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    Fluorescent whitening agents
    2.
    发明申请
    Fluorescent whitening agents 失效
    荧光增白剂

    公开(公告)号：US20010014989A1

    公开(公告)日：2001-08-23

    申请号：US09766984

    申请日：2001-01-22

    发明人： Peter Rohringer ,  Georges Metzger ,  Dieter Reinehr

    IPC分类号： D06L001/00 ,  C09B001/00 ,  C11D009/42

    CPC分类号： C09B23/148 ,  C07D251/68 ,  C11D3/42 ,  D06L4/621 ,  D06L4/657 ,  D06L4/75 ,  D06M13/07 ,  D06M13/358 ,  D06P1/6426 ,  D21H21/30 ,  Y10S8/919

    摘要： The present invention provides new compounds having the formula: 1 in which X is O or, preferably, NH; M is hydrogen, an alkali metal atom, ammonium or a cation formed from an amine; each R1, independently, is an aminoacid residue from which a hydrogen atom on the amino group has been removed; n is 1 or 2; and each R2, independently, is hydrogen, C1-C3alkyl, halogen, cyano, COOR in which R is hydrogen or C1-C3alkyl, CONH-R in which R has its previous significance, SO2NH-R in which R has its previous significance, NH-COR in which R has its previous significance, SO3M in which M has its previous significance or, when n is 1, R2 can also be CO-R3 in which R3 is C1-C3alkyl or phenyl; provided that those compounds are excluded in which a) X is NH, n is 1 and R2 is SO3M in which M has its previous significance; or b) X is NH, n is 2 and one R2 is SO3M in which M has its previous significance, and the other R2 is hydrogen, methyl or halogen; or c) X is NH, n is 1, R1 is glycine and R2 is H or CO2H; or d) X is NH, n is 2, each R2 is SO3M in which M has its previous significance and the SO3M groups are in 2,5-positions in the phenyl ring and R1 is D,L-alanine, L-valine, L-leucine, L-isoleucine, L-threonine, L-aspartic acid, L-glutamic acid, L-phenylalanine, L-proline, (),L- methionine or glycine. Most of the new class of 4,4null-diaminostilbene-2,2null-disulfonic acid compounds are useful as fluorescent whitening agents, especially for paper.

    摘要翻译： 本发明提供了新的具有下式的化合物：其中X为O或优选为NH; M是氢，碱金属原子，铵或由胺形成的阳离子; 每个R 1独立地是氨基酸被除去的氨基酸残基; n为1或2; 并且每个R 2独立地是氢，C 1 -C 3烷基，卤素，氰基，其中R是氢或C 1 -C 3烷基的COOR，其中R具有其先前含义的CONH-R，其中R具有其先前含义的SO 2 NH- 其中R具有其先前含义的NH-COR，其中M具有其先前含义的SO 3 M，或当n为1时，R 2也可以是其中R 3为C 1 -C 3烷基或苯基的CO-R 3; 条件是排除这些化合物，其中a）X是NH，n是1，R2是其中M具有其先前意义的SO 3 M; 或b）X是NH，n是2，一个R2是SO3M，其中M具有其先前的含义，另一个R 2是氢，甲基或卤素; 或c）X是NH，n是1，R1是甘氨酸，R2是H或CO2H; 或d）X是NH，n是2，每个R2是SO3M，其中M具有其先前的意义，SO 3 M基团在苯环中是2.5位，R 1是D，L-丙氨酸，L-缬氨酸， L-亮氨酸，L-异亮氨酸，L-苏氨酸，L-天冬氨酸，L-谷氨酸，L-苯丙氨酸，L-脯氨酸，（），L-甲硫氨酸或甘氨酸。 大多数新类的4,4'-二氨基芪-2,2'-二磺酸化合物可用作荧光增白剂，特别是用于纸。

    Methods of recovering waste fibers
    3.
    发明授权
    Methods of recovering waste fibers 失效
    回收废物纤维的方法

