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    Method for recovering di-trimethylolpropane by distillation
    2.
    发明授权
    Method for recovering di-trimethylolpropane by distillation 有权

    公开(公告)号：US09745236B2

    公开(公告)日：2017-08-29

    申请号：US14351306

    申请日：2012-10-24

    申请人： Oxea GmbH

    发明人： Guido D. Frey ,  Norman Nowotny ,  Kurt Schalapski ,  Heinz Strutz

    IPC分类号： B01D1/06 ,  B01D3/14 ,  C07C29/80 ,  C07C41/42 ,  C07C41/44 ,  C07C43/13

    CPC分类号： C07C29/80 ,  B01D1/06 ,  B01D1/065 ,  B01D3/14 ,  B01D3/143 ,  B01D3/148 ,  C07C41/42 ,  C07C41/44 ,  C07C43/13 ,  C07C43/132

    摘要： Distillative process for obtaining ditrimethylolpropane from solutions includes separating ditrimethylolpropane from the solution in a first distillation unit into a first tops fraction comprising low-boiling compounds having a lower boiling point than ditrimethylolpropane and a first bottoms fraction; introducing the first bottoms fraction into a second distillation unit having at least 5 theoretical plates, said unit being configured as a thin-film evaporator with a column attachment and drawing off a second tops fraction comprising intermediate-boiling compounds having a lower boiling point than ditrimethylolpropane as well as withdrawing a second bottoms fraction from the second distillation unit and introducing the second bottoms fraction into a third distillation unit having at least 4 theoretical plates, said unit being configured as a thin-film evaporator with a column attachment, such that ditrimethylolpropane is obtained as a third tops fraction and high boilers are removed as a third bottoms fraction.

    Glyceryl ether compounds and their use
    5.
    发明授权
    Glyceryl ether compounds and their use 有权
    甘油醚化合物及其用途

    公开(公告)号：US08575371B2

    公开(公告)日：2013-11-05

    申请号：US13656890

    申请日：2012-10-22

    申请人： Segetis, Inc.

    发明人： Sergey Selifonov

    IPC分类号： C07D317/18

    CPC分类号： C07D317/22 ,  A01N25/30 ,  C07C43/132 ,  C07C59/305 ,  C07C69/708 ,  C07D307/20 ,  C07D407/12

    摘要： Glyceryl ether compounds prepared by the reaction of glycerol and olefin epoxides are disclosed. The compounds are renewable biomass-based surfactants useful as detergents and emulsifiers in formulations for cleaning, laundry, personal care, cosmetics, and industrial uses.

    摘要翻译： 公开了通过甘油和烯烃环氧化物的反应制备的甘油醚化合物。 这些化合物是可用作清洁剂，洗衣，个人护理，化妆品和工业用途的制剂中的洗涤剂和乳化剂的可再生生物质基表面活性剂。

    Ether compounds
    8.
    发明授权
    Ether compounds 失效
    醚化合物

    公开(公告)号：US06790953B2

    公开(公告)日：2004-09-14

    申请号：US10205939

    申请日：2002-07-26

    申请人： Jean-Louis Henri Dasseux ,  Carmen Daniela Oniciu

    发明人： Jean-Louis Henri Dasseux ,  Carmen Daniela Oniciu

    IPC分类号： C07D29503

    CPC分类号： C07D233/72 ,  C07C43/132 ,  C07C59/125 ,  C07C311/04 ,  C07F9/091 ,  Y10S514/866 ,  Y10S514/909

    摘要： The present invention relates to novel ether compounds, compositions comprising ether compounds, and methods useful for treating and preventing cardiovascular diseases, dyslipidemias, dysproteinemias, and glucose metabolism disorders comprising administering a composition comprising an ether compound. The compounds, compositions, and methods of the invention are also useful for treating and preventing Alzheimer's Disease, Syndrome X, peroxisome proliferator activated receptor-related disorders, septicemia, thrombotic disorders, obesity, pancreatitis, hypertension, renal disease, cancer, inflammation, and impotence. In certain embodiments, the compounds, compositions, and methods of the invention are useful in combination therapy with other therapeutics, such as hypocholesterolemic and hypoglycemic agents.

    摘要翻译： 本发明涉及新型醚化合物，包含醚化合物的组合物和用于治疗和预防心血管疾病，血脂异常，dysproteinemias和葡萄糖代谢紊乱的方法，包括施用包含醚化合物的组合物。 本发明的化合物，组合物和方法还可用于治疗和预防阿尔茨海默病，综合征X，过氧化物酶体增殖物激活受体相关病症，败血症，血栓形成障碍，肥胖症，胰腺炎，高血压，肾脏疾病，癌症，炎症和 阳。 在某些实施方案中，本发明的化合物，组合物和方法可用于与其它治疗剂如降胆固醇和降血糖药物组合治疗。

    Processes for preparing linear polyglycerols and polyglycerol esters
    9.
    发明申请
    Processes for preparing linear polyglycerols and polyglycerol esters 有权
    制备线性聚甘油和聚甘油酯的方法

