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公开(公告)号：WO2009083163A1
公开(公告)日：2009-07-09
申请号：PCT/EP2008/010802
申请日：2008-12-18
Applicant: LINDE AG , SAUDI BASIC INDUSTRIES CORPORATION , MÜLLER, Wolfgang , FRITZ, Peter, M. , BÖLT, Heinz , WELLENHOFER, Anton , MEISWINKEL, Andreas , TAUBE, Carsten , SCHNEIDER, Richard , WINKLER, Florian , FRITZ, Helmut , HOFMANN, Karl-Heinz , ZANDER, Hans-Jörg , ULBRICH, Peter , SEGATZ, Jan , MOUSA, Fuad , AL-HAZMI, Mohammed , AL-THAUYYAN, Abdullah , AL-MUSNED, Mohammed
Inventor： MÜLLER, Wolfgang , FRITZ, Peter, M. , BÖLT, Heinz , WELLENHOFER, Anton , MEISWINKEL, Andreas , TAUBE, Carsten , SCHNEIDER, Richard , WINKLER, Florian , FRITZ, Helmut , HOFMANN, Karl-Heinz , ZANDER, Hans-Jörg , ULBRICH, Peter , SEGATZ, Jan , MOUSA, Fuad , AL-HAZMI, Mohammed , AL-THAUYYAN, Abdullah , AL-MUSNED, Mohammed
CPC classification number: B01J19/18 , B01J19/1806 , C07C2/22 , C07C11/04 , C07C2521/06 , C07C2531/14 , Y02P20/52
Abstract: The present invention relates to a method for the oligomerisation of ethylene, comprising the steps of: (i) oligomerising ethylene in a reactor in the presence of a solvent and a catalyst composition; (ii) discharging a catalyst composition containing outlet stream from the reactor; (iii) deactivating and extracting the catalyst composition with a polar phase, wherein the outlet stream and the polar phase are mixed in a dynamic mixing device having rotor and stator elements comprising concentric tool rings as well as to a reactor system therefore.
Abstract translation: 本发明涉及乙烯低聚方法，包括以下步骤：（i）在溶剂和催化剂组合物存在下，在反应器中使乙烯低聚; （ii）从反应器排出含有出口物流的催化剂组合物; （iii）用极性相去活化和萃取催化剂组合物，其中出口流和极性相在具有包括同心工具环的转子和定子元件以及反应器系统的动态混合装置中混合。
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2.发明申请CATALYST COMPOSITION AND PROCESS FOR DI-, TRI- AND/OR TETRAMERIZATION OF ETHYLENE 审中-公开催化剂组合物和乙烯二异氰酸酯和/或叔丁基化方法
公开(公告)号：WO2009006979A3
公开(公告)日：2009-03-26
申请号：PCT/EP2008004815
申请日：2008-06-16
Applicant: LINDE AG , SAUDI BASIC IND CORP , MUELLER BERND H , FRITZ PETER M , BOELT HEINZ , WOEHL ANINA , MUELLER WOLFGANG , WINKLER FLORIAN , WELLENHOFER ANTON , ROSENTHAL UWE , HAPKE MARKO , PEULECKE NORMEN , AL-HAZMI MOHAMMED HASSAN , ALIYEV VUGAR O , MOSA FUAD MOHAMMED
Inventor： MUELLER BERND H , FRITZ PETER M , BOELT HEINZ , WOEHL ANINA , MUELLER WOLFGANG , WINKLER FLORIAN , WELLENHOFER ANTON , ROSENTHAL UWE , HAPKE MARKO , PEULECKE NORMEN , AL-HAZMI MOHAMMED HASSAN , ALIYEV VUGAR O , MOSA FUAD MOHAMMED
CPC classification number: B01J31/2495 , B01J31/143 , B01J31/1885 , B01J31/189 , B01J2231/20 , B01J2531/0258 , B01J2531/62 , C07C2/32 , C07C2/36 , C07C2531/14 , C07C2531/24 , C07F9/224 , C07F9/46 , C07F9/4883 , C07F9/65848 , C07F9/6587 , Y02P20/52 , C07C11/107
Abstract: The present invention relates to a catalyst composition and a process for di-, tri- and/or tetramerization of ethylene, wherein the catalyst composition comprises a chromium compound, a ligand of the general structure (A) R1R2P -N(R3)-P(R4)-N(R5)-H or (B) R1R2P- N(R3-P(R4)-N(R5)-PR6R7, or any cyclic derivatives of (A) and (B), wherein at least one of the P or N atoms of the PNPN-unit or PNPNP -unit is member of a ring system, the ring system being formed from one or more constituent compounds of structures (A) or (B) by substitution and a co-catalyst or activator.
