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公开(公告)号：WO2008033230A3
公开(公告)日：2008-10-02
申请号：PCT/US2007019186
申请日：2007-08-30
申请人： EXXONMOBIL RES & ENG CO , CAO GUANG , SHAH MATU J
发明人： CAO GUANG , SHAH MATU J
CPC分类号： C01B37/005 , B01J29/035 , B01J29/047 , B01J29/70 , C01B39/06 , C01B39/08 , Y02P30/20
摘要： The present invention relates to new methods of making crystalline materials isostructural to ITQ-21, as well as to new crystalline materials obtainable by such methods, and their use in hydrocarbon conversion processes. In one of its aspects, the invention relates to a method of making a crystalline material iso-structural to ITQ-21, the method comprising: (a) providing a synthesis mixture comprising water, at least one source of germanium, at least one source of a tetravalent element X other than germanium, at least one structure directing agent R, optionally at least one source of trivalent element Y and optionally at least one source of fluoride, wherein the structure directing agent R is a compound of formula C 1 C 2 R 1 R 2 N + A - (I), in which C 1 and C 2 each independently represent a substituted or unsubstituted cyclohexyl or cyclopentyl group, R 1 and R 2 each independently represent a methyl group, an ethyl group or a propyl group, or R 1 and R 2 together with the nitrogen atom they are connected to form a ring containing 5 or 6 atoms, and A represents hydroxyl, fluorine, chlorine, bromine or iodine, (b) forming said crystalline material from the synthesis mixture; (c) recovering said crystalline material.
摘要翻译： 本发明涉及制备与ITQ-21同构的结晶材料的新方法，以及可通过这些方法获得的新结晶材料及其在烃转化方法中的应用。 在其一个方面，本发明涉及制备与ITQ-21异构结构的结晶材料的方法，所述方法包括：（a）提供合成混合物，其包含水，至少一种锗源，至少一种源 除了锗之外的四价元素X，至少一种结构导向剂R，任选地至少一种三价元素Y源和任选的至少一种氟化物源，其中结构导向剂R是式C的化合物， 1 2 2 R （I）其中C 1和C 2各自独立地表示取代或未取代的环己基或环戊基，R 1和R 2 > 2 各自独立地表示甲基，乙基或丙基，或R 1和R 2和它们连接的氮原子一起 形成含有5或6个原子的环，A表示羟基，氟，氯 溴，碘，（b）从合成混合物中形成所述结晶物质; （c）回收所述结晶材料。
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公开(公告)号：WO2016094774A2
公开(公告)日：2016-06-16
申请号：PCT/US2015065200
申请日：2015-12-11
发明人： LI QUANCHANG , AFEWORKI MOBAE , CALABRO DAVID CHARLES , GRIFFIN DAVID , NINES MEGHAN , WESTON SIMON CHRISTOPHER , PODSIADLO PAUL , BEECKMAN JEAN WILLEM LODEWIJK , KAMAKOTI PREETI , MAO KANMI , SHAH MATU J
CPC分类号： B01J20/262 , B01D15/00 , B01D53/02 , B01D53/0462 , B01D53/047 , B01D67/0088 , B01D69/10 , B01D71/70 , B01D2253/20 , B01D2253/25 , B01D2256/245 , B01D2257/302 , B01D2257/304 , B01D2257/40 , B01D2257/504 , B01D2257/80 , B01J20/0229 , B01J20/0237 , B01J20/06 , B01J20/08 , B01J20/10 , B01J20/103 , B01J20/16 , B01J20/18 , B01J20/22 , B01J20/264 , B01J20/28011 , B01J20/28057 , B01J20/28061 , B01J20/28064 , B01J20/28066 , B01J20/28069 , B01J20/28071 , B01J20/28073 , B01J20/28076 , B01J20/28078 , B01J20/28083 , B01J20/286 , B01J20/3042 , B01J20/3204 , B01J20/3212 , B01J20/3236 , B01J20/3238 , B01J20/3272 , B01J23/42 , B01J23/44 , B01J31/0274 , B01J31/125 , B01J31/127 , B01J35/1019 , B01J35/1023 , B01J35/1028 , B01J35/1061 , B01J37/0213 , B01J37/0236 , B01J37/036 , B01J2220/86 , B01J2231/641 , B01J2231/646 , C01B37/00 , C07C5/10 , C07F7/0807 , C07F7/0818 , C08F2/10 , C08G77/26 , C08G77/60 , C10G25/003 , C10G31/09 , C10G35/06 , C10G45/00 , C10G45/34 , C10G45/44 , C10G45/46 , C10G45/52 , C10G45/60 , C10G45/64 , C10G47/02 , C10G50/00 , C10K1/32 , C10M101/02 , C23C16/56 , Y02C10/08 , Y02P20/152
摘要： Methods of preparing organosilica materials, which is a polymer comprising independent siloxane units of Formula [Z3Z4SiCH2]3 (I), wherein each Z3 represents a hydroxyl group, a C1-C4 alkoxy group or an oxygen atom bonded to a silicon atom of another siloxane unit and each Z4 represents a hydroxyl group, a C1-C4 alkoxy group, a C1-C4 alkyl group, or an oxygen atom bonded to a silicon atom of another siloxane, in the absence of a structure directing agent and/or porogen are provided herein. Processes of using the organosilica materials, e.g., for gas separation, etc., are also provided herein.
摘要翻译： 制备有机硅材料的方法，其为包含式[Z 3 Z 4 SiCH 2] 3（I）的独立硅氧烷单元的聚合物，其中每个Z 3表示羟基，C1-C4烷氧基或与另一硅氧烷的硅原子键合的氧原子 在不存在结构导向剂和/或致孔剂的情况下，Z4表示羟基，C1-C4烷氧基，C1-C4烷基或与另一硅氧烷的硅原子键合的氧原子。 于此。 本文还提供了使用有机二氧化硅材料的方法，例如用于气体分离等。
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