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    Process for making alkyl naphthalene sulfonate surfactants
    2.
    发明授权
    Process for making alkyl naphthalene sulfonate surfactants 失效
    制备烷基萘磺酸盐表面活性剂的方法

    公开(公告)号：US5110981A

    公开(公告)日：1992-05-05

    申请号：US717131

    申请日：1991-06-18

    申请人： Norman Milstein

    发明人： Norman Milstein

    IPC分类号： B01F17/12 ,  C07C309/37 ,  C11D1/22

    CPC分类号： C11D1/22

    摘要： Incremental alternating additions of sulfonating agent acids and alkylating alcohols give superior results in the synthesis of alkyl naphthalene sulfonate surfactant products from naphthalene starting material.

    摘要翻译： 磺化剂酸和烷基化醇的增量交替添加在萘原料合成烷基萘磺酸盐表面活性剂产物方面提供了优异的结果。

    Preparation of improved alkylphenylsulfonates
    3.
    发明授权
    Preparation of improved alkylphenylsulfonates 失效
    改进的烷基苯基磺酸盐的制备

    公开(公告)号：US4298547A

    公开(公告)日：1981-11-03

    申请号：US176367

    申请日：1980-08-08

    申请人： Lewis B. Young

    发明人： Lewis B. Young

    IPC分类号： B01J29/06 ,  C07B61/00 ,  C07C4/06 ,  C07C67/00 ,  C07C301/00 ,  C07C303/06 ,  C07C309/31 ,  C07C309/37 ,  C07C143/24

    CPC分类号： C07C309/00 ,  C07C4/06 ,  C07C2529/40 ,  C07C2529/50 ,  C07C2529/65 ,  C07C2529/70

    摘要： An improved process for production of phenylalkylsulfonate compounds whereby the proportion of the 2-alkylphenylsulfonate isomer is reduced relative to the higher numbered isomers thereof (3-alkyl; 4-alkyl; etc.). After alkylation of aromatic compounds to produce a mixture of alkylbenzenes, the 2-alkylbenzene isomer is selectively cracked to lower boiling products, leaving the higher numbered isomers substantially unreacted. Subsequent sulfonation results in alkylphenylsulfonate derivatives having improved detergency properties.

    摘要翻译： 苯基烷基磺酸盐化合物的改进方法，其中2-烷基苯基磺酸酯异构体的比例相对于其较高数量的异构体（3-烷基; 4-烷基等）而降低。 在芳族化合物烷基化以产生烷基苯的混合物之后，2-烷基苯异构体选择性地裂解成较低沸点产物，留下较高数量的异构体基本上未反应。 随后的磺化导致烷基苯磺酸盐衍生物具有改善的去污力性能。

    Continuous process for sulfonating alkyl aromatics
    4.
    发明授权
    Continuous process for sulfonating alkyl aromatics 失效
    磺化烷基芳烃的连续方法

    公开(公告)号：US4113765A

    公开(公告)日：1978-09-12

    申请号：US741842

    申请日：1976-11-15

    申请人： Eugene E. Richardson ,  Frank Sidorowicz

    发明人： Eugene E. Richardson ,  Frank Sidorowicz

    IPC分类号： C07C303/06 ,  C07C309/31 ,  C07C309/37 ,  C07C309/38 ,  C07C143/24

    CPC分类号： C07C303/06 ,  C07C2103/24

    摘要： Disclosed is a continuous process for the sulfonation of an alkylaromatic reactant involving heating liquid sulfur trioxide in a vaporizer and mixing this sulfur trioxide gas stream with a hexane-alkylaromatic stream containing about 1 to about 3 wt. % quantity of a promoter, which can be either sulfuric acid or an alkyl benzene sulfonic acid, in a sulfonator - static inline mixer, mixing water with the sulfonated product as it passes to the water reactor - static inline mixer, passing the aqueous sulfonated product through degassing column-heat exchanger apparatus and separating the sulfonated product from the aqueous sulfuric acid. The reaction is conducted under controlled temperature and pressure conditions.

    摘要翻译： 公开了一种用于磺化烷基芳族反应物的连续方法，所述方法涉及在汽化器中加热液体三氧化硫，并将该三氧化硫气流与含有约1至约3重量％ 在磺化器 - 静态在线混合器中，可以是硫酸或烷基苯磺酸的促进剂的量的量，当水经过水反应器 - 静态在线混合器时，将水与磺化产物混合，将水性磺化产物 通过脱气柱 - 热交换器装置并将磺化产物与硫酸水溶液分离。 反应在控制的温度和压力条件下进行。

    Process for the production of aromatic sulfonates
    5.
    发明授权
    Process for the production of aromatic sulfonates 失效
    生产芳香磺酸盐的方法

    公开(公告)号：US3957859A

    公开(公告)日：1976-05-18

    申请号：US358312

    申请日：1973-05-08

    申请人： George W. Thielcke

    发明人： George W. Thielcke

    IPC分类号： C07C303/44 ,  C07C309/37 ,  C07C143/24

    CPC分类号： C07C303/44

    摘要： Aromatic sulfonates having, respectively, preferential oil-, and water- and alcohol-solubility are prepared by reacting aromatic compounds and sulfuric acid in a medium capable of liquid-liquid extraction with water; the product stream is then subjected to countercurrent extraction against water in a first multi-stage column; the water stream is next subjected to countercurrent extraction against a water-immiscible higher alcohol in a second multi-stage column; and the sulfonate having preferential water- and alcohol-solubility, which has transferred from the product stream, to the water stream, and finally to the higher alcohol, is recovered from the latter as the free acid or as a salt thereof. The process is especially adapted to the production of dinonylnaphthalene disulfonic acid.