Abstract translation: 本发明涉及一种催化剂组合物和乙烯二，三和/或四聚的方法，其中催化剂组合物包含铬化合物，通式结构的配体（A）R 1 R 2 P -N（R 3）-P （R4）-N（R5）-H或（B）R1R2P-N（R3-P（R4）-N（R5）-PR6R7或（A）和（B））的任何环状衍生物，其中至少一个 PNPN单元或PNPNP单元的P或N原子是环系的成员，环体系由一种或多种结构（A）或（B）的组成化合物通过取代和助催化剂或活化剂 。
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3.发明申请METHOD FOR OLIGOMERIZATION OF ETHYLENE AND REACTOR SYSTEM THEREFOR WITH REMOVAL OF HEAVY MOLECULAR WEIGHT OLIGOMERS 审中-公开乙烯和反应器体系低分子量去除重分子重量低聚物的方法
公开(公告)号：WO2007045305A1
公开(公告)日：2007-04-26
申请号：PCT/EP2006/008651
申请日：2006-09-06
Applicant: LINDE AG ZENTRALE PATENTABTEILUNG , SAUDI BASIC INDUSTRIES CORPORATION , SCHNEIDER, Richard , FRITZ, Peter, M. , MUSCHELKNAUTZ, Sebastian , BÖLT, Heinz , ALI, Talal , MOUSA, Fuad
Inventor： SCHNEIDER, Richard , FRITZ, Peter, M. , MUSCHELKNAUTZ, Sebastian , BÖLT, Heinz , ALI, Talal , MOUSA, Fuad
CPC classification number: C07C7/00 , B01J8/006 , B01J2208/00539 , C07C2/08 , C08F110/02 , C08F2500/02
Abstract: The present invention relates to a method for oligomerization of ethylene to form linear alpha- olefins in an oligomerization reactor in the presence of solvent and catalyst, wherein a reaction product containing heavy molecular weight oligomers (HMWO) is discharged from the oligomerization reactor and is passed to and filtrated in a filtration unit, characterized in that the filtration residue of HMWO is removed from the filtration unit discontinuously via a discharge valve; and to a reactor system therefore.
Abstract translation: 本发明涉及一种在溶剂和催化剂存在下，在低聚反应器中乙烯低聚形成直链α-烯烃的方法，其中含有重分子量低聚物（HMWO）的反应产物从低聚反应器中排出并通过 在过滤单元中过滤，其特征在于，通过排出阀不连续地从过滤单元中除去HMWO的过滤残余物; 并且因此反应器系统。
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公开(公告)号：WO2010127752A1
公开(公告)日：2010-11-11
申请号：PCT/EP2010/002191
申请日：2010-04-08
Applicant: LINDE AG , SAUDI BASIC INDUSTRIES CORPORATION , MOSA, Fuad , AZAM, Shahid , RAFI, Mohammed, Ghouse , ALI, Syed , AL-ONIZI, Abdullah , FRITZ, Peter, M. , BÖLT, Heinz , MEISWINKEL, Andreas , TAUBE, Carsten , WINKLER, Florian , MÜLLER, Wolfgang , WÖHL, Anina , GÖKE, Volker , SCHNEIDER, Richard , FRITZ, Helmut
Inventor： MOSA, Fuad , AZAM, Shahid , RAFI, Mohammed, Ghouse , ALI, Syed , AL-ONIZI, Abdullah , FRITZ, Peter, M. , BÖLT, Heinz , MEISWINKEL, Andreas , TAUBE, Carsten , WINKLER, Florian , MÜLLER, Wolfgang , WÖHL, Anina , GÖKE, Volker , SCHNEIDER, Richard , FRITZ, Helmut
Abstract: The present invention relates to a method for removal of an organic amine from hydrocarbon stream containing the amine, comprising the steps of : - reacting the amine of the hydrocarbon stream containing the amine with an acid and forming an amine salt, and - extracting the amine-salt formed into an aqueous phase, wherein the hydrocarbon stream containing the amine is an outlet stream from a reactor for preparing linear alpha -olefins (LAO) by oligomerization of ethylene or a fraction of such an outlet stream, wherein the reactor contains a catalyst comprising a zirconium component and an organoaluminum component.
