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    PREPARATION OF SEVOFLURANE WITH NEGLIGIBLE WATER CONTENT
    41.
    发明申请
    PREPARATION OF SEVOFLURANE WITH NEGLIGIBLE WATER CONTENT 审中-公开
    具有可忽略的水含量的七氟醚的制备

    公开(公告)号：WO2006113636A3

    公开(公告)日：2007-01-18

    申请号：PCT/US2006014427

    申请日：2006-04-18

    Applicant: MINRAD INC

    Inventor： TERRELL ROSS C ,  LEVINSON JOSHUA A ,  MCNEIRNEY JOHN C

    IPC: C07C41/00

    CPC classification number: A61K31/075 ,  C07C41/36 ,  C07C43/123

    Abstract: Provided is a sevoflurane anesthetic product which can remain substantially undegraded after long periods of storage, as well as a method for preparing the product. The product comprises sevoflurane in a glass container having a water content of less than 130 ppm. The method comprises drying sevoflurane having a water content of greater than 130 ppm to a water content les than 130 ppm. A preferred method of drying comprises contacting a sevoflurane composition having a water content of greater than 130 ppm with alumina-containing molecular sieves such that the water content is reduced to less than 130 ppm.

    Abstract translation: 本发明提供一种七氟醚麻醉剂产品，其长期储存后可保持基本上未降解，以及制备该产品的方法。 该产品在含水量小于130ppm的玻璃容器中包含七氟烷。 该方法包括将水含量大于130ppm的七氟醚干燥至130ppm以下的水含量。 优选的干燥方法包括使具有大于130ppm水含量的七氟烷组合物与含氧化铝的分子筛接触，使得水含量降低至小于130ppm。

    COMPOSITION AND METHOD USING SAME TO REMOVE URETHANE PRODUCTS FROM A SUBSTRATE
    43.
    发明申请
    COMPOSITION AND METHOD USING SAME TO REMOVE URETHANE PRODUCTS FROM A SUBSTRATE 审中-公开

    公开(公告)号：WO2006124394A3

    公开(公告)日：2006-11-23

    申请号：PCT/US2006/017860

    申请日：2006-05-03

    Applicant: TEPOLT, Danny, P. ,  TEPOLT, Nancy, M.

    Inventor： COLEMAN, Kenneth ,  WEINHOLD, Dennis

    IPC: C07C41/00 ,  C07C43/18

    Abstract: A composition for removing urethane products from a wide variety of substrates without the need for scraping, scrubbing, sanding, sandblasting and the like is provided. The composition is formed by combining water, a polar organic solvent, a mixture of organic esters, a hydrocarbon, and a polyether. The composition may optionally be formed by combining the components recited above along with an anionic surfactant. The composition may optionally be formed by combining the components recited above along with a thickener.

    A METHOD FOR PREPARING PARA-(2-HYDROXYALKYLOXY) STYRENE MONOMERS AND OLIGOMERS
    44.
    发明申请
    A METHOD FOR PREPARING PARA-(2-HYDROXYALKYLOXY) STYRENE MONOMERS AND OLIGOMERS 审中-公开
    制备PARA-（2-羟基喹啉）苯乙烯单体和低聚物的方法

    公开(公告)号：WO2005079537A3

    公开(公告)日：2006-10-19

    申请号：PCT/US2005005548

    申请日：2005-02-17

    Applicant: DU PONT ,  ARTHUR SAMUEL DAVID ,  KUNITSKY KEITH ,  TROST BARRY M ,  WAGMAN MARK E

    Inventor： ARTHUR SAMUEL DAVID ,  KUNITSKY KEITH ,  TROST BARRY M ,  WAGMAN MARK E

    IPC: C07C37/00 ,  C07C41/00 ,  C07C41/03 ,  C07C43/23 ,  C08F116/12 ,  C08F122/10 ,  C08F124/00

    CPC classification number: C07C41/03 ,  C08F12/22 ,  C07C43/23

    Abstract: A method for preparing p-(2-hydroxyalkyloxy)styrene monomers and oligomers is described. The method comprises a base-catalyzed reaction of a styrene ester, a suitable alcohol and an alkylene oxide in a single vessel reaction. In this method, the reactive p-hydroxystyrene is generated in situ via the base-catalyzed transesterification reaction between the styrene ester and the alcohol in the presence of the base catalyst. The p-hydroxystyrene formed reacts with the alkylene oxide to form the p-(2-hydroxyalkyloxy)styrene monomer or oligomer.

