PROCESS FOR PRODUCING HYDROGELS
    1.
    发明申请
    PROCESS FOR PRODUCING HYDROGELS 审中-公开
    生产水凝胶的方法

    公开(公告)号:US20140319418A1

    公开(公告)日:2014-10-30

    申请号:US14008757

    申请日:2012-04-13

    IPC分类号: C01B33/154 C01B33/157

    摘要: The invention relates to a process for producing a hydrogel, which is performed in a reactor which has a body A which rotates about an axis of rotation and a metering system. A component comprising at least i) a soluble salt of an acidic or amphoteric oxygen-containing molecular anion and ii) a component comprising a precipitant are applied with the aid of the metering system to the surface of the rotating body A, such that a mixture of components i) and ii) flows over the surface of the rotating body A to an outer region of the surface of the rotating body A, the mixture leaves the surface and the pH of the mixture after leaving the surface of the body A is between 2 and 12. Additionally disclosed is the use of the resulting hydrogels for production of aerogels.

    摘要翻译: 本发明涉及一种制备水凝胶的方法,该方法在具有围绕旋转轴线旋转的主体A和计量系统的反应器中进行。 包含至少i)酸性或两性含氧分子阴离子的可溶性盐和ii)包含沉淀剂的组分在计量系统的帮助下被施加到旋转体A的表面,使得混合物 的组分i)和ii)在旋转体A的表面上流动到旋转体A的表面的外部区域,混合物离开表面,并且离开体A的表面之后的混合物的pH在 另外公开了所得到的水凝胶用于生产气凝胶的用途。

    Method For Producing Metal Nanoparticles In Polyols
    2.
    发明申请
    Method For Producing Metal Nanoparticles In Polyols 审中-公开
    在多元醇中生产金属纳米粒子的方法

    公开(公告)号:US20110132144A1

    公开(公告)日:2011-06-09

    申请号:US13003785

    申请日:2009-07-15

    IPC分类号: B22F9/18 B22F9/00 B82Y40/00

    CPC分类号: B22F9/24

    摘要: The invention relates to a process for the preparation of metal nanoparticles, selected from the group consisting of lead, bismuth, zinc, antimony, indium, gold, nickel, cobalt, palladium, platinum, iridium, osmium, rhodium, ruthenium, rhenium, vanadium, chromium, manganese, niobium, molybdenum, tungsten, tantalum, cadmium, silver and/or copper, on a rotating body, characterized in that a reduction of corresponding metal salts, corresponding metal salt complexes, corresponding metal hydroxides and/or corresponding metal oxides by polyols having a number of hydroxyl groups in the polyol of 1 to 10 and a molecular weight of the polyols of 2000 to 18 000 Da is effected.

    摘要翻译: 本发明涉及一种选自铅,铋,锌,锑,铟,金,镍,钴,钯,铂,铱,锇,铑,钌,铼,钒的金属纳米颗粒的制备方法 ,铬,锰,铌,钼,钨,钽,镉,银和/或铜,其特征在于相应的金属盐,相应的金属盐络合物,相应的金属氢氧化物和/或相应的金属氧化物的还原 通过在多元醇中具有多个羟基的多元醇为1至10,多元醇的分子量为2000至18000Da。

    Continuous Production of Copolymers Suitable as Flow Agents
    3.
    发明申请
    Continuous Production of Copolymers Suitable as Flow Agents 审中-公开
    适用于流动剂的共聚物的连续生产

    公开(公告)号:US20110306696A1

    公开(公告)日:2011-12-15

    申请号:US13122663

    申请日:2009-10-08

    摘要: The invention relates to a process for the preparation of copolymers containing acid monomer structural units and polyether macromonomer structural units, which is carried out in a continuous mode of operation in a reactor which has α) a body B rotating about an axis of rotation and having a reaction surface, β) a metering system and γ) a device for irradiating the reaction surface, i) the components of a starting reaction composition being applied individually and/or as a mixture with the aid of the metering system in a thin film on an inner region of the reaction surface of the rotating body B so that the thin film flows over the reaction surface of the rotating body B to an outer region of the reaction surface of the rotating body B, the thin film on the reaction surface being electromagnetically irradiated by means of the device for the irradiation of the reaction surface, ii) the thin film leaving the reaction surface as a reaction composition which has copolymer containing acid monomer structural units and polyether macromonomer structural units and iii) the reaction composition being collected after leaving the reaction surface, an acid monomer, a polyether macromonomer and a photoinitiator being present as components of the starting reaction composition.

