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    Alicyclic alcohol
    1.
    发明授权
    Alicyclic alcohol 有权
    脂环醇

    公开(公告)号：US09056820B2

    公开(公告)日：2015-06-16

    申请号：US13977274

    申请日：2011-12-27

    申请人： Mitsuharu Kitamura ,  Yoshiharu Ataka ,  Kazuyuki Fukuda

    发明人： Mitsuharu Kitamura ,  Yoshiharu Ataka ,  Kazuyuki Fukuda

    IPC分类号： C07C31/135 ,  C11B9/00 ,  C07C29/147 ,  C07C53/44 ,  C07C35/08 ,  C07C29/149 ,  C07C51/58 ,  C07C67/14

    CPC分类号： C07C35/08 ,  C07C29/149 ,  C07C31/1355 ,  C07C51/58 ,  C07C67/14 ,  C07C2601/14 ,  C11B9/0034 ,  C07C61/08 ,  C07C69/75

    摘要： Provided is an alicyclic alcohol compound which can be used as a raw material for a compound perfume, and which has excellent floral-green-like aromas which are crisp and fresh; also provided are a manufacturing method for the same, and a perfume composition which contains the alicyclic alcohol compound. An alicyclic alcohol compound having a specified structure represented by chemical formula (1) has excellent floral-green-like aromas which are crisp and fresh; and a method for manufacturing the alicyclic alcohol compound represented by chemical formula (1) by reacting, in the presence of hydrogen fluoride, 1-isopropyl-4-methylcyclohexene and carbon monoxide, reacting the resulting 4-isopropyl-1-methylcyclohexane carboxylic acid fluoride with alcohol, and, after having acquired a cyclohexane carbonyl compound, reducing the cyclohexane carbonyl compound.

    摘要翻译： 提供可用作复合香料的原料的脂环族醇化合物，其具有优良的鲜绿色的花绿色香气， 还提供了其制备方法和含有脂环族醇化合物的香料组合物。 由化学式（1）表示的具有特定结构的脂环族醇化合物具有优异的花绿色香气，其清爽新鲜; 以及在氟化氢，1-异丙基-4-甲基环己烯和一氧化碳的存在下使化学式（1）表示的脂环族醇化合物的制造方法，使得到的4-异丙基-1-甲基环己烷羧酸氟化物 与醇反应后，在获得环己烷羰基化合物后，还原环己烷羰基化合物。

    Fluorinated carbocylic compounds
    3.
    发明授权
    Fluorinated carbocylic compounds 失效
    氟化碳环化合物

    公开(公告)号：US4792618A

    公开(公告)日：1988-12-20

    申请号：US680695

    申请日：1984-12-12

    申请人： Joseph F. Bieron ,  David Y. Tang

    发明人： Joseph F. Bieron ,  David Y. Tang

    IPC分类号： C07C51/567 ,  C07C69/75 ,  C07C49/303 ,  C07C53/44 ,  C07C121/46

    CPC分类号： C07C51/567

    摘要： Fluoro-substituted carbocyclic compounds are prepared by(A) reacting hydrogen fluoride with a chloro-cyclohexenyl compound of the formula ##STR1## where R.sub.1 and R.sub.2 are independently selected from the group consisting of --H, --CH.sub.2 OH, --COF, --COCl, --CF.sub.3, --CN, ##STR2## and --CH.sub.2 R, where R is --H or alkyl of 1-4 carbon atoms, to form a gem-dihalocyclohexane compound of the formula ##STR3## where X is chlorine and R.sub.1 and R.sub.2 are as defined above, (B) dehydrohalogenating the gem-dihalocyclohexane compound in the vapor phase to form a fluoro-cyclohexenyl compound of the formula ##STR4## (C) contacting the fluoro-cyclohexenyl compound, in the vapor phase, with a dehydrogenation catalyst to form a fluoro-substituted aromatic compound of the formula ##STR5##

    摘要翻译： 氟取代的碳环化合物是通过（A）使氟化氢与式（IMAGE）的氯 - 环己烯基化合物反应来制备的，其中R 1和R 2独立地选自-H，-CH 2 OH，-COF，-COCl， -CF 3，-CN，和-CH 2 R，其中R是-H或1-4个碳原子的烷基，以形成式为“IMAGE”的偕 - 二卤代环己烷化合物，其中X为氯，R 1和R 2为 （B）在蒸气相中脱氢卤化偕 - 二卤代环己烷化合物以形成下式的氟 - 环己烯基化合物：（C）使气相中的氟 - 环己烯基化合物与脱氢催化剂接触形成 具有下式的氟取代的芳族化合物

