摘要:
An annealing separator for manufacturing grain-oriented silicon steel with mirror-like surface having good magnetic performance consists of the composition of which is 77˜98 by wt % of Al2O3 powder, 1˜8 by wt % of alkaline earth powder, 1˜15 by wt % of alkali metal chloride and/or alkaline earth metal chloride. The annealing separator of the invention can avoid forming a glass-film undercoating on the surface of the steel sheet during high-temperature annealing, and at the same time, the oxide embedded at near-surface of the sheet is removed by means of corrosive reaction of the chloride, so that a produce with smooth surface and stable magnetic performance is obtained.
摘要:
A method of manufacturing oriented Si steel containing Cu with high electric-magnetic property comprises: hot rolling slab; after first cold rolling, heating it to 800° C. or higher temperature and performing intermediate decarburization annealing in a protective atmosphere with PH2O/PH2 of 0.50˜0.88 for 3-8 minutes, to decrease carbon content of the steel plate to less than 30 ppm; then peening and acid-pickling to remove oxide of Fe on surface and to control oxygen content to lower than 500 ppm; secondary cold rolling to final thickness and coating separation agent in water-slurry form; drying to decrease water content to lower than 1.5%; high-temperature annealing in a protective atmosphere containing hydrogen with oxidation degree (PH2O/PH2) of 0.0001-0.2; finally applying a tension coating and leveling tension annealing.
摘要:
A method of manufacturing oriented Si steel containing Cu with high electric-magnetic property comprises: hot rolling slab; after first cold rolling, heating it to 800° C. or higher temperature and performing intermediate decarburization annealing in a protective atmosphere with PH2O/PH2 of 0.50˜0.88 for 3-8 minutes, to decrease carbon content of the steel plate to less than 30 ppm; then peening and acid-pickling to remove oxide of Fe on surface and to control oxygen content to lower than 500 ppm; secondary cold rolling to final thickness and coating separation agent in water-slurry form; drying to decrease water content to lower than 1.5%; high-temperature annealing in a protective atmosphere containing hydrogen with oxidation degree (PH2O/PH2) of 0.0001-0.2; finally applying a tension coating and leveling tension annealing.
摘要:
A manufacturing method of oriented Si steel with high electric-magnetic property comprises the following steps: smelting steel in converter or electric furnace; refining molten steel in two stages; continuous casting to obtain slab; hot rolling; first cold rolling; decarburizing annealing; secondary cold rolling; applying an annealing separator based on MgO and annealing at high temperature; applying an insulating coating and leveling tension annealing. The slab comprises (in wt %): C 0.020-0.050%, Si 2.6-3.6%, S 0.015-0.025%, Als 0.008-0.028%, N 0.005-0.020%, Mn 0.15-0.5%, Cu 0.3-1.2%, balance Fe and inevitable impurities, in which 10≦Mn/S≦20 and Cu/Mn≧2. The method could produce oriented Si steel with high magnetic induction intensity and low iron loss at low cost.
摘要:
A manufacturing method of oriented Si steel with high electric-magnetic property comprises the following steps: smelting steel in converter or electric furnace; refining molten steel in two stages; continuous casting to obtain slab; hot rolling; first cold rolling; decarburizing annealing; secondary cold rolling; applying an annealing separator based on MgO and annealing at high temperature; applying an insulating coating and leveling tension annealing. The slab comprises (in wt %): C 0.020-0.050%, Si 2.6-3.6%, S 0.015-0.025%, Als 0.008-0.028%, N 0.005-0.020%, Mn 0.15-0.5%, Cu 0.3-1.2%, balance Fe and inevitable impurities, in which 10≦Mn/S≦20 and Cu/Mn≧2. The method could produce oriented Si steel with high magnetic induction intensity and low iron loss at low cost.
摘要:
The invention provides a method for producing grain-oriented silicon steel with single cold rolling, comprising: 1) smelting, refining and continuous casting to obtain a casting blank; 2) hot rolling; 3) normalization, i.e. normalizing annealing and cooling; 4) cold-rolling, i.e. single cold rolling at a cold rolling reduction rate of 75-92%; 5) decarburizing annealing at 780-880° C. for 80-350 s in a protective atmosphere having a due point of 40-80° C., wherein the total oxygen [O] in the surface of the decarburized sheet: 171/t≦[O]≦313/t (t represents the actual thickness of the steel sheet in mm), the amount of absorbed nitrogen: 2-10 ppm; 6) high temperature annealing, wherein the dew point of the protective atmosphere: 0-50° C., the temperature holding time at the first stage: 6-30 h, the amount of absorbed nitrogen during high-temperature annealing: 10-40 ppm; 7) hot-leveling annealing. The invention may control the primary recrystallization microstructure of steel sheet effectively by controlling the normalization process of hot rolled sheet to form sufficient favorable (Al, Si)N inclusions from nitrogen absorbed by slab during decarburizing annealing and low-temperature holding of high-temperature annealing, facilitating the generation of stable, perfect secondary recrystallization microstructure of the final products. In addition, the invention avoids the impact of nitridation using ammonia on the underlying layer in prior art, and thus the formation of a good glass film underlying layer is favored.