    公开(公告)号：US3843321A

    公开(公告)日：1974-10-22

    申请号：US28538972

    申请日：1972-08-30

    申请人： JOHNSON & JOHNSON

    发明人： DRELICH A

    IPC分类号： D06L4/75 ,  D21C5/02 ,  D06M13/10 ,  D06M11/14

    CPC分类号： D21C5/022 ,  D06L4/75 ,  D21C5/02 ,  Y02W30/648

    摘要： 1. A METHOD OF RECOVERING WASTE FIBERS FROM A MIXTURE OF WASTE AND SYNTHETIC, CROSS-LINKED RESIN BINDER MATERIALS WHICH COAT OR IMPREGNATE SAID WASTE FIBERS WHICH COMPRISES:HEATING SAID MIXTURE OF WASTE FIBERS AND SYNTHETIC, CROSS-LINKED RESIN BINDER MATERIALS WHICH COAT OR IMPREGNATE SAID WASTE FIBERS WITHIN THE RANGE OF FROM ABOUT 212*F. TO ABOUT 275*F. FOR A PERIOD OF FROM BOUT 3/4 HOUR TO ABOUT FIVE HOURS IN AN AQUEOUS TREATING SOLUTION CONTAINING AN ALKALI METAL HYDROXIDE AND A NORMALLY LIQUID, ORGANIC COMPOUND SELECTED FROM THE GROUP CONSISTING OF HYDROCARBON KETONES, ALCOHOLS, LACTONES AND SULFOXIDES, SAID NORMALLY LIQUID ORGANIC COMPOUND BEING SUFFICIENTLY WATER-SOLUBLE AS TO BE CAPABLE OF FORMING AQUEOUS SOLUTIONS OF AT LEAST ABOUT TWO PERCENT BY WEIGHT; ADDING A NEUTRAL OR ALKALINE OXIDIZING AGENT TO THE MIXTURE OF WASTE FIBERS AND SYNTHETIC, CROSS-LINKED RESIN MATERISL; HEATING THE MIXTURE OF WASTE FIBERS AND SYNTHETIC, CROSSLINKED MATERIALS IN THE PRESENCE OF SAID NEUTRAL OR ALKALINE OXIDIZING AGENT TO PARTIALLY DECOMPOSE OR SOLUBILIZE THE SYNTHETIC, CROSS-LINKED RESIN; AND RECOVERING THE WASTE FIBERS FROM THE MIXTURE OF WASTE FIBERS AND DECOMPOSED OR SOLUBILIZED SYNTHETIC, CROSS-LINKED RESIN MATERIALS.

    PROCESS TO PRODUCE HYGIENICALLY CLEAN TEXTILE
    5.
    发明申请
    PROCESS TO PRODUCE HYGIENICALLY CLEAN TEXTILE 审中-公开
    生产卫生清洁纺织品的工艺

    公开(公告)号：US20160168780A1

    公开(公告)日：2016-06-16

    申请号：US14571394

    申请日：2014-12-16

    申请人： Washing Systems, LLC

    发明人： Ryan Coggeshall ,  Adam Stein

    IPC分类号： D06L3/16 ,  D06L3/08

    CPC分类号： D06L4/75 ,  C11D3/3956 ,  C11D11/0017 ,  D06L4/24

    摘要： Textiles are hygienically cleaned by subjecting them to a low-temperature wash, generally less than 140°, and typically about 100° F. Once cleaned, they are subjected to a low temperature bleaching step at a pH of generally around 9 or less. The bleaching step is again conducted a low temperature, such as 140°, 100° F. Treated textiles can then be rinsed and treated to any typical post-washing operations. By conducting the washing and the bleaching at low temperatures, energy is saved. Further, maintaining the low temperature and low pH for the bleaching solution achieves better disinfection and, at the same time, minimizes damage to the textile.