Abstract translation: 本发明涉及一种从含有胺的烃流中除去有机胺的方法，包括以下步骤：使含有胺的烃流的胺与酸形成胺盐反应，并提取胺 盐形成水相，其中含有胺的烃流是来自用于通过乙烯低聚或这种出口物流的一部分制备直链α-烯烃（LAO）的反应器的出口物流，其中反应器含有催化剂 包括锆组分和有机铝组分。
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5.发明申请CATALYST FOR OLIGOMERIZATION OF ETHYLENE, METHOD FOR PREPARATION THEREOF AND PROCESS FOR OLIGOMERIZATION USING IT 审中-公开用于乙烯低聚的催化剂，其制备方法和使用其的低分子化方法
公开(公告)号：WO2009121456A8
公开(公告)日：2010-10-21
申请号：PCT/EP2009001518
申请日：2009-03-04
Applicant: LINDE AG , SAUDI BASIC IND CORP , ALIYEV VUGAR O , AL-HAZMI MOHAMMED , MOSA FUAD , ROSENTHAL UWE , MUELLER BERND H , HAPKE MARKO , PEULECKE NORMEN , WOEHL ANINA , FRITZ PETER M , BOELT HEINZ , MUELLER WOLFGANG , WINKLER FLORIAN , WELLENHOFER ANTON
Inventor： ALIYEV VUGAR O , AL-HAZMI MOHAMMED , MOSA FUAD , ROSENTHAL UWE , MUELLER BERND H , HAPKE MARKO , PEULECKE NORMEN , WOEHL ANINA , FRITZ PETER M , BOELT HEINZ , MUELLER WOLFGANG , WINKLER FLORIAN , WELLENHOFER ANTON
CPC classification number: B01J31/1658 , B01J31/189 , B01J2231/20 , B01J2531/62
Abstract: The present invention relates to a catalyst for oligomerization of ethylene, comprising a functionalized solid support; a ligand immobilized on the solid support by chemical bonding, wherein the immobilized ligand has, the structure (R1)(R2)P-N(R3)-P(R4)-Y-support or (R1)(R2)P-N(R3)-P(R4)-N(R5)-P(R6)-Y-support, wherein R1 R2, R3, R4, R5 and R6 are independently selected from aliphatic group, aryl group, amino group and trimethylsilyl group and Y is the functional group of the support or a derivative thereof; and a chromium compound reacted with the ligand.; and to a method for its preparation and a process for oligomerization of ethylene utilizing the catalyst.
Abstract translation: 本发明涉及乙烯低聚催化剂，其包括官能化固体载体; 结构（R1）（R2）PN（R3）-P（R4）-Y-支持或（R1）（R2）PN（R3） - 的固定化配位体固定在固体支持体上的配体， P（R4）-N（R5）-P（R6）-Y-支持物，其中R1R2，R3，R4，R5和R6独立地选自脂族基团，芳基，氨基和三甲基甲硅烷基，Y是官能团 一组支持或其衍生物; 与配位体反应的铬化合物。 以及其制备方法和利用该催化剂使乙烯低聚的方法。
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Patent Agency Ranking6.发明申请CATALYST COMPOSITION AND PROCESS FOR DI-, TRI- AND/OR TETRAMERIZATION OF ETHYLENE 审中-公开乙烯的二元，三元和/或四元化催化剂组合物和方法
公开(公告)号：WO2009006979A8
公开(公告)日：2009-12-23
申请号：PCT/EP2008004815
申请日：2008-06-16
Applicant: LINDE AG , SAUDI BASIC IND CORP , FRITZ PETER M , BOELT HEINZ , WOEHL ANINA , MUELLER WOLFGANG , WINKLER FLORIAN , WELLENHOFER ANTON , ROSENTHAL UWE , MUELLER BERND H , HAPKE MARKO , PEULECKE NORMEN , AL-HAZMI MOHAMMED HASSAN , ALIYEV VUGAR O , MOSA FUAD MOHAMMED
Inventor： FRITZ PETER M , BOELT HEINZ , WOEHL ANINA , MUELLER WOLFGANG , WINKLER FLORIAN , WELLENHOFER ANTON , ROSENTHAL UWE , MUELLER BERND H , HAPKE MARKO , PEULECKE NORMEN , AL-HAZMI MOHAMMED HASSAN , ALIYEV VUGAR O , MOSA FUAD MOHAMMED
CPC classification number: B01J31/2495 , B01J31/143 , B01J31/1885 , B01J31/189 , B01J2231/20 , B01J2531/0258 , B01J2531/62 , C07C2/32 , C07C2/36 , C07C2531/14 , C07C2531/24 , C07F9/224 , C07F9/46 , C07F9/4883 , C07F9/65848 , C07F9/6587 , Y02P20/52 , C07C11/107
Abstract: The present invention relates to a catalyst composition and a process for di-, tri- and/or tetramerization of ethylene, wherein the catalyst composition comprises a chromium compound, a ligand of the general structure (A) R1R2P -N(R3)-P(R4)-N(R5)-H or (B) R1R2P- N(R3-P(R4)-N(R5)-PR6R7, or any cyclic derivatives of (A) and (B), wherein at least one of the P or N atoms of the PNPN-unit or PNPNP -unit is member of a ring system, the ring system being formed from one or more constituent compounds of structures (A) or (B) by substitution and a co-catalyst or activator.