摘要:
The invention provides a method for producing grain-oriented silicon steel with single cold rolling, comprising: 1) smelting, refining and continuous casting to obtain a casting blank; 2) hot rolling; 3) normalization, i.e. normalizing annealing and cooling; 4) cold-rolling, i.e. single cold rolling at a cold rolling reduction rate of 75-92%; 5) decarburizing annealing at 780-880° C. for 80-350 s in a protective atmosphere having a due point of 40-80° C., wherein the total oxygen [0] in the surface of the decarburized sheet: 171/t≦[O]≦313/t (t represents the actual thickness of the steel sheet in mm), the amount of absorbed nitrogen: 2-10 ppm; 6) high temperature annealing, wherein the dew point of the protective atmosphere: 0-50° C., the temperature holding time at the first stage: 6-30 h, the amount of absorbed nitrogen during high-temperature annealing: 10-40 ppm; 7) hot-leveling annealing. The invention may control the primary recrystallization microstructure of steel sheet effectively by controlling the normalization process of hot rolled sheet to form sufficient favorable (Al, Si)N inclusions from nitrogen absorbed by slab during decarburizing annealing and low-temperature holding of high-temperature annealing, facilitating the generation of stable, perfect secondary recrystallization microstructure of the final products. In addition, the invention avoids the impact of nitridation using ammonia on the underlying layer in prior art, and thus the formation of a good glass film underlying layer is favored.
摘要:
A method for detecting electromagnetic property of oriented silicon steel, the method comprises: measuring Euler angles of each of crystal grains in a specimen by use of metallographic etch-pit method; calculating orientation deviation angle θi (degree) of the crystal grain; combining area Si (mm2) of the crystal grain and correction coefficient X of element Si (X=0.1˜10 T/degree); correcting on the basis of the magnetic property B0 (saturation magnetic induction, T) of single-crystal material by using these parameters (θi, Si, X), formula for correcting is B 8 = - 0.015 × X × ∑ n = 1 i S i θ i ∑ n = 1 i S i + ( B 0 - 0.04 ) ( 1 ) obtaining electromagnetic property B8 of the oriented silicon steel by the above calculations. The present invention can implement detection of electromagnetic property of a specimen under the circumstances that there is no magnetizm measuring device or that magnetizm measuring devices cannot be used due to reasons such as weight and size of the specimen being too small or surface quality of the specimen being poor.
摘要:
A method for manufacturing a grain-oriented silicon steel having excellent magnetic performance, comprising steps as follows 1)conventionally melting and casting into a steel blank; 2) heating the steel blank and hot rolling the same into a strip of steel; 3)normalizing process; carrying out the normalizing process having two stages, wherein the strip is firstly heated to 1100˜1200° C., then cooled to 900˜1000° C. within 50˜200 s; and next, the strip is rapidly cooled in water having a temperature of 10-100; in this period, a tension force is applied to the strip of steel, the strip of steel in the temperature range of 900 ° C.˜500° C. has a stress of 1˜200N/mm2; 4)cold rolling, i.e. carrying out a primary cold rolling, or a double cold rolling with intermediate annealing; 5)carrying out primary recrystallizing annealing, then coating an annealing separator, whose main composition is MgO, to carry out final product annealing comprising secondary recrystallizing annealing and purifying annealing. The invention optimizes the content and distribution of martensite in the steel plate after normalization by adjusting the tension force applied to the steel plate while normalization transformation, so as to make the content of martensite in the range ensuring a better magnetic performance of the final product and to optimize the magnetic performance of final products.
摘要:
A fast-speed laser scoring method is provided, in which a set of related laser scoring device is used to simultaneously score lines on the upper surface and the lower surface of an oriented silicon steel strip, which is being fed and traveling forwards on a production line, with high-focalized continuous wave laser beam; the lines scored on the upper surface and the lines scored on the lower surface have the same space between every two adjacent scored lines but are staggered each other in order to reduce iron loss evenly. The space between every two adjacent scored lines on the same surface is 6-12 mm, laser power is 1000-3000 W and scanning speed is 100-400 m/min. The machining rate of the scoring method and device attains 1.5-2 times the one of conventional scoring methods which can not simultaneously score the upper and lower surfaces of a steel strip at a time. The lines scored on a steel strip by the method can reduce iron loss of the strip by 10-16%.