    摘要翻译： 纺织品通过经受低温洗涤（通常小于140°，通常约100°F）进行卫生清洁。一旦清洁，将其进行低于约9或更低pH的低温漂白步骤。 漂白步骤再次进行低温，例如140°，100°F。然后处理的纺织品可以冲洗并处理成任何典型的后洗涤操作。 通过在低温下进行洗涤和漂白，节省能量。 此外，保持漂白溶液的低温和低pH实现更好的消毒，同时最小化对织物的损害。

    BLEACHED FIBER PRODUCT PRODUCTION METHOD, APPARATUS TO BE USED THEREFOR, AND BLEACHED FIBER PRODUCT PRODUCED THEREBY
    7.
    发明申请
    BLEACHED FIBER PRODUCT PRODUCTION METHOD, APPARATUS TO BE USED THEREFOR, AND BLEACHED FIBER PRODUCT PRODUCED THEREBY 有权
    漂白纤维产品生产方法，其使用的设备和生产的漂白纤维产品

    公开(公告)号：US20100116450A1

    公开(公告)日：2010-05-13

    申请号：US12528534

    申请日：2007-12-26

    申请人： Shigenori Aono ,  Koichi Abe ,  Keigo Takeda

    发明人： Shigenori Aono ,  Koichi Abe ,  Keigo Takeda

    IPC分类号： D21C9/153 ,  D21F7/00

    CPC分类号： D06B23/28 ,  D06B5/16 ,  D06L4/50 ,  D06L4/75

    摘要： An inventive method includes the steps of: loading a fiber product in an appropriate form into a treatment vessel; wetting the fiber product; forcibly circulating an ozone-containing liquid in contact with the wetted fiber product to thereby bleach the fiber product; and forcibly circulating an ozone decomposing chemical agent liquid in contact with the ozone-treated fiber product to decompose ozone. This method ensures efficient bleaching of the fiber product with the ozone. Further, the method is advantageous in that the resulting bleached fiber product is less liable to be yellowed over time.

    摘要翻译： 本发明的方法包括以下步骤：以适当形式将纤维制品装载到处理容器中; 润湿纤维制品; 强制地将含有臭氧的液体与湿润的纤维产品接触，从而漂白纤维制品; 并强制循环与经臭氧处理的纤维制品接触的臭氧分解化学剂液体以分解臭氧。 该方法可确保纤维产品与臭氧的有效漂白。 此外，该方法的优点在于所得到的漂白纤维产品随着时间的推移不易变黄。

    Single-bath preparation of cellulosic materials
    8.
    发明申请
    Single-bath preparation of cellulosic materials 审中-公开
    纤维素材料的单浴制备

    公开(公告)号：US20030041387A1

    公开(公告)日：2003-03-06

    申请号：US10187518

    申请日：2002-07-01

    申请人： Novozymes North America, Inc.

    发明人： Hui Xu ,  Jiyin Liu ,  Eric Otto ,  Brian Condon

    IPC分类号： D06M010/00

    CPC分类号： D06L1/14 ,  D06L4/13 ,  D06L4/15 ,  D06L4/40 ,  D06L4/75

    摘要： The present invention provides methods for single-bath desizing, scouring and bleaching of cellulosic materials, which are carried out by contacting the cellulosic simultaneously or sequentially with an enzyme system and a peracid bleaching system under conditions that do not require emptying the bath or rinsing the cellulosic materials between desizing, scouring and bleaching steps.

    摘要翻译： 本发明提供了用于纤维素材料的单浴退浆，冲洗和漂白的方法，其通过在不需要排空浴或漂洗的条件下将纤维素同时或依次与酶系统和过酸漂白系统接触来进行 退浆，精练和漂白步骤之间的纤维素材料。

    Fluorescent whitening agents
    9.
    发明授权
    Fluorescent whitening agents 失效
    荧光增白剂

    公开(公告)号：US06458169B2

    公开(公告)日：2002-10-01

    申请号：US09767112

    申请日：2001-01-22

    申请人： Peter Rohringer ,  Georges Metzger ,  Dieter Reinehr

    发明人： Peter Rohringer ,  Georges Metzger ,  Dieter Reinehr

    IPC分类号： C07D25100

    CPC分类号： C09B23/148 ,  C07D251/68 ,  C11D3/42 ,  D06L4/621 ,  D06L4/657 ,  D06L4/75 ,  D06M13/07 ,  D06M13/358 ,  D06P1/6426 ,  D21H21/30 ,  Y10S8/919

