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    RECOVERY OF RARE EARTHS FROM CONCENTRATES CONTAINING FLUORINE
    1.
    发明申请
    RECOVERY OF RARE EARTHS FROM CONCENTRATES CONTAINING FLUORINE 审中-公开
    从含有氟的浓度恢复稀土

    公开(公告)号：WO2017015435A1

    公开(公告)日：2017-01-26

    申请号：PCT/US2016/043270

    申请日：2016-07-21

    Applicant: HAZEN RESEARCH, INC.

    Inventor： SUN, Kang ,  BAUGHMAN, David, R. ,  HAZEN, Wayne, W.

    IPC: C01F17/00 ,  C01G23/02 ,  C22B1/14 ,  C22B34/12 ,  C22B34/14 ,  C22B34/24

    CPC classification number: C22B59/00 ,  C01F5/32 ,  C01F17/0043 ,  C01F17/0068 ,  C01G23/02 ,  C01G23/04 ,  C01G25/02 ,  C01G25/04 ,  C22B1/08 ,  C22B3/10 ,  C22B34/12 ,  C22B34/14 ,  C22B34/24 ,  Y02P10/234

    Abstract: The present invention relates to the recovery of rare earths, scandium, niobium, tantalum, zirconium, hafnium, titanium, and the like from ores or concentrates containing fluorine. More specifically, the ores or concentrates are pretreated by carbochlorination to convert the rare earths and other metals into their chlorides and then subjected to dilute hydrochloric acid leaching to recover the valuable rare earths and other metals from the leachate. Niobium, tantalum, zirconium, hafnium, and titanium can be recovered as their chlorides or oxychlorides from the gaseous products of carbochlorination, or converted into their oxides while simultaneously regenerating chlorine.

    Abstract translation: 本发明涉及从含有氟的矿石或精矿中回收稀土，钪，铌，钽，锆，铪，钛等。 更具体地说，矿石或浓缩物通过碳氯化进行预处理，以将稀土和其它金属转化为氯化物，然后进行稀盐酸浸出，以从浸出液回收有价值的稀土和其它金属。 铌，钽，锆，铪和钛可以作为它们的氯化物或氯氧化物从碳氯化合物的气体产物中回收，或者转化成它们的氧化物同时再生氯。

    PROCESS FOR MANUFACTURING LOWER CHLORIDES OF TITANIUM
    3.
    发明申请
    PROCESS FOR MANUFACTURING LOWER CHLORIDES OF TITANIUM 审中-公开
    制造钛酸锂的方法

    公开(公告)号：WO2012059939A1

    公开(公告)日：2012-05-10

    申请号：PCT/IN2011/000734

    申请日：2011-10-24

    Applicant: HORMUSJI, Gharda Keki

    Inventor： HORMUSJI, Gharda Keki

    IPC: C01G23/02 ,  C25C3/28 ,  C22B34/12

    CPC classification number: C01G23/02 ,  C01G23/026 ,  C22B34/1218 ,  C25C3/28 ,  Y02P10/23

    Abstract: A process for preparation of lower chlorides of titanium is provided, in which titanium tetrachloride (TiCl 4 ) is reduced using a reducing agent in at least one molten alkali metal salt at a temperature of about 300 to about 1400°C to obtain a reduced mass containing lower chlorides of titanium. A process for preparation of titanium metal from the lower chlorides of titanium is also provided.

    Abstract translation: 提供了制备低级氯化钛的方法，其中使用还原剂在至少一种熔融碱金属盐中在约300至约1400℃的温度下还原四氯化钛（TiCl 4）以获得含有 较低的氯化钛。 还提供了由钛的低级氯化物制备钛金属的方法。

    A PROCESS FOR THE PRODUCTION OF TITANIUM SALTS
    4.
    发明申请
    A PROCESS FOR THE PRODUCTION OF TITANIUM SALTS 审中-公开
    生产钛盐的方法

    公开(公告)号：WO2009001365A4

    公开(公告)日：2009-03-05

    申请号：PCT/IL2008000889

    申请日：2008-06-29

    Applicant: ASHER VITNER LTD ,  VITNER ASHER

    Inventor： VITNER ASHER

    IPC: C01G23/02

    CPC classification number: C01G23/02 ,  C01G23/022 ,  C01G23/026 ,  C01G23/028

    Abstract: The present invention provides a method for the Industrial production of a titanium salt TP, said method comprising the steps of: i. Precipitation of titanic acid from a solution comprising titanium salt TP1; ii. Production of a titanium containing product TP2 from a medium comprising of said titanic acid and an acid; and iii. Thermal conversion of titanium containing product TP3 to a titanium salt TP at temperature higher than 17Oº C

    Abstract translation: 本发明提供了钛盐TP的工业化生产方法，所述方法包括以下步骤： 从包含钛盐TP1的溶液中沉淀钛酸; II。 从包含所述钛酸和酸的介质中制备含钛产物TP2; 和iii。 含钛产物TP3在高于170℃的温度下热转化成钛盐TP

    CYCLICAL VACUUM CHLORINATION PROCESSES, INCLUDING LITHIUM EXTRACTION
    5.
    发明申请
    CYCLICAL VACUUM CHLORINATION PROCESSES, INCLUDING LITHIUM EXTRACTION 审中-公开
    循环真空氯化过程，包括锂萃取

    公开(公告)号：WO2005094289A2

    公开(公告)日：2005-10-13

    申请号：PCT/US2005/010273

    申请日：2005-03-29

    Applicant: THOMAS AND WENDELL DUNN, INC.

