公开(公告)号：US20040237716A1

公开(公告)日：2004-12-02

申请号：US10492246

申请日：2004-06-21

发明人： Yoshihiro Hirata ,  Yoshio Ueda ,  Hiroaki Takase ,  Kazuaki Suzuki

IPC分类号： B22F009/14

CPC分类号： B22F1/0022 ,  A61K33/24 ,  B22F9/14 ,  B22F2998/00 ,  B82Y30/00 ,  C02F1/005 ,  C02F1/444 ,  C02F1/4608 ,  C02F1/68 ,  C02F2001/46133 ,  C02F2103/026

摘要： Produce titanium-group metal micro-dispersion water that contains ion vapor of titanium-group metal in micro-dispersed state and that can be used as a material for health products, medical products, cosmetics, etc., by using an apparatus comprising a water tank, a high-voltage discharge generator equipped with a titanium-group metal electrode and its counter electrode, a water inlet, an outlet for produced water, and a titanium-group metal electrode feeder, in a manner causing plasma discharge in water between the titanium-group metal electrode and its counter electrode.

摘要翻译： 通过使用包含水的装置，生产含有微分散状态的钛族金属的离子蒸气的钛族金属微分散水，可用作保健品，医疗用品，化妆品等的材料 罐，配置有钛族金属电极及其对电极的高压放电发生器，进水口，出水口和钛族金属电极给料器，以使得水中的等离子体放电 钛族金属电极及其对电极。

公开(公告)号：US20040123699A1

公开(公告)日：2004-07-01

申请号：US10457957

申请日：2003-06-10

申请人： Industrial Technology Research Institute

发明人： Shih-Chieh Liao ,  Jin-Ming Chen ,  Song-Wein Hong ,  Zhong-Ren Wu

IPC分类号： B22F009/14

CPC分类号： B22F9/082 ,  B22F1/0044 ,  B22F2009/0836 ,  B22F2009/084 ,  B22F2009/0848 ,  B22F2009/086 ,  B22F2998/00 ,  B22F2999/00 ,  B22F1/0048 ,  B22F2202/03 ,  B22F9/14

摘要： The present invention relates to a nanostructured metal powder and a method of fabricating the same. A twin-wire electric arc process is performed to melt the wire tips, and metal melt is formed. Simultaneously, the metal melt is broken up into melt droplets by an atomizing device. The operating temperature of the electric arc process is controlled between melting point and boiling point of the wire, to avoid vaporization of the melt droplets. Then, a fast cooling is performed to quench the melt droplets. Thus, melt droplets are solidified to nullm-scaled, spherical and dense powders comprising nano-grains (d

摘要翻译： 纳米结构金属粉末及其制造方法技术领域本发明涉及纳米结构金属粉末及其制造方法。 进行双线电弧工艺以熔化线尖，并且形成金属熔体。 同时，通过雾化装置将金属熔体分解成熔体液滴。 电弧工艺的操作温度在熔丝和熔点之间进行控制，以避免熔体液滴的蒸发。 然后，进行快速冷却以淬灭熔体液滴。 因此，熔融液滴固化成包含纳米晶粒（d <100nm）的成瘤鳞片状，球形和致密的粉末。

公开(公告)号：US20040007093A1

公开(公告)日：2004-01-15

申请号：US10191957

申请日：2002-07-10

申请人： LEADER MACHINE CO., LTD

发明人： Shang-Wen Tang

IPC分类号： B22F009/14

CPC分类号： B22F9/12 ,  A61K33/24 ,  B22F2999/00 ,  B22F1/0081 ,  B22F2202/01

摘要： The present invention provides a method for producing gold powders. The method comprises providing a vacuum environment and using an electric target to vaporize a source gold to produce gold powders. A spinner is operated and provides ultrasonic vibration effects. The spinner has cooling devices on the inner wall of spinner to cool down the up-rising gold powers and reduce the adhesive force of the gold powders. A static-electronic collector is then used to collect the gold powders.