    摘要： The present invention provides new compounds having the formula: in which X is O or, preferably, NH; M is hydrogen, an alkali metal atom, ammonium or a cation formed from an amine; each R1, independently, is an aminoacid residue from which a hydrogen atom on the amino group has been removed; n is 1 or 2; and each R2, independently, is hydrogen, C1-C3alkyl, halogen, cyano, COOR in which R is hydrogen or C1-C3alkyl, CONH—R in which R has its previous significance, SO2NH—R in which R has its previous significance, NH—COR in which R has its previous significance, SO3M in which M has its previous significance or, when n is 1, R2 can also be CO—R3 in which R3 is C1-C3alkyl or phenyl; provided that those compounds are excluded in which a) X is NH, n is 1 and R2 is SO3M in which M has its previous significance; or b) X is NH, n is 2 and one R2 is SO3M in which M has its previous significance, and the other R2 is hydrogen, methyl or halogen; or c) X is NH, n is 1, R1 is glycine and R2 is H or CO2H; or d) X is NH, n is 2, each R2 is SO3M in which M has its previous significance and the SO3M groups are in 2,5-positions in the phenyl ring and R1 is D,L-alanine, L-valine, L-leucine, L-isoleucine, L-threonine, L-aspartic acid, L-glutamic acid, L-phenylalanine, L-proline, D,L-methionine or glycine. Most of the new class of 4,4′-diaminostilbene-2,2′-disulfonic acid compounds are useful as fluorescent whitening agents, especially for paper.

    摘要翻译： 本发明提供了新的具有下式的化合物：其中X为O或优选为NH; M是氢，碱金属原子，铵或由胺形成的阳离子; 每个R 1独立地是氨基酸被除去的氨基酸残基; n为1或2; 并且每个R 2独立地是氢，C 1 -C 3烷基，卤素，氰基，其中R是氢或C 1 -C 3烷基的COOR，其中R具有其先前含义的CONH-R，其中R具有其先前含义的SO 2 NH- 其中R具有其先前意义的NH-COR，其中M具有其先前含义的SO 3 M，或当n为1时，R 2也可以是其中R 3为C 1 -C 3烷基或苯基的CO-R 3;条件是将这些化合物排除在 哪一个）X是NH，n是1，R2是SO3M，其中M具有其先前的意义; 环）X是NH，n是2，一个R2是SO3M，其中M具有其先前的意义，另一个R 2是氢，甲基或卤素; orc）X是NH，n是1，R1是甘氨酸，R2是H或CO2H; ord）X是NH，n是2，每个R2是SO3M，其中M具有其先前的意义，SO3M基团在苯环中是2,5位，R1是D，L-丙氨酸，L-缬氨酸，L L-亮氨酸，L-异亮氨酸，L-苏氨酸，L-天冬氨酸，L-谷氨酸，L-苯丙氨酸，L-脯氨酸，D，L-甲硫氨酸或甘氨酸。新的4,4'-二氨基芪 - 2,2'-二磺酸化合物可用作荧光增白剂，特别是用于纸。

    Method for delivering proper amounts of bleach and mill dye to discolored regions of a carpet using a roller-ball applicator
    10.
    发明授权
    Method for delivering proper amounts of bleach and mill dye to discolored regions of a carpet using a roller-ball applicator 有权

    公开(公告)号：US11846065B2

    公开(公告)日：2023-12-19

    申请号：US16997927

    申请日：2020-08-19

    申请人： Jerry Gordon Roper

    发明人： Jerry Gordon Roper

    IPC分类号： D06L4/26 ,  D06L4/75

    CPC分类号： D06L4/75 ,  D06L4/26

    摘要： A new method of delivering more precise amounts of carpet mill dye to regions of discoloration using a roller-ball applicator enables precisely metered delivery of the three primary dye colors to discolored carpet fibers. The method eliminates the need for a water extraction, enables the restoration of a more uniform color pattern, and eliminates dye overspray outside of the treated region that is inherent with the use of a spray bottle. The applicator is held with a loose grip and the roller ball is alternately moved in clockwise and counter-clockwise directions while in contact with the carpet fibers to be dyed. This ensures that dye is delivered to all sides of the fiber. To ensure even dye penetration and improved motion of the roller ball, an emulsifier is added to the dye solution. After each application, a microfilament cloth is wiped across the treated region.