公开(公告)号：US20160002749A1

公开(公告)日：2016-01-07

申请号：US14770843

申请日：2014-09-02

申请人： JX Nippon Mining & Metals Corporation

发明人： Kazuto Yagi

IPC分类号： C22B47/00 ,  C22C22/00 ,  C22B9/04 ,  C22B5/16 ,  C22B9/00

CPC分类号： C22B47/00 ,  C22B5/16 ,  C22B9/003 ,  C22B9/006 ,  C22B9/04 ,  C22C22/00 ,  C23C14/3414

摘要： The present invention relates to a method for manufacturing a high purity Mn, the method comprising: placing a flake-like electrolytic Mn raw material in a magnesia crucible to perform melting with the use of a vacuum induction melting furnace (VIM furnace) at a melting temperature of 1240 to 1400° C. under an inert atmosphere of 500 Torr or less; then adding calcium in a range between 0.5 and 2.0% of the weight of Mn to perform deoxidation and desulfurization; casting the resultant in an iron mold after the completion of the deoxidation and desulfurization to manufacture an ingot; then placing the Mn ingot into a magnesia crucible to perform melting with the use of a vacuum induction melting furnace (VIM furnace) at a melting temperature, which is adjusted to 1200 to 1450° C. and maintained for 10 to 60 minutes, under an inert atmosphere of 200 Torr or less; casting the resultant in an iron mold to manufacture an ingot; then placing the metal Mn ingot in an alumina crucible; reducing pressure to 0.01 Torr with a vacuum pump; and then heating to develop a sublimation and distillation reaction. Provided is a method for manufacturing a high purity metal Mn from a commercially available electrolytic Mn. In particular, an object is to obtain a high purity metal Mn in which the amount of impurities such as B, Mg, Al and Si is small.

摘要翻译： 高纯度Mn的制造方法技术领域本发明涉及一种高纯度Mn的制造方法，其特征在于，包括：将薄片状电解Mn原料放置在氧化镁坩埚中，使用真空感应熔炼炉（VIM炉）进行熔融， 温度为1240〜1400℃，在500乇以下的惰性气氛中， 然后加入在Mn重量的0.5〜2.0％范围内的钙进行脱氧脱硫; 在脱氧脱硫完成后将铸件铸造在铁模上制造锭; 然后将Mn锭放入氧化镁坩埚中，使用真空感应熔炼炉（VIM炉）在熔融温度下进行熔融，熔融温度调节至1200至1450℃并保持10至60分钟， 200乇以下的惰性气氛; 在铁模中铸造所得物以制造锭; 然后将金属Mn锭放置在氧化铝坩埚中; 用真空泵减压至0.01乇; 然后加热开发升华和蒸馏反应。 提供从市售的电解Mn制造高纯度金属Mn的方法。 特别地，目的是获得其中诸如B，Mg，Al和Si的杂质的量小的高纯度金属Mn。

公开(公告)号：US08685138B2

公开(公告)日：2014-04-01

申请号：US13610551

申请日：2012-09-11

申请人： Erik D. Grimm

发明人： Erik D. Grimm

IPC分类号： C22B9/00 ,  C22B21/00 ,  F27B7/12 ,  F27B14/14 ,  F27D1/18

CPC分类号： F27B14/14 ,  C22B9/006 ,  C22B21/0069 ,  C22B21/0092 ,  F27B7/12 ,  F27B7/2083 ,  F27B7/24 ,  F27B7/3205 ,  F27D1/18 ,  Y02P10/218

摘要： A tilting rotary furnace with a door assembly that seals against a furnace vessel. The seal between the door and the furnace vessel allows for regulation of the internal environment of the furnace and control over thermitting of the aluminum. As a result, aluminum recovery may be carried out without the use of salt. A portion of the door may rotate with the furnace vessel and a portion of the door may remain rotationally stationary with respect to the furnace vessel and the rotating portion of the door.

摘要翻译： 一种倾斜旋转炉，其具有密封炉膛的门组件。 门和炉容器之间的密封件允许调节炉的内部环境并控制铝的熔化。 结果，可以不使用盐进行铝的回收。 门的一部分可以与炉容器一起旋转，并且门的一部分可以相对于炉容器和门的旋转部分保持旋转静止。

公开(公告)号：US20130000450A1

公开(公告)日：2013-01-03

申请号：US13610551

申请日：2012-09-11

申请人： Erik D. Grimm

发明人： Erik D. Grimm

IPC分类号： C22B21/00

CPC分类号： F27B14/14 ,  C22B9/006 ,  C22B21/0069 ,  C22B21/0092 ,  F27B7/12 ,  F27B7/2083 ,  F27B7/24 ,  F27B7/3205 ,  F27D1/18 ,  Y02P10/218

摘要： A tilting rotary furnace with a door assembly that seals against a furnace vessel. The seal between the door and the furnace vessel allows for regulation of the internal environment of the furnace and control over thermitting of the aluminum. As a result, aluminum recovery may be carried out without the use of salt. A portion of the door may rotate with the furnace vessel and a portion of the door may remain rotationally stationary with respect to the furnace vessel and the rotating portion of the door.