摘要翻译： 本发明提供一种金粉的制造方法。 该方法包括提供真空环境并使用电目标来蒸发源金以产生金粉末。 旋转器运行并提供超声波振动效果。 旋转器在旋转器内壁上具有冷却装置，以冷却上升的黄金功率并降低金粉的粘附力。 然后使用静电收集器收集金粉末。

公开(公告)号：US20030145681A1

公开(公告)日：2003-08-07

申请号：US10066365

申请日：2002-02-05

发明人： M. Samy El-Shall ,  Sarojini Deevi ,  Yezdi B. Pithawalla ,  Seetharama C. Deevi ,  A. Clifton Lilly JR.

IPC分类号： B22F009/14

CPC分类号： B82Y30/00 ,  B01J23/80 ,  B01J35/0013 ,  B22F9/12 ,  B22F2999/00 ,  C23C14/14 ,  C23C14/28 ,  B22F2202/11

摘要： A method of making Cu, Zn, and/or Cu/Zn alloy nanoparticles subjects one or more targets to laser energy to form a vapor and condenses the vapor to form nanoparticles having an average particle size of less than 20 nm. The optional application of an electric field results in nanoparticles with aspect ratios greater than 1.0. The target(s) can be a single target or separate targets comprising a mixture of copper, zinc, and/or copper/zinc. When separate targets are used, the laser beam can be split to form two separate beams each of which is made incident upon one of the targets. The nanoparticles can be formed in a chamber having an inert atmosphere or a reactive atmosphere and a convection current is created in the chamber by maintaining the top plate at a lower temperature than the bottom plate.

摘要翻译： 一种制备Cu，Zn和/或Cu / Zn合金纳米颗粒的方法使一个或多个靶发生激光能量以形成蒸气并使蒸气冷凝以形成平均粒度小于20nm的纳米颗粒。 电场的可选应用导致长宽比大于1.0的纳米颗粒。 靶可以是单个靶或包含铜，锌和/或铜/锌的混合物的单独靶。 当使用单独的目标时，激光束可以被分割以形成两个单独的光束，每个光束入射到其中一个目标上。 纳米颗粒可以在具有惰性气氛或反应性气氛的室中形成，并且通过将顶板保持在低于底板的温度下而在室中产生对流。

公开(公告)号：US20040103754A1

公开(公告)日：2004-06-03

申请号：US10387502

申请日：2003-03-14

发明人： Shuang-Shii Lian ,  Ming Lung Shih

IPC分类号： B22F009/14

CPC分类号： B22F9/14 ,  B22F9/10 ,  B22F2009/084 ,  B22F2999/00 ,  B22F2201/12

摘要： A process for manufacturing alloy powder with dual consumable rotary electrodes arc melting is suitable for manufacturing pure and low-surface-area powder of metal, active metals and their alloys. In the process, rotary electrode and tungsten electrode adopted by conventional rotary electrode and arc process for manufacturing powder are respectively replaced with a rotary or anodic electrode containing a first metal and a feed or cathodic electrode containing a second metal. An inert gas is supplied into equipment for implementing the process to serve as a protective atmosphere and stabilize generated electric arc. The cathodic electrode melts under the high temperature of the arc at a cathodic spot, and droplets of the molten cathodic or second metal are sprayed toward the anodic electrode to mix with molten anodic or first metal and thrown out by a centrifugal force of the rotary electrode to produce round-shaped alloy powder containing the first and the second metal.

摘要翻译： 制造具有双耗电旋转电极的合金粉末电弧熔炼的方法适用于制造金属，活性金属及其合金的纯低表面积粉末。 在此过程中，常规旋转电极采用的旋转电极和钨电极以及用于制造粉末的电弧工艺分别由含有第一金属和含有第二金属的进料或阴极电极的旋转或阳极电极代替。 将惰性气体供给到用于实施该过程的设备中以用作保护气氛并稳定产生的电弧。 阴极电极在阴极点处在电弧的高温下熔化，并将熔融的阴极或第二金属的液滴喷射到阳极电极，与熔融的阳极或第一金属混合并通过旋转电极的离心力 以生产含有第一和第二金属的圆形合金粉末。

