the accommodating section defined in the tubular barrel and the evaporating section can be varied and hence, this deposited-film forming apparatus also exhibits an effect similar to that in the deposited-film forming apparatus according to the first embodiment of the present invention.
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