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公开(公告)号：WO2016055542A1
公开(公告)日：2016-04-14
申请号：PCT/EP2015/073184
申请日：2015-10-07
CPC分类号： C07C51/265 , B01D1/16 , B01D53/68 , B01D53/8659 , B01D2251/30 , B01D2257/2022 , B01D2257/2042 , B01D2257/2062 , B01D2257/70 , Y02P20/154 , C07C63/26
摘要： The present invention provides a process for the production of an aromatic dicarboxylic acid comprising the catalytic oxidation of a hydrocarbon precursor in an organic solvent, wherein off-gas generated by the oxidation reaction is vented to the atmosphere after treatment to remove HBr and/or Br 2 , wherein said process comprises scrubbing in a scrubbing column a gas stream derived from off-gas generated by said oxidation reaction and comprising HBr and/or Br 2 , characterised in that: (i) the gas stream is irrigated with liquid phase water and a wash stream comprising alkali metal ions within said scrubbing column; (ii) the scrubbed gas stream is withdrawn from a vent located in an upper region of the scrubbing column; and (iii)a stream comprising water, said alkali metal ions and bromide ions is withdrawn from an effluent outlet located in a lower region of the scrubbing column. The present invention further provides a scrubbing column for carrying out the process.
摘要翻译： 本发明提供一种生产芳族二羧酸的方法，其包括在有机溶剂中催化氧化烃前体，其中通过氧化反应产生的废气在处理后排放到大气中以除去HBr和/或Br 2 其中所述方法包括在洗涤塔中洗涤源自由所述氧化反应产生的废气并包含HBr和/或Br 2的气流，其特征在于：（i）气流用液相水和洗涤液 在所述洗涤塔内包含碱金属离子; （ii）洗涤气流从位于洗涤塔上部区域的排气口排出; 和（iii）包含水的流，所述碱金属离子和溴离子从位于洗涤塔的下部区域的流出物出口排出。 本发明还提供一种用于进行该方法的洗涤塔。
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公开(公告)号：WO2015057697A1
公开(公告)日：2015-04-23
申请号：PCT/US2014/060473
申请日：2014-10-14
IPC分类号： D04B1/18
CPC分类号： D04B1/18 , D10B2403/0114 , Y02P70/633
摘要： An article comprising a knit fabric having a surface side and a base side, and including a set of ground yarns and a layer of effect yarns, wherein the ground yarns and effect yarns are knit through intermesh points in a predetermined arrangement wherein the effect yarns are alternately arranged with the ground yarns and wherein the ground yarns comprise at least one elastic fiber and optionally at least one hard fiber, and the effect yarns comprise at least one hard fiber and optionally an elastic fiber.
摘要翻译： 一种制品，包括具有表面侧和底侧的针织织物，并且包括一组研磨纱线和一层效果纱线，其中所述研磨纱线和效果纱线以预定布置编织穿过相互间的点，其中所述效果纱线是 交替地布置有研磨纱线，并且其中所述研磨纱线包括至少一种弹性纤维和任选的至少一种硬质纤维，并且所述效果纱线包括至少一种硬质纤维和任选的弹性纤维。
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公开(公告)号：WO2015057650A1
公开(公告)日：2015-04-23
申请号：PCT/US2014/060404
申请日：2014-10-14
发明人： RAO, Sundar , RYAN, John Paul
CPC分类号： B32B7/12 , B32B3/266 , B32B3/30 , B32B5/022 , B32B5/18 , B32B25/08 , B32B27/065 , B32B27/08 , B32B27/12 , B32B27/28 , B32B27/285 , B32B27/302 , B32B27/306 , B32B27/308 , B32B27/32 , B32B27/34 , B32B27/36 , B32B27/40 , B32B2262/0246 , B32B2262/0253 , B32B2262/0261 , B32B2262/0276 , B32B2262/062 , B32B2262/065 , B32B2262/067 , B32B2262/08 , B32B2262/14 , B32B2266/0278 , B32B2270/00 , B32B2274/00 , B32B2307/54 , B32B2307/5825 , B32B2307/7145 , B32B2307/724 , B32B2307/7246 , B32B2307/7265 , B32B2307/732 , B32B2307/734 , B32B2307/758 , B32B2471/00 , B32B2471/02 , B32B2479/00 , B32B2601/00
摘要： A composite film comprising one or more barrier film layers, wherein the one or more barrier film layers are liquid impermeable and have a total moisture vapor transfer rate (MVTR) of at least 14.6 g/24hr/m 2 according to ASTM E96B and one or more dimensionally stable layers, wherein the composite film has a robustness of greater than about 1.49 pound force.