摘要翻译： 一种倾斜旋转炉，其具有密封炉膛的门组件。 门和炉容器之间的密封件允许调节炉的内部环境并控制铝的熔化。 结果，可以不使用盐进行铝的回收。 门的一部分可以与炉容器一起旋转，并且门的一部分可以相对于炉容器和门的旋转部分保持旋转静止。

公开(公告)号：US20120145353A1

公开(公告)日：2012-06-14

申请号：US13384142

申请日：2010-07-15

申请人： Jumpei Nakayama ,  Tatsuhiko Kusamichi

发明人： Jumpei Nakayama ,  Tatsuhiko Kusamichi

IPC分类号： B22D7/00 ,  B22D23/00

CPC分类号： C22B9/003 ,  C21C7/064 ,  C21C7/068 ,  C22B9/006 ,  C22B9/10 ,  Y02P10/253

摘要： Disclosed is a method for producing alloy ingot including: a step of: charging alloy starting material into a cold crucible in a cold-crucible induction melter, and forming melt pool of the alloy starting material by induction heating in inert gas atmosphere; a step of continuing the induction heating and adding first refining agent to the melt pool, and then reducing the content of at least phosphorus from among impurity elements present in the melt pool; and a step of forming alloy ingot by solidifying the melt, the phosphorus content of which has been reduced. The first refining agent is mixture of metallic Ca and flux, where the flux contains CaF2 and at least one of CaO and CaCl2. The weight proportion of the sum of CaO and CaCl2 with respect to CaF2 ranges from 5 to 30 wt % and the weight proportion of metallic Ca with respect to the melt pool is 0.4 wt % or greater.

摘要翻译： 公开了一种合金锭的制造方法，其特征在于，包括以下步骤：将合金原料装入冷坩埚感应熔炉中的冷坩埚中，并通过在惰性气体气氛中感应加热形成合金原料的熔池; 继续感应加热并将第一精炼剂加入到熔池中，然后从存在于熔池中的杂质元素中减少至少磷的含量的步骤; 以及通过使熔融物固化而形成合金锭的步骤，其中磷含量已经降低。 第一精炼剂是金属Ca和助熔剂的混合物，其中助熔剂含有CaF 2和CaO和CaCl 2中的至少一种。 CaO和CaCl 2之和相对于CaF 2的重量比例为5〜30重量％，金属Ca相对于熔融池的重量比例为0.4重量％以上。

公开(公告)号：US20100310411A1

公开(公告)日：2010-12-09

申请号：US12867668

申请日：2009-02-13

申请人： Satoru Ohsaki ,  Tatsuya Takahashi ,  Koji Kajikawa ,  Eiji Maeda ,  Yoshikuni Kadoya ,  Ryuichi Yamamoto ,  Takashi Nakano

发明人： Satoru Ohsaki ,  Tatsuya Takahashi ,  Koji Kajikawa ,  Eiji Maeda ,  Yoshikuni Kadoya ,  Ryuichi Yamamoto ,  Takashi Nakano

IPC分类号： C22C19/05 ,  C22C30/00

CPC分类号： C22F1/10 ,  B22D7/005 ,  C22B9/006 ,  C22C19/055 ,  C22C19/056 ,  C22C19/057

摘要： A subject for the invention is to diminish the occurrence of streak-type segregation in producing a material comprising a Ni-based superalloy.The invention relates to a Ni-based superalloy having excellent unsusceptibility to segregation, characterized by comprising: 0.005 to 0.15 mass % of C; 8 to 22 mass % of Cr; 5 to 30 mass % of Co; equal to or greater than 1 and less than 9 mass % of Mo; 5 to 21 mass % of W; 0.1 to 2.0 mass % of Al; 0.3 to 2.5 mass % of Ti; up to 0.015 mass % of B; and up to 0.01 mass % of Mg, with the remainder comprising Ni and unavoidable impurities.

