METHOD AND DEVICE FOR ACCURATELY CONTROLLING REDUCTION VALENCE STATE OF HIGH-PURITY VANADIUM PENTOXIDE

    公开(公告)号:US20230257854A1

    公开(公告)日:2023-08-17

    申请号:US18157014

    申请日:2023-01-19

    IPC分类号: C22B34/22 C22B5/12

    CPC分类号: C22B34/22 C22B5/12

    摘要: The present application relates to the technical field of non-ferrous metal reduction, and specifically to a method and device for accurately controlling a reduction valence state of high-purity vanadium pentoxide. An example method includes: introducing a reducing gas into the vanadium pentoxide to carry out a reduction reaction under a heating condition to obtain a mixture; weighing the mixture during the reduction reaction, and stopping the reaction when the weight of the mixture reaches a specified value; and introducing a cooling gas into the mixture for cooling to obtain calcine. An example device includes: a conveying member; a casing arranged on the conveying member; a partition member on the casing and dividing the inside of the casing into a reduction zone and a protection cooling zone; a material storage member on the conveying member for placing materials; and a weighing member on the conveying member.

    MATERIAL TREATMENT APPARATUS AND PROCESS USING HYDROGEN

    公开(公告)号:US20230063785A1

    公开(公告)日:2023-03-02

    申请号:US17792610

    申请日:2021-01-13

    发明人: Tomas Mach

    IPC分类号: B01J6/00 C22B5/12 C21B13/00

    摘要: A process for treating a material, such as by calcination or reduction processes, is disclosed. The process comprises reacting hydrogen and oxygen in a reaction chamber and producing heat and steam, discharging steam from the reaction chamber, using the heat to treat the material and produce a treated material, and returning at least some of the steam discharged from the reaction chamber to the process. An apparatus is also disclosed.

    RARE EARTH EXTRACTION APPARATUS AND METHOD OF USE THEREOF

    公开(公告)号:US20220259699A1

    公开(公告)日:2022-08-18

    申请号:US17736930

    申请日:2022-05-04

    IPC分类号: C22B59/00 C22B5/12

    摘要: The invention comprises an apparatus and method of use thereof for generating a rare earth from a rare earth oxide, comprising the steps of: (1) dissociating the rare earth oxide and hydrogen gas in a reaction chamber by inductively heating the reaction chamber to greater than 2000° K to form the associated rare earth and water vapor in a reaction process; (2) driving the reaction process forward by removing the water vapor from the reaction chamber by condensing and freezing the water vapor on a first cold trap surface as water ice, where the reaction comprises: RE2O3+3H2→2RE+3 H2O, where REO is a rare earth oxide and RE comprises a rare earth in the rare earth oxide; and/or (3) monitoring the reaction process by monitoring generation of at least one of the rare earth and the water in a control system designed for continuous/semi-continuous operation.

    REDUCTION DEVICE USING LIQUID METAL
    9.
    发明申请

    公开(公告)号:US20170349969A1

    公开(公告)日:2017-12-07

    申请号:US15537025

    申请日:2015-12-18

    摘要: The present invention relates to a reduction device using a liquid metal, which can improve the oxidation reaction of a reducing agent for reducing a material to be reduced using a liquid metal, while simultaneously effectively controlling the same. The reduction device according to the present invention comprises: a storage unit in which the liquid metal is supplied and stored; a reducing agent positioned in the storage unit; a reduction unit positioned on a side of the storage unit, which receives a material to be reduced and enables fluid communication with the storage unit; and a liquid metal storage unit. According to the present invention, a reducing agent, which has strong reducing ability, is sublimated using a liquid metal, thereby further improving the reduction capability, and the same is also controlled precisely, thereby removing restrictions on use resulting from the explosive reaction of the reducing agent, and guaranteeing efficient operation.