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    PENTAMETHINE CYANINE FLUORESCENT DYES, PREPARATION METHODS AND USES THEREOF
    1.
    发明申请
    PENTAMETHINE CYANINE FLUORESCENT DYES, PREPARATION METHODS AND USES THEREOF 有权
    戊胺衍生物荧光染料，其制备方法及其用途

    公开(公告)号：US20130309715A1

    公开(公告)日：2013-11-21

    申请号：US13982089

    申请日：2011-01-31

    申请人： Xiaojun Peng ,  Zhigang Yang ,  Yanxia He ,  Jingyun Wang ,  Jiangli Fan ,  Shiguo Sun ,  Fengling Song

    发明人： Xiaojun Peng ,  Zhigang Yang ,  Yanxia He ,  Jingyun Wang ,  Jiangli Fan ,  Shiguo Sun ,  Fengling Song

    IPC分类号： G01N33/52

    CPC分类号： G01N33/52 ,  C07D403/06 ,  C09B23/0008 ,  C09B23/005 ,  C09B23/0058 ,  C09B23/08

    摘要： A pentamethine cyanine fluorescent dye having the general formula I, a synthetic method and a use thereof are disclosed. In the general formula, X is CHO or CHCR3R4; R1 and R2 are independently selected from the group consisting of (CH2)nR2 and et al.; R3 and R4 are independently selected from the group consisting of CN, COOH and COOR16; R5, R6 and R7 are independently selected from the group consisting of H, SO3R10 and COOR11; R8 is H or C1-18 alkyl; R9 is H or CH3; R10 is N(R12R13R14R15); R11 is C1-18 alkyl; R12, R13, R14, R15 and R16 are independently selected from the group consisting of H, C1-18 alkyl, (CH2)mOR8 and (CHR9CH2O)pR8; Y− is halogen anion or OTs−; and n, m and p are integers of 0-18. The dye can be utilized to sensitively detect viscosity of micro-environment such as tissues and cells.

    摘要翻译： 公开了具有通式I的合成方法及其用途的五甲代花青荧光染料。 在通式中，X是CHO或CHCR3R4; R 1和R 2独立地选自（CH 2）n R 2等。 R3和R4独立地选自CN，COOH和COOR16; R5，R6和R7独立地选自H，SO3R10和COOR11; R8是H或C1-18烷基; R9为H或CH3; R10为N（R12R13R14R15）; R11为C1-18烷基; R 12，R 13，R 14，R 15和R 16独立地选自H，C 1-18烷基，（CH 2）mOR 8和（CHR 9 CH 2 O）p R 8; Y-是卤素阴离子或OTs-; 并且n，m和p是0-18的整数。 染料可用于敏感地检测微环境如组织和细胞的粘度。

    Hydrophilic, thiol-reactive cyanine dyes and conjugates thereof with biomolecules for fluorescence diagnosis
    3.
    发明申请
    Hydrophilic, thiol-reactive cyanine dyes and conjugates thereof with biomolecules for fluorescence diagnosis 审中-公开
    亲水性，硫醇反应性花青染料及其与生物分子的缀合物用于荧光诊断

    公开(公告)号：US20040260072A1

    公开(公告)日：2004-12-23

    申请号：US10762582

    申请日：2004-01-23

    发明人： Kai Licha ,  Christin Perlitz

    IPC分类号： C07K014/47 ,  C07D417/02 ,  C07D413/02 ,  C07D43/02

    CPC分类号： C09B23/0008 ,  C09B23/0025 ,  C09B23/005 ,  C09B23/0066 ,  C09B23/086 ,  G01N33/533 ,  G01N33/582

    摘要： This invention relates to new fluorescence dyes from the class of cyanine dyes, especially indotricarbocyanines with an absorption and fluorescence maximum in the spectral range of 700 to 900 nm, a thiol-specific reactive group, and three, preferably four, sulfonate groups, to an increase of water solubility as well as the production of dyes. This invention also relates to the conjugates of these dyes with biomolecules and uses thereof.