摘要翻译： 本发明的主题是减少在制造包含Ni基超级合金的材料时的条纹型偏析的发生。 本发明涉及具有优异的偏析性不良的Ni基超级合金，其特征在于包括：C：0.005〜0.15质量％ 8〜22质量％的Cr; Co：5〜30质量％ 等于或大于1且小于9质量％的Mo; W：5〜21质量％ Al：0.1〜2.0质量％ 0.3〜2.5质量％的Ti; 高达0.015质量％的B; 和0.01质量％的Mg，其余为Ni和不可避免的杂质。

公开(公告)号：US20100263848A1

公开(公告)日：2010-10-21

申请号：US12662263

申请日：2010-04-08

申请人： Yuuichi Aoki

发明人： Yuuichi Aoki

IPC分类号： F28F1/00 ,  B32B15/04 ,  B32B3/10 ,  C22B21/00

CPC分类号： C22B9/006 ,  B32B15/017 ,  C22B21/06 ,  C23C8/02 ,  C23C28/322 ,  C23C28/34 ,  F28F3/12 ,  F28F21/084 ,  F28F2013/006 ,  H01L21/4871 ,  H01L23/3735 ,  H01L23/4334 ,  H01L23/473 ,  H01L2224/48091 ,  H01L2224/48247 ,  H01L2224/73265 ,  H01L2924/13055 ,  Y10T428/24612 ,  Y10T428/31678 ,  H01L2924/00014 ,  H01L2924/00

摘要： Molten aluminum is heated in the range of 900° C. to 1300° C. under a nitrogen atmosphere using magnesium as an auxiliary agent to form aluminum nitride directly on the molten aluminum and bond the aluminum nitride to the aluminum so that an Al—AlN composite material is formed. Because aluminum nitride power needs not to be sintered at high temperature equal to or higher than 1900° C., the Al—AlN composite material can be formed at low temperature in the range of 900° C. to 1300° C. compared with the high temperature equal to or higher than 1900° C., and thereby the high-density aluminum nitride can be obtained.

摘要翻译： 使用镁作为助剂，将熔融铝在900℃〜1300℃的范围内加热，直接在熔融铝上形成氮化铝，并将氮化铝与铝结合，使Al-AlN 形成复合材料。 因为氮化铝功率不需要在等于或高于1900℃的高温下烧结，所以Al-AlN复合材料可以在900℃至1300℃的低温下形成，与 高温等于或高于1900℃，从而可以获得高密度氮化铝。

公开(公告)号：US20100116453A1

公开(公告)日：2010-05-13

申请号：US12578195

申请日：2009-10-13

申请人： John R. Grassi ,  John Campbell ,  Christopher Shaw

发明人： John R. Grassi ,  John Campbell ,  Christopher Shaw

IPC分类号： B22D18/06 ,  B22D27/00

CPC分类号： C22B9/006 ,  B22D18/06 ,  C21C5/567 ,  C22B9/023 ,  C22B21/0084 ,  C22B21/06 ,  F27B3/045 ,  F27D3/145 ,  Y02P10/234

摘要： A quiescent melt handling system includes a melting furnace and a holding furnace communicating with the melting furnace for holding a molten metal melt. The holding furnace has a relatively large surface area and a relatively shallow depth, having a width to depth ratio in the range of 4-100 to 1. Also provided is structure in the holding furnace for separating inclusions from the melt in the holding furnace. A mold communicates with the holding furnace. A counter gravity casting system, which might comprise a vacuum assisted casting system, draws the melt into the mold.

摘要翻译： 静态熔体处理系统包括熔化炉和与熔化炉连通以保持熔融金属熔体的保持炉。 保持炉具有相对较大的表面积和相对较浅的深度，其深度比在4-100:1的范围内。还提供了用于从夹持炉中的熔体中分离夹杂物的保持炉中的结构。 模具与保温炉相通。 可以包括真空辅助铸造系统的反向重力铸造系统将熔体吸入模具中。

公开(公告)号：US07550027B2

公开(公告)日：2009-06-23

申请号：US11979175

申请日：2007-10-31

申请人： Hiroshi Sanui ,  Yuji Nomura ,  Hidetoshi Ohta

发明人： Hiroshi Sanui ,  Yuji Nomura ,  Hidetoshi Ohta

IPC分类号： C22B26/00 ,  C22C1/06 ,  C22B11/10 ,  C22B9/00 ,  C22C1/00

CPC分类号： B22D21/007 ,  C22B9/006 ,  C22B9/05 ,  C22B26/22

摘要： In order to provide a method for supplying a cover gas which has sufficient preventive effects of oxidation-combustion and prevents cost-increase by containing a necessary and sufficient amount of fluoroketone in the cover gas which is supplied in a melting furnace of magnesium, the present invention provides a method for supplying a cover gas containing fluoroketone in a melt furnace to prevent oxidation and combustion of a melt of magnesium in the melt furnace, wherein the moisture concentration of gas in the melt furnace is measured, and the concentration of fluoroketone in the cover gas is adjusted to a range from 1/50 to 1/5 relative to the moisture concentration.