公开(公告)号：US20020051728A1

公开(公告)日：2002-05-02

申请号：US09805366

申请日：2001-03-14

发明人： Koji Sato ,  Takeshi Kuboi ,  Masayoshi Date

IPC分类号： C22C013/00 ,  C22C013/02 ,  B22F009/06 ,  B22F009/14

CPC分类号： C22C13/02 ,  B22F1/0048 ,  B22F9/06 ,  B22F2999/00 ,  B23K35/0244 ,  B23K35/262 ,  C22C13/00 ,  H05K3/3436 ,  H05K3/3463 ,  H05K3/3478 ,  H05K2203/041 ,  Y02P70/613 ,  Y10S75/953 ,  B22F2202/01

摘要： A solder ball having a diameter of 1.2 mm or less, a dispersion of a diameter distribution of 5% or less and sphericity of 0.95 or more, an area ratio of the maximum dendrite being 80% or less of a cross section including a center of the solder ball, comprises a first additional element of 0.5-8 mass% of Ag and/or 0.1-3 mass % of Cu, and 0.006-10 mass %, in total, of at least one second additional element selected from the group consisting of Bi, Ge, Ni, P, Mn, Au, Pd, Pt, S, In and Sb, the balance being substantially Sn. The solder ball is produced by a uniform droplet-spraying method comprising the steps of vibrating a melt of a solder alloy in a crucible under pressure to force the melt to drop through orifices of the crucible; permitting the melt dropping through the orifices to become spherical droplets in a non-oxidizing gas atmosphere; and rapidly solidifying them.

摘要翻译： 直径为1.2mm以下的焊球，直径分布为5％以下，球形度为0.95以上的分散体，最大枝晶的面积比为包含中心的截面的80％以下 所述焊球包含0.5〜8质量％的Ag和/或0.1〜3质量％的Cu的第一附加元素和0.006〜10质量％的至少一种第二附加元素，所述至少一种第二添加元素选自 的Bi，Ge，Ni，P，Mn，Au，Pd，Pt，S，In和Sb，余量基本上为Sn。 焊球通过均匀的液滴喷涂方法制造，包括以下步骤：在坩埚内在压力下振动焊料合金的熔体，迫使熔体通过坩埚的孔口落下; 允许在非氧化性气体气氛中通过孔口的熔体熔滴成球形液滴; 并迅速凝固。

公开(公告)号：US20020029659A1

公开(公告)日：2002-03-14

申请号：US09860802

申请日：2001-05-18

发明人： Melissa Orme-Marmerelis ,  Robert F. Smith

IPC分类号： B22F009/14

CPC分类号： B22F9/08 ,  B22F2009/0816 ,  B22F2009/0836 ,  B22F2999/00 ,  H05K3/3457 ,  H05K3/3478 ,  B22F2202/01

摘要： In a high-speed fabrication process for producing highly uniform metallic microspheres, a molten metal is passed through a small orifice, producing a stream of molten metal therefrom. A series of molten metal droplets forms from the break up of the capillary stream. To achieve high uniformity of the spheres and avoid defects, the droplets are cooled before being captured. Separating the droplets, by causing them to travel in different paths than their adjacent droplets, helps to facilitate the cooling of the droplets. The droplets can be separated by electrostatically charging them as they break off from the capillary stream. The droplets are then passed through an electric field, which can be produced by a pair of deflection plates. The droplets are dispersed by varying the electric fieldnulle.g., by rotating the plates or by varying the voltage applied theretonullor by varying the electrostatic charge of the droplets. Advantageously, the droplets can be actively cooled in flight by passing them through a cryogenic gas chamber.

摘要翻译： 在用于生产高度均匀的金属微球的高速制造工艺中，熔融金属通过小孔，从中产生熔融金属流。 从毛细管流的分解形成一系列熔融金属液滴。 为了获得球的高度均匀性并避免缺陷，液滴在被捕获之前被冷却。 通过使液滴通过不同于其相邻液滴的路径进行分离，有助于液滴的冷却。 当液滴从毛细管流中分离时，它们可以通过静电充电来分离。 然后液滴通过电场，其可以由一对偏转板产生。 通过改变电场（例如通过旋转板或通过改变施加到其上的电压）或通过改变液滴的静电电荷来分散液滴。 有利地，液滴可以通过使它们通过低温气体室而在飞行中被主动冷却。