摘要翻译： 一种复合膜，其包括一个或多个阻挡膜层，其中所述一个或多个阻挡膜层是液体不可渗透的，并且根据ASTM E96B具有至少14.6g / 24hr / m2的总湿气蒸气传输速率（MVTR），并且一个或多个 其中复合膜具有大于约1.49磅力的坚固性。
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公开(公告)号：WO2015009847A1
公开(公告)日：2015-01-22
申请号：PCT/US2014/046881
申请日：2014-07-16
IPC分类号： C07C255/07 , C07C253/34
CPC分类号： C07C253/10 , B01D3/143 , B01J31/185 , C07C253/34 , C07C255/07 , C07C255/04
摘要： A solvent is at least partially separated from a catalyst. The catalyst comprises nickel and a bidentate phosphorus-containing ligand. The method for separation involves distilling a catalyst solution. The ratio of 2-pentenenitrile to 3-pentenenitrile in distillation column bottoms is controlled to reduce the amount of 3-pentenenitrile which is isomerized to form 2-methyl-3-butenenitrile. Isomerization of 3-pentenenitrile to 2- methyl-3-butenenitrile, and subsequent isomerization of 2-methyl-3-butenenitrile to 2- methyl-2-butenenitrile, and/or hydrocyanation of 2-methyl-3-butenenitrile to methylglutaronitrile represents a loss in adiponitrile yield in a process for making adiponitrile.
摘要翻译： 溶剂与催化剂至少部分分离。 催化剂包括镍和二齿磷含量配体。 分离方法包括蒸馏催化剂溶液。 控制蒸馏塔底馏分中2-戊烯腈与3-戊烯腈的比例，以减少异构化形成2-甲基-3-丁烯腈的3-戊烯腈的量。 3-戊烯腈异构化为2-甲基-3-丁烯腈，随后将2-甲基-3-丁烯腈异构化为2-甲基-2-丁烯腈，和/或2-氰基-3-丁烯腈氢化为甲基戊二烯代表 在制造己二腈的方法中己二腈产率的损失。
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公开(公告)号：WO2014179066A1
公开(公告)日：2014-11-06
申请号：PCT/US2014/034224
申请日：2014-04-15
发明人： WELCH, Robert J.
IPC分类号： C07C51/41 , C07C55/14 , C07C55/02 , C07C209/68 , C07C211/09 , C07C211/12 , C08G69/28
CPC分类号： C08L77/06 , C07C51/412 , C08G69/28 , G01N27/4167 , G01N33/442 , Y02P20/582 , C07C55/14 , C07C55/02
摘要： A process for producing a partially balanced acid solution that involves metering dicarboxylic acid powder, based on weight, from a loss-in-weight feeder to a feeding conduit that transfers the dicarboxylic acid powder at a low variability feed rate into an in-line disperser, adding a first feed stream of diamine to the in-line disperser in an amount sufficient to form the partially balanced acid solution having a solids content of less than 60%, and storing the partially balanced acid solution at a temperature to maintain the dissolved dicarboxylic acid and to prevent formation of a slurry. The partially balanced acid solution may be used as a feed solution to prepare a nylon salt solution. Process controls for the process are also disclosed.