    摘要翻译： 本发明涉及一种来自花青染料的新型荧光染料，特别是在700-900nm的光谱范围内具有吸收和荧光最大值，硫醇特异性反应性基团和三个，优选四个磺酸盐基团的吲哚氰菊酯， 增加水溶性以及生产染料。 本发明还涉及这些染料与生物分子的缀合物及其用途。

    Sulfonyl-containing styrene derivatives and their use in electrophotographic processes
    4.
    发明授权
    Sulfonyl-containing styrene derivatives and their use in electrophotographic processes 失效
    含磺酰基的苯乙烯衍生物及其在电子照相方法中的应用

    公开(公告)号：US4869983A

    公开(公告)日：1989-09-26

    申请号：US831450

    申请日：1986-02-20

    申请人： Albert Bender ,  Dieter Guenther ,  Juergen Lingnau

    发明人： Albert Bender ,  Dieter Guenther ,  Juergen Lingnau

    IPC分类号： G03G5/00 ,  C07D239/42 ,  C07D279/02 ,  C09B23/00 ,  C09B23/01 ,  C09B23/10 ,  G03G5/06 ,  G03G5/09 ,  H05K1/03

    CPC分类号： C07D239/42 ,  C07D279/02 ,  C09B23/005 ,  C09B23/105 ,  G03G5/09 ,  H05K1/0346

    摘要： Method and composition for a sulfonyl-containing styrene derivative of the general formula ##STR1## in which R.sub.1 and R.sub.2 are identical or different and denote hydrogen, optionally halogen-, hydroxyl-, cyano- or (C.sub.1 -C.sub.4 -alkoxy mono- or poly-substituted (C.sub.1 -C.sub.8)-alkyl or phenyl, R.sub.3 denotes hydrogen or a (C.sub.1 -C.sub.4)-alkyl or -alkoxy group, n is a number from 1 to 4 or R.sub.1, R.sub.2 and R.sub.3 together with the associated aminophenyl radical denote julolidinyl or N-(C.sub.1 -C.sub.3)-alkylcarbazol-3-yl, R.sub.4 and R.sub.5 denote hydrogen or the necessary valences for forming a condensation product with formamide derivatives, and R.sub.6 denotes a cyano group, or R.sub.4 denotes hydrogen and R.sub.5 and R.sub.6 together denote the grouping C.dbd.N--R.sub.7, with R.sub.7 being a benzoyl radical which is unsubstituted or substituted by (C.sub.1 -C.sub.4)-alkyl or -alkoxy groups, halogen, cyno, amino or mono- or di-(C.sub.1 -C.sub.4)-alkylamino groups, to a process for their preparation and to their use as dyes or in electrophotographic recording materials.

    摘要翻译： 其中R 1和R 2相同或不同并表示氢，任选地为卤素，羟基，氰基或（C 1 -C 4 - 烷氧基单 - 或多）的通式为“IMAGE”的含磺酰基的苯乙烯衍生物的方法和组合物 取代的（C 1 -C 8） - 烷基或苯基，R 3表示氢或（C 1 -C 4） - 烷基或烷氧基，n是1至4的数，或R 1，R 2和R 3与相应的氨基苯基表示 四环素基或N-（C 1 -C 3） - 烷基咔唑-3-基，R 4和R 5表示氢或用于与甲酰胺衍生物形成缩合产物的必需化合价，R 6表示氰基，或R 4表示氢，R 5和R 6一起 表示分组C = N-R7，其中R 7为未被取代或被（C 1 -C 4） - 烷基或 - 烷氧基，卤素，c，氨基或单 - 或二 - （C 1 -C 4） - 烷基氨基，其制备方法及其作为染料或电子照相记录材料的用途。

    Thermal print element comprising a yellow merocyanine dye stabilized with a cyan indoaniline dye
    5.
    发明授权
    Thermal print element comprising a yellow merocyanine dye stabilized with a cyan indoaniline dye 失效
    热敏打印元件包含用青色苯并苯胺染料稳定的黄色部花青染料

