Method of making super-hard articles

    公开(公告)号:US11261133B2

    公开(公告)日:2022-03-01

    申请号:US15327047

    申请日:2015-07-10

    发明人: Santonu Ghosh

    摘要: This application describes a method of making a super-hard article that includes a super-hard structure bonded to a substrate. The super-hard structure generally includes a sintered plurality of super-hard grains made from cubic boron nitride. The method generally includes providing raw material powder suitable for sintering the super-hard structure; combining the raw material powder with an organic binder material in a liquid medium to form a paste; providing a substrate assembly having a formation surface area configured for forming a boundary of the super-hard structure, the substrate having a recess coterminous with the formation surface area; extruding the paste into contact with the formation surface area to provide a paste assembly; and heat treating and/or sintering the paste assembly to remove the binder material and provide a pre-sinter assembly.

    Method for manufacturing graphitic sheet

    公开(公告)号:US10787366B2

    公开(公告)日:2020-09-29

    申请号:US16120494

    申请日:2018-09-04

    发明人: Shu-Chen Hsieh

    摘要: A method for manufacturing a graphitic sheet is used to obtain the graphitic sheet with similar characteristics to graphene. The method includes forming an octadecyltrichlorosilane (OTS) layer on a substrate to obtain a composite. The composite is annealed at 250-400° C. for 30-90 minutes, forming the graphitic sheet on the substrate via self-assembly of octadecyltrichlorosilane (OTS) in the OTS layer. The annealed composite is immersed in water, followed by being sonicated for 2 minutes with a frequency of 40 kHz and a power output of 200 W, to separate the graphitic sheet from the substrate.

    Polycrystalline abrasive constructions

    公开(公告)号:US10703679B2

    公开(公告)日:2020-07-07

    申请号:US15556256

    申请日:2016-03-08

    摘要: A method of manufacturing a polycrystalline abrasive construction comprises providing a plurality of particles of a superhard material, the particles coated with a first matrix precursor material, providing a plurality of second matrix precursor particles having an average size less than 2 micron, the second matrix precursor particles including a liquid phase sintering agent, mixing together the plurality of particles of superhard material with particles of the second matrix precursor material and consolidating and sintering the particles of superhard material and the particles of matrix precursor material. A polycrystalline abrasive construction comprises a particles of a superhard material dispersed in a matrix material comprising a material derived from a liquid phase sintering aid and chemical barrier particles having an average particle size of less than 100 nm dispersed in the matrix. Greater than 50% of the chemical barrier particles are located substantially at boundaries between superhard particles and the matrix.

    SUPERHARD CONSTRUCTIONS AND METHODS OF MAKING SAME

    公开(公告)号:US20190337855A1

    公开(公告)日:2019-11-07

    申请号:US16474290

    申请日:2017-12-28

    摘要: A super hard polycrystalline construction has a first region comprising a body of thermally stable polycrystalline super hard material having an exposed surface forming a working surface, and a peripheral side edge, said polycrystalline super hard material comprising a plurality of intergrown grains of super hard material; a second region forming a substrate to the first region; and a third region interposed between the first and second regions. The third region extends across a surface of the second region along an interface, the interface comprising at least a portion having an uneven topology, the third region comprising a composite material having a first phase comprising a plurality of non-intergrown grains of super hard material, and a matrix material, the third region having a wear resistance at least three times less than sintered polycrystalline diamond material having the same average grain size of diamond grains as the super hard grains in the third region.