公开(公告)号：US20040231461A1

公开(公告)日：2004-11-25

申请号：US10492333

申请日：2004-06-22

发明人： Yoshihiro Hirata ,  Yoshio Ueda ,  Hiroaki Takase ,  Kazuaki Suzuki

IPC分类号： B22F009/14

CPC分类号： A61K8/044 ,  A23L33/16 ,  A23V2002/00 ,  A61K8/19 ,  A61K2800/83 ,  A61Q19/00 ,  A23V2200/254 ,  A23V2250/1568

摘要： Efficiently produce micro-dispersion water of super-fine noble metal particles having a desired concentration by using a very safe, compact production apparatus comprising a power supply for high-voltage/current discharge, a high-voltage discharge generator equipped with a noble metal electrode and its counter electrode, a water tank, a water inlet to the water tank, and an outlet for micro-dispersion water of super-fine noble metal particles, by causing plasma discharge in water between the noble metal electrode and its counter electrode and then causing the generated noble metal ion vapor to contact, and micro-disperse in, water. The obtained water can be effectively used as drinking water.

摘要翻译： 通过使用非常安全，紧凑的生产设备来有效地生产具有所需浓度的超细贵金属颗粒的微分散水，其包括用于高压/电流放电的电源，配备有贵金属电极的高压放电发生器 通过在贵金属电极与其对电极之间的水中引起等离子体放电，然后将其对置电极，水箱，水箱的进水口和超细贵金属颗粒的微分散水出口，然后 导致产生的贵金属离子蒸汽接触，并微分散在水中。 所得水可以有效地用作饮用水。

公开(公告)号：US20040079195A1

公开(公告)日：2004-04-29

申请号：US10450661

申请日：2003-12-15

发明人： Joseph W. Perry ,  Seth R. Marder ,  Francesco Stellacci

IPC分类号： B22F009/14

CPC分类号： B82Y30/00 ,  B22F1/0018 ,  B22F1/0022 ,  B22F2998/00 ,  B82Y10/00 ,  H01B1/02 ,  H01B1/22 ,  H01L21/76838 ,  Y10S977/783 ,  Y10T428/12181 ,  Y10T428/2991 ,  Y10T428/2998 ,  Y10T428/31855 ,  Y10T428/31942

摘要： Continous, conducting metal patterns can be formed from metal nanoparticle containing fils by exposure to radiation. The metal patterns can be one, two, or three dimensional and have high resolution resulting in feature sizes in the order of micron to nanometers

摘要翻译： 连续的，导电的金属图案可以通过暴露于辐射由含金属纳米颗粒的杂质形成。 金属图案可以是一维，二维或三维，并且具有高分辨率，导致特征尺寸为微米到纳米级

公开(公告)号：US20030164064A1

公开(公告)日：2003-09-04

申请号：US10335993

申请日：2003-01-02

申请人： Wm. Marsh Rice University

发明人： Nancy J. Halas ,  Robert Kelley Bradley

IPC分类号： B22F009/06 ,  B22F009/08 ,  B22F009/10 ,  B22F009/14

CPC分类号： B82Y30/00 ,  B22F1/0022 ,  B22F1/025

摘要： A method for purifying a suspension containing colloid-seeded nanoparticles and excess colloids is provided that includes adding to the suspension a filter aid comprising a salt. The method further includes filtering the suspension with a filter of a pore size intermediate between the average colloid-seeded nanoparticle size and the average excess colloid size, so as to form a retentate that includes the majority of the colloid-seeded nanoparticles and a filtrate that includes the majority of the excess colloids. Still further, the method includes collecting the retentate. The method may be incorporated into a method of making metallized nanoparticles, such as nanoshells, by reduction of metal ions onto the purified colloid-seed nanoparticles so as to form the metallized nanoparticles.

摘要翻译： 提供了一种用于纯化含有胶体接种的纳米颗粒和过量胶体的悬浮液的方法，其包括向悬浮液中加入包含盐的助滤剂。 该方法还包括用平均胶体接种的纳米颗粒尺寸和平均过量胶体尺寸之间的中等孔径的过滤器过滤悬浮液，以形成包含大部分胶体接种的纳米颗粒的保留物和滤液， 包括大部分过量胶体。 此外，该方法包括收集滞留物。 该方法可以通过将金属离子还原到纯化的胶体 - 种子纳米颗粒上以形成金属化纳米颗粒而被并入制备金属化纳米颗粒（例如纳米壳）的方法中。