    公开(公告)号：US4748149A

    公开(公告)日：1988-05-31

    申请号：US77364

    申请日：1987-07-24

    申请人： Gary W. Byers

    发明人： Gary W. Byers

    IPC分类号： B41M5/26 ,  B41M5/385 ,  B41M5/39

    CPC分类号： B41M5/3858 ,  C09B23/005 ,  C09B23/0058 ,  C09B23/06 ,  C09B23/105 ,  C09B55/002 ,  B41M5/3854 ,  B41M5/39 ,  Y10S428/913 ,  Y10S428/914 ,  Y10S430/146 ,  Y10T428/24901 ,  Y10T428/31507 ,  Y10T428/31786

    摘要： A thermal print element comprising a support having thereon a layer containing a thermally-transferred dye image, the dye image comprising a yellow merocyanine dye having the formula: ##STR1## wherein: A represents --COR, --COOR, --CONHR, --CN, --SO.sub.2 R or --SO.sub.2 NR.sub.2 ; or A may be combined together withR.sup.4 to form a heterocyclic or carbocyclic ring system;R.sup.4 represents --NHR, --NR.sub.2, --OR, --SR, or --R;n represents 0 to 1;Z represents the atoms necessary to complete a5- or 6-membered substituted or unsubstituted heterocyclic ring; andeach R independently represents a substituted or unsubstituted alkyl or aryl group;the dye image also comprising a cyan indoaniline dye in the same areas as the yellow merocyanine dye to provide improved stability to light for the yellow merocyanine dye, the cyan indoaniline dye having the formula: ##STR2## wherein: R.sup.1 and R.sup.2 are each independently hydrogen or a substituted or unsubstituted alkyl, cycloalkyl, or aryl group;R.sup.3 is hydrogen, a substituted or unsubstituted alkyl group, halogen, --NHCOR.sup.1 or --NHSO.sub.2 R.sup.1 ; andX represents hydrogen or the atoms necessary to complete a 5- or 6-membered, substituted or unsubstituted, carbocyclic or heterocyclic ring system.

    Monomethine dyestuffs
    6.
    发明授权
    Monomethine dyestuffs 失效
    单甲基染料

    公开(公告)号：US4018796A

    公开(公告)日：1977-04-19

    申请号：US558647

    申请日：1975-03-17

    申请人： Horst Harnisch

    发明人： Horst Harnisch

    IPC分类号： C09B57/02 ,  C09B23/01 ,  D06P1/00 ,  D06P1/13 ,  D06P5/00 ,  D06P5/28 ,  C07D311/06

    CPC分类号： C09B23/0058 ,  C09B23/005 ,  D06P1/0012 ,  D06P1/13 ,  D06P5/006

    摘要： The invention relates to monomethine dyestuffs of the formula ##STR1## wherein Z.sup.1 is alkyl, cycloalkyl, aralkyl or arylZ.sup.2 is hydrogen or Z.sup.1Q is CN, COOR.sup.2 or CONR.sup.3 R.sup.4,R.sup.1 u.R.sup.4 is hydrogen or alkyl,R.sup.2 is alkyl, alkenyl, aralkyl, cycloalkyl or aryl andR.sup.3 is alkyl, cycloakyl, aralkyl, aryl or acyl.The dyestuffs are suitable for the dyeing of natural and synthetic fibers, which are dyed in orange or red shades with high brilliancy.

    摘要翻译： 本发明涉及下式的单甲基染料，其中Z1是烷基，环烷基，芳烷基或芳基，Z2是氢或Z1Q是CN，COOR2或CONR3R4，R1u.R4是氢或烷基，R2是烷基，链烯基，芳烷基 ，环烷基或芳基，R3是烷基，环烷基，芳烷基，芳基或酰基。

    Azolindolines and azolindoline dyestuffs
    7.
    发明授权
    Azolindolines and azolindoline dyestuffs 失效
    唑啉酮和唑啉二酚染料

