Method of separating saccharides from aqueous product solution of cellulose hydrolysis process

    公开(公告)号:US10308991B2

    公开(公告)日:2019-06-04

    申请号:US15392632

    申请日:2016-12-28

    IPC分类号: C13K1/04

    摘要: A method of separating a saccharide from an aqueous product solution of the cellulose hydrolysis process is provided. The aqueous product solution comprises a saccharide and a cellulose swelling agent. The cellulose swelling agent is zinc chloride, magnesium chloride or a combination thereof. The method comprises the following steps in the given order: (a) adding a first tertiary amine and an optional first organic solvent to the aqueous product solution to provide a mixture; (b) performing a solid-liquid separation to obtain a solution from the mixture; and (c) performing a liquid-liquid extraction by adding a second tertiary amine and a second organic solvent to the solution, and then removing the organic phase and collecting the aqueous phase, wherein the first tertiary amine and the second tertiary amine are the same or different, and the first organic solvent and the second organic solvent are the same or different.

    SACCHARIFIED SOLUTION PRODUCTION METHOD AND SACCHARIFIED SOLUTION PRODUCTION APPARATUS THAT USE CELLULOSIC BIOMASS AS STARTING MATERIAL
    8.
    发明申请
    SACCHARIFIED SOLUTION PRODUCTION METHOD AND SACCHARIFIED SOLUTION PRODUCTION APPARATUS THAT USE CELLULOSIC BIOMASS AS STARTING MATERIAL 有权
    使用细胞生物质作为起始材料的解决方案生产方法和解决方案生产方法

    公开(公告)号:US20150329926A1

    公开(公告)日:2015-11-19

    申请号:US14655485

    申请日:2012-12-25

    IPC分类号: C13K1/04

    摘要: A saccharified solution production method includes: a saccharifying step of saccharifying hemicellulose or cellulose contained in cellulosic biomass to C5 or C6 saccharides by subjecting a slurry of cellulosic biomass to a hot water treatment in a supercritical state or subcritical state; a washing step of successively washing a solid in the slurry with washing water after the saccharifying step, by using multiple stages of thickeners for washing arranged in series so that the direction of movement of the solid in the slurry and the direction of movement of overflow water are opposite to each other; and a concentration step of removing a solid residue from the washing water recovered in the washing step by using a thickener for still standing that is different from the thickeners for washing, and then concentrating a supernatant of the thickener for still standing by using a concentration device to give a saccharified solution.

    摘要翻译: 糖化溶液制备方法包括:通过使纤维素生物质的浆料经受超临界状态或亚临界状态的热水处理,将纤维素生物质中所含的半纤维素或纤维素糖化为C5或C6糖的糖化步骤; 在糖化步骤之后用洗涤水依次洗涤浆料中的固体的洗涤步骤,通过使用多级的用于洗涤的增稠剂进行串联排列,使得固体在浆料中的移动方向和溢流水的移动方向 彼此相对; 以及浓缩步骤,通过使用与用于洗涤的增稠剂不同的静置的增稠剂,从洗涤步骤中回收的洗涤水中除去固体残余物,然后使用浓缩装置浓缩浓缩器的上清液静置 给出糖化溶液。