    公开(公告)号：US20020058781A1

    公开(公告)日：2002-05-16

    申请号：US10012026

    申请日：2001-11-06

    发明人： Daniel Wayne Lemke

    IPC分类号： C08K003/22 ,  C08K003/18 ,  C08L001/00

    CPC分类号： C07C67/08 ,  C07C41/09 ,  C07C67/03 ,  C07C69/52 ,  C07C69/33 ,  C07C69/003 ,  C07C43/132 ,  C07C43/135

    摘要： Applicant has discovered processes for preparing polyglycerols and polyglycerol esters in high yield and with minimal formation of cyclic polyglycerols and cyclic polyglycerol esters. Furthermore, the processes of this invention produce a high proportion of linear polyglycerols and polyglycerol esters. The linear polyglycerols have very desirable physical characteristics, including a clear appearance at melt, a desirable Gardner color, a mild odor, and a bland taste. The polyglycerols and polyglycerol esters prepared by the method of the present invention are well suited for use as cosmetic and food additives. Since few, if any, cyclic polyglycerols and polyglycerol esters are formed by the processes of this invention, costly and time consuming distillation steps to remove such by-products are not needed. More specifically, applicants have discovered that if a calcium containing compound, such as calcium hydroxide, is used in place of potassium or sodium hydroxide during polymerization of glycerol, polyglycerol, or a mixture thereof or esterification of polyglycerols, the formation of cyclic polyglycerols is greatly reduced. One embodiment of the invention is a method of preparing a polyglycerol comprising polymerizing glycerol, polyglycerol, or a mixture thereof in the presence of a calcium containing compound, such as calcium hydroxide. Preferably, the calcium containing compound is present in a catalytically effective amount. Another embodiment is a method of preparing a polyglycerol ester by esterifying a polyglycerol in the presence of a calcium containing compound.

    摘要翻译： 申请人已经发现了以高产率制备聚甘油和聚甘油酯并且形成环状聚甘油和环状聚甘油酯的方法。 此外，本发明的方法产生高比例的线性聚甘油和聚甘油酯。 线性聚甘油具有非常理想的物理特性，包括在熔融时的清晰外观，所需的加纳尔颜色，温和的气味和平淡的味道。 通过本发明的方法制备的聚甘油和聚甘油酯非常适合用作化妆品和食品添加剂。 由于通过本发明的方法形成了少量（如果有的话）环状聚甘油和聚甘油酯，所以不需要昂贵且耗时的蒸馏步骤来除去这些副产物。 更具体地，申请人已经发现，如果在甘油，聚甘油或其混合物或聚甘油的酯化反应期间使用钙等化合物如氢氧化钙代替氢氧化钾或氢氧化钠，则聚环氧甘油的形成大大 减少 本发明的一个实施方案是制备聚甘油的方法，其包括在含钙化合物如氢氧化钙的存在下聚合甘油，聚甘油或其混合物。 优选地，含钙化合物以催化有效量存在。 另一个实施方案是通过在含钙化合物的存在下酯化聚甘油来制备聚甘油酯的方法。

    Process for recovering ditrimethylolpropane
    10.
    发明申请
    Process for recovering ditrimethylolpropane 审中-公开
    回收二羟甲基丙烷的方法

    公开(公告)号：US20020033325A1

    公开(公告)日：2002-03-21

    申请号：US09918648

    申请日：2001-08-01

    发明人： Teruyuki Ninomiya ,  Toshio Watanabe ,  Atsushi Iwamoto ,  Soemu Miyashita ,  Masafumi Watanabe

    IPC分类号： B01D003/12 ,  B01D009/00 ,  C07C027/28

    CPC分类号： C07C41/01 ,  C07C41/40 ,  C07C41/42 ,  C07C43/132

    摘要： The present invention provides a process for recovering ditrimethylolpropane from a still residue obtained by extracting and then distilling off trimethylolpropane from a reaction solution obtained by reacting n-butyraldelhyde with formaldehyde in the presence of a basic catalyst, wherein the still residue is distilled to remove high-boiling components therefrom, and the resultant distillate is subjected to crystallization. When the above process is combined with the acid decomposition, it becomes possible to decompose a linear formal compound obtained from 2 molecules of TMP contained in the still residue as crude TMP and one molecule of formaldehyde, so that di-TMP having a higher purity is obtained.

    摘要翻译： 本发明提供从通过在碱性催化剂存在下将正丁醛与甲醛反应获得的反应溶液萃取，然后蒸馏出三羟甲基丙烷所得的静止残余物中回收二羟甲基丙烷的方法，其中将残余物蒸馏除去高 沸腾成分，并使得到的馏出物进行结晶。 当上述方法与酸分解结合时，可以将残留物中所含的2分子TMP得到的线性形式化合物分解为粗TMP和一分子甲醛，使得具有较高纯度的二-TMP为 获得。