    公开(公告)号：US4016172A

    公开(公告)日：1977-04-05

    申请号：US434022

    申请日：1974-01-17

    申请人： Horst Harnisch

    发明人： Horst Harnisch

    IPC分类号： C07D473/00 ,  C07D498/04 ,  C09B23/01 ,  C09B23/10 ,  C09B23/16 ,  C09B69/06 ,  D06P1/90 ,  C07D263/56

    CPC分类号： C09B23/164 ,  C07D473/00 ,  C09B23/005 ,  C09B23/0058 ,  C09B23/105 ,  C09B69/06 ,  D06P1/908

    摘要： Azolindolines of the formula ##STR1## wherein Z represents hydrogen or an optionally modified aldehyde group,R.sub.1 and R.sub.2 denote alkyl or represent the remaining members of a cycloalkyl radical,R.sub.3 denotes alkyl or aralkyl,X represents oxygen, sulphur or --NR.sub.4,whereinR.sub.4 denotes hydrogen or alkyl, cycloalkyl or aralkyl, and A represents the remaining members of an aromatic radical,As well as their preparation, and, moreover, compounds of the formula ##STR2## wherein A, X, R.sub.1, R.sub.2 and R.sub.3 have the same meaning as above and R.sub.5 denotes alkyl or aralkylAs well as their preparation and their use for the dyeing of synthetic fiber materials.

    摘要翻译： 其中Z代表氢或任选改性的醛基的式IMAMA的唑啉酮，R 1和R 2表示烷基或代表环烷基的剩余成员，R 3表示烷基或芳烷基，X表示氧，硫或-NR 4，其中R 4 表示氢或烷基，环烷基或芳烷基，A表示芳族基团的剩余成员，以及其制备方法，以及更优选的化合物，其中A，X，R 1，R 2和R 3具有相同 如上所述，R 5表示烷基或芳烷基，作为其制备及其用于合成纤维材料的染色的用途。

    Novel basic indoline dyestuffs
    8.
    发明授权
    Novel basic indoline dyestuffs 失效
    新型基础吲哚衍生物

    公开(公告)号：US3850913A

    公开(公告)日：1974-11-26

    申请号：US26531972

    申请日：1972-06-22

    申请人： BAYER AG

    发明人： PSAAR H

    IPC分类号： C07D209/08 ,  C09B23/01 ,  C09B23/10 ,  C09B23/00

    CPC分类号： C09B23/0033 ,  C07D209/08 ,  C09B23/005 ,  C09B23/0058 ,  C09B23/105 ,  Y10S8/927

    摘要： 1. BASIC DYESTUFF OF THE FORMULA

    (1-R3,2-((2-R1,3,3-DI(H3C-),5-R-INDOLIN-1-YL)-CH=C(-R2)-),

    3,3-DI(H3C-),5-R4-INDOLE)(+) AN(-)