摘要翻译： 一种制备部分平衡的酸溶液的方法，其涉及将二羧酸粉末以重量计从重量损失进料器计量到以低变异性进料速率将二羧酸粉末转移到在线分散器中的进料管道 将二胺的第一进料流以足以形成固体含量小于60％的部分平衡的酸溶液的量向在线分散器中加入，并将该部分平衡的酸溶液储存在一定温度以保持溶解的二羧酸 酸，并防止淤浆的形成。 部分平衡的酸溶液可以用作进料溶液以制备尼龙盐溶液。 还公开了该方法的过程控制。
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公开(公告)号：WO2014099610A1
公开(公告)日：2014-06-26
申请号：PCT/US2013/074668
申请日：2013-12-12
IPC分类号： C01C3/02 , C07C209/48 , C07C253/10
CPC分类号： C01C3/0212 , C01C3/04 , C07C209/48 , C07C253/10 , Y02P20/125 , C07C255/04 , C07C211/12
摘要： Described is a process for the integrated production of hexamethylenediamine. The process includes integrating an HCN production process, a dinitrile compound production process, and a diamine production process. The HCN production process provides HCN for hydrocyanating butadiene to form a dinitrile compound and a hydrogen stream for hydrogenating the dinitrile compound to form a diamine. The HCN production process includes forming a crude hydrogen cyanide product and separating the crude hydrogen cyanide product to form an off-gas stream and a hydrogen cyanide product stream. The off-gas stream is further separated to recover hydrogen. The hydrogen cyanide product stream is further processed to recover hydrogen cyanide.
摘要翻译： 描述了一体化生产六亚甲基二胺的方法。 该方法包括将HCN生产过程，二腈化合物生产过程和二胺生产过程相结合。 HCN生产方法提供用于氢化氰化丁二烯的HCN以形成二腈化合物和用于氢化二腈化合物形成二胺的氢气流。 HCN生产方法包括形成粗制氰化氢产物并分离粗制氰化氢产物以形成废气流和氰化氢产物流。 进一步分离废气流以回收氢气。 进一步处理氰化氢产物流以回收氰化氢。
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公开(公告)号：WO2013148659A1
公开(公告)日：2013-10-03
申请号：PCT/US2013/033848
申请日：2013-03-26
CPC分类号： D03D15/08 , D02G3/328 , D03D1/00 , D03D15/0027 , D03D15/0094 , D10B2201/01 , D10B2321/02 , D10B2331/02 , D10B2331/04 , D10B2501/00 , Y10T442/3024
摘要： An article including a woven fabric comprising warp yarns and weft yarns, wherein at least one of either the warp yarns or the weft yarns includes: (a) a corespun elastic base yarn having a denier and including staple fiber and an elastic fiber core; and (b) a separate control yarn selected from the group consisting of a single filament yarn, a multiple filament yarn, a composite yarn, and combinations thereof; having a denier greater than zero to about 0.8 times the denier of the corespun elastic base yam; wherein the woven fabric includes (1 ) a ratio of corespun base yarn ends to control yarn ends of up to about 6:1; or (2) a ratio of corespun base yarn picks to control yarn picks of up to about 6:1; or (3) both a ratio of corespun base yarn ends to control yarn ends of up to about 6:1; and a ratio of corespun base yarn picks to control yarn picks of up to about 6:1.
摘要翻译： 一种包括经纱和纬纱的织物的制品，其中经纱或纬纱中的至少一种包括：（a）具有旦尼尔并包括短纤维和弹性纤维芯的芯绒弹性基纱; 和（b）选自单丝纱，多丝纱，复合纱及其组合的单独对照丝; 具有大于零至约0.8倍核心弹性基础纱线的丹尼尔的旦尼尔; 其特征在于，所述机织织物包括：（1）芯纱基纱线端部的比例，以控制纱线末端高达约6:1; 或（2）芯绒纱线选择的比例控制高达约6：1的纱线挑选; 或者（3）两芯纱线的纱线端部之间的比例控制纱线端部高达约6:1; 以及芯绒纱线的纱线比例控制在6：1左右。
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8.发明申请HIGH TENACITY OR HIGH LOAD BEARING NYLON FIBERS AND YARNS AND FABRICS THEREOF 审中-公开高强度或高负载尼龙纤维及其纱线及织物
公开(公告)号：WO2016061103A1
公开(公告)日：2016-04-21
申请号：PCT/US2015/055333
申请日：2015-10-13
IPC分类号： D04H1/4334
CPC分类号： D01D5/082 , D01D5/0023 , D01D5/12 , D01D10/02 , D01F6/60 , D04H1/4334 , D04H3/005 , D04H3/009
摘要： High strength or load bearing nylon fiber with break tenacity greater than 7.5 g/den and/or a tenacity at 10% elongation of greater than 4.0g/den as well as yarns, fabrics and articles of manufacture thereof and methods for their production are provided.