    Abstract translation: 描述了制备对 - （2-羟基烷氧基）苯乙烯单体和低聚物的方法。 该方法包括在单容器反应中苯乙烯酯，合适的醇和烯化氧的碱催化反应。 在该方法中，在碱催化剂存在下，通过苯乙烯酯与醇之间的碱催化酯交换反应原位生成反应性对羟基苯乙烯。 所形成的对羟基苯乙烯与烯化氧反应形成对 - （2-羟基烷氧基）苯乙烯单体或低聚物。

    PROCESS FOR PREPARING ALKOXY OR ARYLMETHOXY AROXYETHANES
    48.
    发明申请
    PROCESS FOR PREPARING ALKOXY OR ARYLMETHOXY AROXYETHANES 审中-公开
    制备烷基或芳基甲氧基硅氧烷的方法

    公开(公告)号：WO01060775A1

    公开(公告)日：2001-08-23

    申请号：PCT/US2001/003328

    申请日：2001-02-01

    IPC: C07B61/00 ,  C07C41/16 ,  C07C43/20 ,  C07C43/205 ,  C07C43/23 ,  C07C41/00 ,  C07C43/02

    CPC classification number: C07C41/16 ,  C07C43/2055 ,  C07C43/225

    Abstract: The present invention is a novel process, with or without solvent, for manufacture of compounds of formula (a), wherein P is selected from phenyl and naphthyl; wherein R1 and R2 and R3 are each independently selected from hydrogen, alykl, alkoxy, aryl, aralkyl, aralkoxy, halogen, alkoxyalkoxy, and aralkoxyalkoxy; wherein R5 is selected from substituted or unsubstituted phenyl, and substituted or unsubstituted naphthyl, the substituents being each independently selected from alkyl (C1-C8), alkoxy (C1-C8), aroxy, aralkoxy (C1-C8) and halogen. The process comprises reacting substituted phenols or naphthols of the formula (b) with ethylene carbonate in the presence of a first catalyst selected from metal halide, quaternary ammonium halide and quarternary phosphonium halide thereby forming an intermediate of the formula (c), then reacting the intermediate with a first compound selected from alkyl or aralkylhalide, alkyl or aralkyl sulfate, and alkyl or aralkyl sulfonate together with a metal hydroxide in the presence of a second catalyst, the second catalyst selected from quaternary ammonium salt or quaternary phosphonium salt.

    Abstract translation: 本发明是一种具有或不含溶剂的新方法，用于制备式（a）化合物，其中P选自苯基和萘基; 其中R1和R2和R3各自独立地选自氢，烯丙基，烷氧基，芳基，芳烷基，芳烷氧基，卤素，烷氧基烷氧基和芳烷氧基烷氧基; 其中R5选自取代或未取代的苯基和取代或未取代的萘基，取代基各自独立地选自烷基（C1-C8），烷氧基（C1-C8），芳氧基，芳烷氧基（C1-C8）和卤素。 该方法包括在选自金属卤化物，季铵卤化物和季铵卤化物的第一种催化剂的存在下使式（b）的取代的酚或萘酚与碳酸亚乙酯反应，从而形成式（c）的中间体， 中间体与选自烷基或芳烷基卤的第一种化合物，烷基或芳烷基硫酸盐，和烷基或芳烷基磺酸酯与金属氢氧化物在第二种催化剂存在下，第二种催化剂选自季铵盐或季鏻盐。

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