摘要翻译： 为了提供一种用于提供具有足够的氧化燃烧预防效果的覆盖气体的方法，并且通过在供给到镁的熔化炉中的覆盖气体中含有必要且足够量的氟代酮来防止成本增加， 本发明提供了一种在熔融炉中供给含有氟酮的覆盖气体的方法，以防止熔融炉中的镁熔体的氧化和燃烧，其中测量熔融炉中的气体的水分浓度，并且测量其中的氟酮的浓度 覆盖气体相对于水分浓度被调节到1/50至1/5的范围。

公开(公告)号：US20090136884A1

公开(公告)日：2009-05-28

申请号：US12332666

申请日：2008-12-11

申请人： Stewart C. Jepson

发明人： Stewart C. Jepson

IPC分类号： C21B9/14 ,  F27D7/02

CPC分类号： C22B9/006 ,  C21D1/52 ,  C21D11/00 ,  C22B21/0084 ,  C22B21/064 ,  F27B17/0025 ,  F27D7/02 ,  F27D17/008 ,  F27D99/00 ,  F27D99/0033

摘要： A heating system includes a furnace configured to receive a product to be thermally treated within the furnace, where the furnace includes at least one burner to generate combustion gases from a source of oxygen and a carbon-based fuel source provided to the burner, and the combustion gases provide heat to the product disposed within the furnace. A gas pipeline delivers a heated inert gas into the furnace at a location proximate the product so as to at least partially surround and protect a surface of the product and minimize or prevent the product from chemically reacting with other gases within the furnace.

摘要翻译： 加热系统包括：炉子，其被配置为接收在炉内进行热处理的产品，其中炉子包括至少一个燃烧器以产生来自氧气源的燃烧气体和提供给燃烧器的碳基燃料源， 燃烧气体向设置在炉内的产品提供热量。 气体管道在靠近产品的位置将加热的惰性气体输送到炉中，以至少部分地围绕和保护产品的表面，并使产物与炉内的其它气体发生化学反应最小化或防止。

公开(公告)号：US20090100968A1

公开(公告)日：2009-04-23

申请号：US11976220

申请日：2007-10-23

申请人： Yuan-Pang Wu ,  Hui-Yun Bor ,  Rong-Ruey Jeng

发明人： Yuan-Pang Wu ,  Hui-Yun Bor ,  Rong-Ruey Jeng

IPC分类号： C22B9/00 ,  C21D1/00

CPC分类号： C22B9/02 ,  C22B9/006 ,  C22B23/06 ,  C22B26/22 ,  C22C1/023 ,  C22C19/03 ,  F27B14/04 ,  F27B14/06 ,  F27B14/08 ,  F27D27/00 ,  Y02P10/234 ,  Y10S420/90

摘要： The present invention provides a method and apparatus for manufacturing high-purity hydrogen storage alloy Mg2Ni applicable to industry and capable of manufacturing continuously. First, raw materials of magnesium-nickel with weight percentage of nickel between 23.5 and 50.2 are heated, melt, and mixed uniformly. Cool the magnesium-nickel liquid and control the temperature to be above the solidification temperature and below the liquification temperature in the phase diagram of magnesium-nickel. By making advantage of segregation principle in phase diagrams, solid-state high-purity γ-phase Mg2Ni hydrogen storage alloy is given. The residual waste magnesium-rich liquid in the crucible is poured to another independent crucible, and switch with the position of the crucible originally containing the γ-phase Mg2Ni hydrogen storage alloy. Then, new raw materials of magnesium and nickel are added and heated. Repeat the smelt steps described above continuously, and a continuous manufacturing method is introduced. After the original crucible is cooled, the solid substances at the bottom of the crucible can be tapped down without further special treatments. Then high-purity γ-phase Mg2Ni hydrogen storage alloy with atomic ratio of 2:1, no other phases, and with excellent hydrogen absorption-desorption dynamics is given.

摘要翻译： 本发明提供一种制造适用于工业并能连续制造的高纯度储氢合金Mg2Ni的方法和装置。 首先将镍 - 镍重量百分比为23.5〜50.2的原料加热熔融混合均匀。 在镁 - 镍相图中，冷却镁镍液体，控制温度高于固化温度，低于液化温度。 通过利用相图中的分离原理，给出了固态高纯度γ相Mg2Ni储氢合金。 将坩埚中剩余的富含镁的液体倒入另一个独立的坩埚中，并与原来含有γ相Mg2Ni储氢合金的坩埚的位置一起切换。 然后，加入和加热新的镁和镍原料。 重复上述熔融步骤，连续制造方法。 在原始坩埚冷却后，可以将坩埚底部的固体物质轻轻倒下，无需进一步的特殊处理。 然后提供原子比为2：1的高纯度γ相Mg2Ni储氢合金，没有其他相，并具有优异的氢吸收 - 解吸动力学。