    WHEREIN R AND R4, INDEPENDENTLY OF EACH OTHER, ARE HYDROOGEN, ALKYL OF 1-6 CARBON ATOMS, CYCLOPENTYL, CYCLOHEXYL, PHENYL, NAPHTHYL, PHENYLALKYL OF 1-6 CARBON ATOMS IN THE ALKYL PORTION, ALKOXY OF 1-6 CARBON ATOMS, NAPHTHYLOXY, PHENYLOXY, BENZYLOXY, ALKYLAMINO OF 1-6 CARBON ATOMS, CYCLOHEXYLAMINO, PHENYLAMINO, NAPHTHYLAMINO, BENZYLAMINO, ACETYLAMINO, ETHYLUREIDO, SULFONAMIDO, ALKYLSULFONAMIDO OF 1-6 CARBON ATOMS, PHENYLSULFONAMIDO, NAPHTHYSULFONAMIDO, CARBAMETHOXY, CARBOXAMIDO, HALO, CYANO, OR THE AFORESAID RADICALS WHEREIN THE ALKYL PORTION OF THE AROMATIC RING IS FURTHER SUBSTITUTED BY HALO, HYDROXY, CYCLOHEXYL, CYCLOPENTYL, ALKOXY OF 1-6 CARBON ATOMS BENZYLOXY, PHENYLOKY, ALKOXYCARBONYL OR 1-6 CARBON ATOMS IN THE ALKYL PORTION, CYANO, AMINOCARBONYL, AMINO ALKYLAMINO OR 1-6 CARBON ATOMS DIALKYLAMINO OF 1-6 CARBON ATOMS IN EACH ALKYL PORTION, ACETYLAMINO, SULFONYLAMINO, MERCAPTO, ALKYLMERCAPTO OF 1-6 CARBON ATOMS, OR PHENYLMERCAPTO; AND ADDITIONALLY WHEREIN THE AROMATIC RING IS SUBSTITUTED BY ALKYL OF 1-6 CARBON ATOMS;R1 IS ALKYL OR 1-6 CARBON ATOM, PHENYLALKYL OR 1-6 CARBON ATOMS IN THE ALKYL PORTION, OR THE AROMATIC RADICALS WHEREIN THE ALKYL PORTION OR THE AROMATIC RING FURTHER SUBSTITUTED BY HALO, HYDROXY CYCLOHEXYL, CYCLOPENTYL, ALKOXY OR 1-6 CARBON ATOMS, BENZYLOXY, PHENYLOXY, ALKOXYCARBONYL OR 1-6 CARBON ATOMS IN THE ALKYL PORTION, CYANO, AMINOCARBONYL, AMINO, ALKYLAMINO OF 1-6 CARBON ATOMS, DIALKYLAMINO OF 1-6 CARBON ATOMS IN EACH ALKYL PORTION, ACETYLAMINO, SULFONYLAMINO, MERCAPTO, ALKYLMERCAPTO OF 1-6 CARBON ATOMS, OR PHENYLMERCAPTO; AND ADDITIONALLY WHEREIN THE AROMATIC RING IS SUBSTITUTED BY ALKYL OF 1-6 CARBON ATOMS; R2 IS HYDROGEN, ALKYL OF 1-6 CARBON ATOMS, CYANO, CARBOXAMIDO, ALKYLSULFONYL OR 1-6 CARBON ATOMS, OR SAID ALKYL OR ALKYLSULFONYL WHEREIN THE ALKYL PORTION IS FURTHER SUBSTITUTED BY HALO, HYDROXY, CYCLOHEXYL, CYCLOPENTYL, ALKOXY OF 1-6 CARBON ATOMS, BENZYLOXY, PHENYLOXY, ALKOXYCARBONYL OR 1-6 CARBON ATOMS IN THE ALKYL PORTION, CYANO, AMINOCARBONYL, AMINO, ALKYLAMINO OF 1-6 CARBON ATOMS, DIALKYLAMINO OF 1-6 CARBON ATOMS, IN EACH ALKYL PORTION, ACETYLAMINO, SULFONYLAMINO, MERCAPTO, ALKYLMERCAPTO OF 1-6 CARBON ATOMS, OR PHENYLMERCAPTO; R3 IS ALKYL OR 1-6 CARBON ATOMS, PHENYLALKYL OR 1-6 CARBON ATOMS IN THE ALKYL PORTION, OR THE AFORESAID RADICALS WHEREIN THE ALKYL PORTION OR THE AROMATIC RING IS FURTHER SUBSTITUTED BY HALO, HYDROXY, CYCLOHEXYL, CYCLOPENTYL, ALKOXY OR 1-6 CARBON ATOMS, BENZYLOXY, PHENYLOXY, ALKOXYCARBONYL OF 1-6 CARBON ATOMS IN THE ALKYL PORTION, CYANO, AMINOCARBONYL, AMINO ALKYLAMINO OF 1-6 CARBON ATOMS, DIALKYLAMINO OF 1-6 CARBON ATOMS IN EACH ALKYL PORTION, ACETYLAMINO, SULFONYLAMINO, MERCAPTO, ALKYLMERCAPTO OF 1-6 CARBON ATOMS, OR PHENYLMERCAPTO; AND ADDITIONALLY WHEREIN THE AROMATIC RING IS SUBSTITUTED BY ALKYL OF 1-6 CARBON ATOMS; AND AN (-) IS AN ANION.