Abstract translation: 本发明涉及催化剂组合物和乙烯的二 - ，三 - 和/或四聚的方法，其中所述催化剂组合物包含铬化合物，通式结构（A）R 1 R 2 NP（R 3）-P （R）-N（R 5）-H或（B）R 1 R 2 P -N（R 3 -P（R 4）-N（R 5）-PR 6 R 7，或（A）和（B）的任何环状衍生物， PNPN-单元或PNPNP-单元的P或N原子是环体系的成员，所述环体系由结构（A）或（B）的一种或多种构成化合物通过取代和助催化剂或活化剂形成 。
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7.发明申请CATALYST COMPOSITION AND PROCESS FOR DI-, TRI- AND/OR TETRAMERIZATION OF ETHYLENE 审中-公开乙烯的二元，三元和/或四元化催化剂组合物和方法
公开(公告)号：WO2009006979A2
公开(公告)日：2009-01-15
申请号：PCT/EP2008/004815
申请日：2008-06-16
Applicant: LINDE AG , SAUDI BASIC INDUSTRIES CORPORATION , MÜLLER, Bernd, H. , FRITZ, Peter, M. , BÖLT, Heinz , WÖHL, Anina , MÜLLER, Wolfgang , WINKLER, Florian , WELLENHOFER, Anton , ROSENTHAL, Uwe , HAPKE, Marko , PEULECKE, Normen , AL-HAZMI, Mohammed, Hassan , ALIYEV, Vugar, O , MOSA, Fuad, Mohammed
Inventor： MÜLLER, Bernd, H. , FRITZ, Peter, M. , BÖLT, Heinz , WÖHL, Anina , MÜLLER, Wolfgang , WINKLER, Florian , WELLENHOFER, Anton , ROSENTHAL, Uwe , HAPKE, Marko , PEULECKE, Normen , AL-HAZMI, Mohammed, Hassan , ALIYEV, Vugar, O , MOSA, Fuad, Mohammed
CPC classification number: B01J31/2495 , B01J31/143 , B01J31/1885 , B01J31/189 , B01J2231/20 , B01J2531/0258 , B01J2531/62 , C07C2/32 , C07C2/36 , C07C2531/14 , C07C2531/24 , C07F9/224 , C07F9/46 , C07F9/4883 , C07F9/65848 , C07F9/6587 , Y02P20/52 , C07C11/107
Abstract: The present invention relates to a catalyst composition and a process for di-, tri- and/or tetramerization of ethylene, wherein the catalyst composition comprises a chromium compound, a ligand of the general structure (A) R 1 R 2 P -N(R 3 )-P(R 4 )-N(R 5 )-H or (B) R 1 R 2 P- N(R 3 -P(R 4 )-N(R 5 )-PR 6 R 7 , or any cyclic derivatives of (A) and (B), wherein at least one of the P or N atoms of the PNPN-unit or PNPNP -unit is member of a ring system, the ring system being formed from one or more constituent compounds of structures (A) or (B) by substitution and a co-catalyst or activator.
Abstract translation: 本发明涉及催化剂组合物和乙烯的二 - ，三 - 和/或四聚的方法，其中所述催化剂组合物包含铬化合物，通式结构（A）的配体， （R 3） - P（R 4） - N（R 3）2 - （R）-H或（B）R 1 R 2 -P N（R 3 -P（R 5） N（R 5） - PR 6 R 7，或（A）和（B）的任何环状衍生物， （B），其中PNPN-单元或PNPNP-单元的P或N原子中的至少一个是环体系的成员，所述环体系由结构（A）或（B）的一种或多种构成化合物形成， 通过取代和助催化剂或活化剂。
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8.发明申请METHOD FOR PREPARATION OF LINEAR ALPHA-OLEFINS AND REACTOR SYSTEM THEREFORE 审中-公开用于制备线性α-烯烃和反应器体系的方法
公开(公告)号：WO2008086837A1
公开(公告)日：2008-07-24
申请号：PCT/EP2007/009979
申请日：2007-11-19
Applicant: LINDE AG , SAUDI BASIC INDUSTRIES CORPORATION , FRITZ, Peter, M. , BÖLT, Heinz , WINKLER, Florian , MÜLLER, Wolfgang , SCHNEIDER, Richard , WELLENHOFER, Anton , MOUSA, Fuad
Inventor： FRITZ, Peter, M. , BÖLT, Heinz , WINKLER, Florian , MÜLLER, Wolfgang , SCHNEIDER, Richard , WELLENHOFER, Anton , MOUSA, Fuad
CPC classification number: C07C2/30 , C07C2531/04 , C07C2531/14
Abstract: The present invention relates to a method for the preparation of linear alpha-olefins by oligomerization of ethylene in a reactor in the presence of a catalyst and solvent, wherein an outlet stream from the reactor comprising the solvent, catalyst and linear alpha-olefins is heated by at least one heating means to a temperature to allow substantially all of the linear alpha-olefins to be dissolved and/or melted in the outlet stream; and a reactor system therefore.