    摘要翻译: 本发明涉及一种制备含有酸单体结构单元和聚醚大分子单体结构单元的共聚物的方法,其在反应器中以连续的操作模式进行,所述反应器具有α)围绕旋转轴线旋转并具有 一个反应表面和一个计量系统,γ)一个用于照射反应表面的装置,i)起始反应组合物的组分被单独地和/或作为混合物,借助于计量系统施加在薄膜中 在旋转体B的反应面的内部区域,使得薄膜在旋转体B的反应面上流动到旋转体B的反应面的外侧区域,反应面上的薄膜为 通过用于照射反应表面的装置电磁照射,ii)离开反应表面的薄膜作为反应组合物,其具有含有 酸单体结构单元和聚醚大分子单体结构单元,和iii)离开反应表面后收集反应组合物,酸单体,聚醚大分子单体和光引发剂作为起始反应组合物的组分存在。

    Rotating surfaces for SDR
    9.
    发明申请
    Rotating surfaces for SDR 审中-公开
    旋转表面SDR

    公开(公告)号:US20110309533A1

    公开(公告)日:2011-12-22

    申请号:US13144341

    申请日:2009-12-11

    IPC分类号: C07G99/00 B01J19/00

    摘要: The proposed spinning disc reactor comprises substantially a horizontally rotatable, disc-like and thermostatable support element which has an outer reaction surface, feed means for feeding at least one reactant onto the reaction surface and internal structures for thermostating the reaction surface. In addition, it contains at least one separation apparatus for collecting and removing the reaction product from the reaction surface. The support element is characterized in particular in that it consists of two components a) and b) arranged horizontally one on top of the other and having substantially identical surface measures. These two components are connected to one another in an interlocking manner and tightly during the operating time and the lower component a) has, on its top facing the inner region of the support element, at least one substantially uninterrupted groove milled in over an extensive area and intended for receiving, conducting and discharging a heat-transfer fluid. In addition, it has at least two bores for feeding and discharging the heat-transfer fluid, at least one profiled seal encircling the outer surface region being arranged between the component a) and the component b). The two components a) and b) as a whole are reversibly connected to one another. As a result of such specific features, a simply designed reactor which is advantageous with respect to maintenance, is versatile and permits targeted control of the chemical reaction on its rotating surface is present.

    摘要翻译: 所提出的旋转圆盘反应器基本上包括具有外部反应表面的基本上水平可旋转的盘状和可热膨胀的支撑元件,用于将至少一种反应物进料到反应表面上的进料装置和用于恒温反应表面的内部结构。 此外,它还含有至少一种用于从反应表面收集和除去反应产物的分离装置。 支撑元件的特征在于,其特征在于,它由两个部件a)和b)组成,水平地布置在另一个之上并具有基本上相同的表面测量。 这两个部件在操作时间内以互锁的方式彼此连接并且紧密地连接,并且下部部件a)在其面向支撑元件的内部区域的顶部上具有在广泛区域上铣削的至少一个基本上不间断的凹槽 并且用于接收,导电和排出传热流体。 此外,它具有用于进给和排出传热流体的至少两个孔,至少一个环绕外部表面区域的成形密封件被布置在部件a)和部件b)之间。 两个组件a)和b)作为一个整体可逆地连接在一起。 由于这些具体特征,在维护方面有利的简单设计的反应器是通用的并且允许靶旋转表面上的化学反应的目标控制。