    Process for the preparation of acid chloride compounds
    6.
    发明授权
    Process for the preparation of acid chloride compounds 失效
    酰氯化合物的制备方法

    公开(公告)号：US5639888A

    公开(公告)日：1997-06-17

    申请号：US317260

    申请日：1994-10-03

    申请人： Michael John Bull ,  John Warcup Cornforth

    发明人： Michael John Bull ,  John Warcup Cornforth

    IPC分类号： C07C51/58 ,  C07D213/78 ,  C07D213/46 ,  C07C53/44 ,  C07C53/46

    CPC分类号： C07D213/78 ,  C07C51/58

    摘要： A process for preparing a compound of general formula ##STR1## where Ar represents an optionally substituted aromatic or heteroaromatic group, the process comprising reacting a compound of general formulaAr--C(L.sup.1).sub.2 Cl (II)where each L.sup.1 independently represents a leaving group (preferably a chlorine atom), with water in the presence of a Lewis acid and a chlorocarbon solvent which includes at least two chlorine atoms, is disclosed.

    摘要翻译： 制备通式为（I）的化合物的方法，其中Ar表示任选取代的芳族或杂芳族基团，该方法包括使通式为Ar-C（L 1）2 Cl（II）的化合物，其中每个L1独立地表示 公开了在含有至少两个氯原子的路易斯酸和氯化碳溶剂的存在下，离去基团（优选氯原子）与水。

    Adamantane compounds
    9.
    发明授权
    Adamantane compounds 失效
    ADAMANTANE化合物

    公开(公告)号：US3668220A

    公开(公告)日：1972-06-06

    申请号：US3668220D

    申请日：1970-04-27

    申请人： LILLY CO ELI

    发明人： SZINAI STEPHEN S ,  LUNN WILLIAM H W

    IPC分类号： C07C53/138 ,  C07C53/44 ,  C07C55/30 ,  C07C59/11 ,  C07D209/58 ,  C07D307/77 ,  C07D27/28

    CPC分类号： C07D209/58 ,  C07C53/138 ,  C07C53/44 ,  C07C55/30 ,  C07C59/11 ,  C07D307/77

    摘要： WHEREIN EACH G independently represents hydrogen or straightchain alkyl of from one to six, both inclusive, carbon atoms; G'' represents hydrogen or acetyl; R represents hydrogen or alkyl of from one to six, both inclusive, carbon atoms; R'' represents halo, alkoxy containing from one to six both inclusive, carbon atoms in the alkyl group, hydrogen or alkyl of from one to six, both inclusive, carbon atoms; each R'''' independently represents hydrogen or alkyl of from one to six, both inclusive, carbon atoms; each R'''''' independently represents hydrogen or alkyl of from one to six, both inclusive, carbon atoms or both R'''''' groups taken together represent oxo(-0); X represents halo; and each n independently represents an integer of from zero to one, both inclusive. The terms ''''halo'''' and ''''halide'''' are employed herein to designate occurrences of bromine, chlorine and iodine. The adamantane compounds of formula VII AND VIII are useful as agents to achieve a depressant action on the central nervous system of warm blooded animals. The adamantane compounds of formulas I, II, III, IV, V and VI are useful as intermediates in the synthesis of the compounds of formulas VII and VIII.

    The present invention is directed to adamantane compounds of the formula:

    摘要翻译： 本发明涉及下式的金刚烷化合物：其中每个G独立地表示氢或1-6个碳原子的直链烷基; G'表示氢或乙酰基; R表示氢或1-6个碳原子的烷基， R'表示卤素，含有一至六个或两个以上的烷氧基，烷基中的碳原子，氢或一至六个碳原子的烷基，包括两个碳原子; 每个R“独立地代表氢或一至六个碳原子的烷基; 每个R“独立地表示氢或一至六个，包括两端的碳原子的烷基或两个R”基团一起代表氧代（-O）; X表示卤素; 并且每个n独立地表示0至1的整数。 术语“卤素”和“卤化物”在本文中用于指定溴，氯和碘的出现。