Abstract translation: 本发明涉及通过在反应器中在催化剂和溶剂的存在下使乙烯低聚制备线性α-烯烃的方法，其中来自包含溶剂，催化剂和线性α-烯烃的反应器的出口物流被加热 通过至少一种加热装置达到允许基本上所有直链α-烯烃在出口流中溶解和/或熔化的温度; 和反应器系统。
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9.发明申请BUBBLE COLUMN REACTOR WITH LEVEL MEASURING DEVICE AND METHOD FOR LEVEL MEASUREMENT THEREIN 审中-公开具有水平测量装置的泡沫柱反应器及其水平测量方法
公开(公告)号：WO2007045356A1
公开(公告)日：2007-04-26
申请号：PCT/EP2006/009621
申请日：2006-10-05
Applicant: LINDE AG , SAUDI BASIC INDUSTRIES CORPORATION , SCHNEIDER, Richard , FRITZ, Peter, M. , MUSCHELKNAUTZ, Sebastian , BÖLT, Heinz , ALI, Talal , MOSA, Fuad
Inventor： SCHNEIDER, Richard , FRITZ, Peter, M. , MUSCHELKNAUTZ, Sebastian , BÖLT, Heinz , ALI, Talal , MOSA, Fuad
CPC classification number: G01F23/284 , B01J10/002 , B01J2219/00182 , B01J2219/00247 , C08F10/00 , Y10T137/0318 , C08F2/01
Abstract: The present invention relates to a bubble column reactor comprising a column reactor containing a lower 2-phase section and an upper gaseous phase section, characterized in that the reactor comprises a measurement device for measuring the level of 2-phase section in the column reactor, wherein the measurement device comprises an emitter and a detector for electromagnetic radiation which are positioned outside of the column reactor; and to a method for level measurement in such a reactor.
Abstract translation: 本发明涉及一种泡罩塔反应器，其包括含有下部2相段和上部气相部分的塔式反应器，其特征在于该反应器包括用于测量塔式反应器中2相段的水平的测量装置， 其中所述测量装置包括位于所述塔式反应器外部的发射器和用于电磁辐射的检测器; 以及在这种反应器中用于液位测量的方法。
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10.发明申请METHOD FOR OLIGOMERIZATION OF ETHYLENE AND REACTOR SYSTEM THEREFOR WITH REMOVAL OF HEAVY MOLECULAR WEIGHT OLIGOMERS 审中-公开乙烯和反应器体系低分子量去除重分子重量低聚物的方法
公开(公告)号：WO2007045306A1
公开(公告)日：2007-04-26
申请号：PCT/EP2006/008652
申请日：2006-09-06
Applicant: LINDE AG ZENTRALE PATENTABTEILUNG , SAUDI BASIC INDUSTRIES CORPORATION , SCHNEIDER, Richard , FRITZ, Peter, M. , MUSCHELKNANTZ, Sebastian , BÖLT, Heinz , ALI, Talal , MOUSA, Fuad
Inventor： SCHNEIDER, Richard , FRITZ, Peter, M. , MUSCHELKNANTZ, Sebastian , BÖLT, Heinz , ALI, Talal , MOUSA, Fuad
CPC classification number: C07C7/00 , B01J8/006 , B01J2208/00539 , C07C2/08 , C08F110/02 , C08F2500/02
Abstract: The present invention relates to a bubble column reactor comprising a column reactor having a sparger plate dividing the column reactor into a top reaction compartment and a bottom compartment, characterized in that an inlet and outlet line for introducing and disposing a flushing medium are connected to the bottom compartment; and an operation method thereof.
Abstract translation: 本发明涉及一种鼓泡塔反应器，其包括具有将塔反应器分成顶部反应室和底部隔室的分布器板的塔式反应器，其特征在于用于引入和布置冲洗介质的入口和出口管线连接到 底部隔间 及其操作方法。
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