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公开(公告)号：US20130030150A1
公开(公告)日：2013-01-31
申请号：US13640836
申请日：2011-04-15
申请人： Zhonghao Zhuo , Zhijun Tang , Tianhui Xu
发明人： Zhonghao Zhuo , Zhijun Tang , Tianhui Xu
CPC分类号： B01D15/265 , B01D15/08 , B01D15/42 , B01D15/424 , B01D15/426 , C07K1/14 , C07K1/16 , C07K1/20 , C07K1/22 , C07K7/54 , C07K7/56
摘要： A purification method of the compound represented by formula 1 is provided, which includes the following steps: (1) loading crude compound 1 on macroporous adsorbent resin, (2) washing the macroporous adsorbent resin with an aqueous solution, an organic solvent or a mixture solution of organic solvent and water, (3) eluting with an aqueous solution, an organic solvent or a mixture solution of organic solvent and water. The purified compound represented by formula 1 is obtained.
摘要翻译： 提供由式1表示的化合物的纯化方法，其包括以下步骤：（1）在大孔吸附树脂上加载粗化合物1，（2）用水溶液，有机溶剂或混合物洗涤大孔吸附树脂 有机溶剂和水的溶液，（3）用水溶液，有机溶剂或有机溶剂和水的混合溶液洗脱。 得到由式1表示的纯化化合物。
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公开(公告)号：US09233318B2
公开(公告)日：2016-01-12
申请号：US13640836
申请日：2011-04-15
申请人： Zhonghao Zhuo , Zhijun Tang , Tianhui Xu , Ming Li , Xiaoming Ji , Xiaoliang Gao
发明人： Zhonghao Zhuo , Zhijun Tang , Tianhui Xu , Ming Li , Xiaoming Ji , Xiaoliang Gao
IPC分类号： C07K1/14 , C07K1/16 , C07K1/22 , C07K7/50 , B01D15/26 , B01D15/08 , B01D15/42 , C07K7/54 , C07K1/20 , C07K7/56
CPC分类号： B01D15/265 , B01D15/08 , B01D15/42 , B01D15/424 , B01D15/426 , C07K1/14 , C07K1/16 , C07K1/20 , C07K1/22 , C07K7/54 , C07K7/56
摘要： A purification method of the compound represented by formula 1 is provided, which includes the following steps: (1) loading crude compound 1 on macroporous adsorbent resin, (2) washing the macroporous adsorbent resin with an aqueous solution, an organic solvent or a mixture solution of organic solvent and water, (3) eluting with an aqueous solution, an organic solvent or a mixture solution of organic solvent and water. The purified compound represented by formula 1 is obtained.
摘要翻译： 提供由式1表示的化合物的纯化方法，其包括以下步骤：（1）在大孔吸附树脂上加载粗化合物1，（2）用水溶液，有机溶剂或混合物洗涤大孔吸附树脂 有机溶剂和水溶液，（3）用水溶液，有机溶剂或有机溶剂和水的混合溶液洗脱。 得到由式1表示的纯化化合物。
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3.发明申请AZACYCLOHEXAPEPTIDE OR ITS PHARMACEUTICAL ACCEPTABLE SALT, PREPARING METHOD AND USE THEREOF 审中-公开亚硫酸氢盐或其药学上可接受的盐，其制备方法和用途公开(公告)号：US20120190815A1
公开(公告)日：2012-07-26
申请号：US13389231
申请日：2009-08-06
申请人： Tianhui Xu , Tao Fang , Zhonghao Zhuo , Yunman Zheng , Xiaoming Ji
发明人： Tianhui Xu , Tao Fang , Zhonghao Zhuo , Yunman Zheng , Xiaoming Ji
摘要： The present invention disclosed a novel azacyclohexapeptide or pharmaceutically acceptable salts, preparation methods and uses thereof. The structure of the azacyclohexapeptide is represented by the following formula 4:
摘要翻译： 本发明公开了一种新的氮杂环己肽或其药学上可接受的盐，其制备方法和用途。 氮杂环六肽的结构由下式4表示：
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