摘要翻译： 提供断裂强度大于7.5g / den的强度或承载尼龙纤维和/或在大于4.0g / den的10％伸长率下的韧度以及纱线，织物及其制造方法及其生产方法 。
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9.发明申请INTEGRATED PURIFIED TEREPHTHALIC ACID PRODUCTION AND POLYESTER POLYMERIZATION PLANT WITH CONDENSATE RECYCLING 审中-公开一体化纯化的过硫酸生产和聚酯聚合工厂与冷凝循环
公开(公告)号：WO2016059127A1
公开(公告)日：2016-04-21
申请号：PCT/EP2015/073810
申请日：2015-10-14
IPC分类号： C07C51/265 , C07C51/43 , C08G63/78 , C07C63/26
CPC分类号： C07C51/265 , C07C51/43 , C07C51/47 , C08G63/78 , C07C63/26
摘要： The present invention provides a method for the production of purified terephthalic acid crystals in an integrated terephthalic acid – polyester plant comprising the steps of: i) providing a stream of purified terephthalic acid crystals in an aqueous medium; ii) separating the purified terephthalic acid crystals from the aqueous medium in a filtration zone; and iii) washing the purified terephthalic acid crystals with an aqueous wash liquid, characterised in that at least a portion of the aqueous wash liquid is derived from an aqueous condensate liquor from the polyester plant.
摘要翻译： 本发明提供了一种在对苯二甲酸 - 聚酯装置整体中生产纯对苯二甲酸晶体的方法，包括以下步骤：i）在水性介质中提供纯化的对苯二甲酸晶体流; ii）在过滤区域中将纯化的对苯二甲酸晶体与水性介质分离; 和iii）用水性洗涤液洗涤纯化的对苯二甲酸晶体，其特征在于，所述水性洗涤液体的至少一部分来自所述聚酯装置的水性浓缩液。
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公开(公告)号：WO2016055463A1
公开(公告)日：2016-04-14
申请号：PCT/EP2015/073028
申请日：2015-10-06
摘要： The present invention provides method for removing residues from a first process stream comprising an organic solvent, water, a derivative of the organic solvent and the residues, comprising the steps of: i) feeding the first process stream to a solvent stripper comprising a still pot and a stripper column; ii) removing a vapour stream comprising the organic solvent, water and the derivative of the organic solvent from the stripper column; and iii) removing a residue stream from the still pot; characterised in that: the still pot and the stripper column form an integrated unit and the stripper column comprises a plurality of sieve trays. The present invention further provides an apparatus for carrying out the method, and processes for the production of a purified aromatic dicarboxylic acid incorporating the method.
摘要翻译： 本发明提供了从包含有机溶剂，水，有机溶剂的衍生物和残余物的第一工艺流中除去残余物的方法，包括以下步骤：i）将第一工艺流供给到包含釜的溶剂汽提器 和汽提塔; ii）从汽提塔中除去包含有机溶剂，水和有机溶剂衍生物的蒸气流; 和iii）从所述釜中除去残余物流; 其特征在于：静止罐和汽提塔形成一体的单元，汽提塔包括多个筛板。 本发明还提供了一种用于实施该方法的装置，以及用于制备包含该方法的纯化芳族二羧酸的方法。
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