    Inventor： DUNN, Wendell, E., Jr. ,  VAN JAHNKE, Jeffrey

    IPC: C01B33/00 ,  C01D15/00 ,  C01F7/00 ,  C01G23/00 ,  C01G23/02 ,  C22B1/08 ,  C22B26/12

    CPC classification number: C01G23/022 ,  C01G23/02 ,  C22B1/08 ,  C22B26/12

    Abstract: Cyclical batch processes for halogenation, such as chlorination, of minerals in a fixed bed (12, 42, 62, 82) using a plurality of cycles which include the steps of at least partially evacuating the bed, charging the bed (12, 42, 62, 82) with reactant gas, maintaining the reactant gas in the bed (12, 42, 62, 82) for a predetermined time, and exhausting reaction products under vacuum. Also disclosed is the chlorination of spodumene in its beta crystalline form produced by calcining spodumene in its naturally occurring alpha crystalline form to preferentially extract lithium as lithium chloride.

    Abstract translation: 用于使用多个循环对固定床（12,42,62,82）中的矿物进行卤化（例如氯化）的循环分批处理，所述多个循环包括以下步骤：至少部分地排空床， 用反应气体填充床（12,42,62,82），将反应物气体保持在床（12,42,62,82）中预定时间，并在真空下排出反应产物。 还公开了通过煅烧其天然存在的α结晶形式的锂辉石以优选地以锂氯化物形式提取锂而生产的其β晶形式的锂辉石的氯化。

    PROCESS FOR MANUFACTURING LOWER CHLORIDES OF TITANIUM
    6.
    发明申请
    PROCESS FOR MANUFACTURING LOWER CHLORIDES OF TITANIUM 审中-公开
    制造钛酸锂的方法

    公开(公告)号：WO2012059939A8

    公开(公告)日：2014-01-09

    申请号：PCT/IN2011000734

    申请日：2011-10-24

    Applicant: GHARDA KEKI HORMUSJI

    Inventor： GHARDA KEKI HORMUSJI

    IPC: C01G23/02 ,  C22B34/12 ,  C25C3/28

    CPC classification number: C01G23/02 ,  C01G23/026 ,  C22B34/1218 ,  C25C3/28 ,  Y02P10/23

    Abstract: A process for preparation of lower chlorides of titanium is provided, in which titanium tetrachloride (TiCl4) is reduced using a reducing agent in at least one molten alkali metal salt at a temperature of about 300 to about 1400°C to obtain a reduced mass containing lower chlorides of titanium. A process for preparation of titanium metal from the lower chlorides of titanium is also provided.

    Abstract translation: 提供了制备低级氯化钛的方法，其中使用还原剂在至少一种熔融碱金属盐中在约300至约1400℃的温度下还原四氯化钛（TiCl 4）以获得含有 较低的氯化钛。 还提供了由钛的低级氯化物制备钛金属的方法。

    POLYALUMINUM CHLORIDE AND ALUMINUM CHLOROHYDRATE, PROCESSES AND COMPOSITIONS: HIGH-BASICITY AND ULTRA HIGH-BASICITY PRODUCTS
    8.
    发明申请
    POLYALUMINUM CHLORIDE AND ALUMINUM CHLOROHYDRATE, PROCESSES AND COMPOSITIONS: HIGH-BASICITY AND ULTRA HIGH-BASICITY PRODUCTS 审中-公开
    氯化铝和氯铝酸盐，工艺和组成：高碱性和超高分子产品

    公开(公告)号：WO2007082122A3

    公开(公告)日：2008-01-03

    申请号：PCT/US2007060073

    申请日：2007-01-04

    Applicant: NEXTCHEM LLC ,  PRATT WILLIAM E ,  STEVENS JOSEPH J III

    Inventor： PRATT WILLIAM E ,  STEVENS JOSEPH J III

    IPC: C01B9/00 ,  A61K8/26 ,  A61K8/28 ,  A61K8/44 ,  A61Q15/00 ,  C01B9/02 ,  C01G25/00

    CPC classification number: C01F7/56 ,  A61K8/26 ,  A61Q15/00 ,  B01D61/44 ,  C01B9/02 ,  C01G23/02 ,  C01G25/04 ,  C01G49/10

    Abstract: The invention relates generally to processes for the production of high- basicity and ultr- high basicity polyaluminum chlorides including aluminum chlorohydrate. The processes can produce products of a wide range of basicities and are particularly useful in producing high basicity products. The process can produce a wide range of solution concentrations and are particularly useful in producing high solution concentrations. The processes described generate high purity products, which are free of by-product salt(s). The processes described herein can also be utilized to produce enhanced efficacy polyaluminum chlorides including aluminum chlorohydrate. When compared to conventional processes for manufacturing these compounds the processes disclosed herein are unique in so far as the disclosed processes do not require aluminum metal as a starting material. The products of the processes are suitable in applications including water purification, catalysts, and antiperspirants. In addition, the invention is directed to the products prepared by the processes described herein.

    Abstract translation: 本发明一般涉及生产高碱度和超高碱性聚氯化铝的方法，包括氯化铝水合物。 该工艺可生产各种碱性产品，特别适用于生产高碱度产品。 该方法可产生大范围的溶液浓度，特别适用于生产高溶液浓度。 所述方法产生不含副产物盐的高纯度产物。 本文所述的方法也可用于产生包括氯化铝水合物的增强效力的聚氯化铝。 与用于制造这些化合物的常规方法相比，本文公开的方法是独特的，只要所公开的方法不需要铝金属作为起始材料即可。 该方法的产品适用于包括水净化，催化剂和止汗剂在内的应用。 此外，本发明涉及通过本文所述方法制备的产品。

    METHODS AND SYSTEMS FOR PRODUCING ULTRA HIGH PURITY TITANIUM TETRAIODIDE (TiI4) AND ULTRA HIGH PURITY TITANIUM METAL
    10.
    发明申请
    METHODS AND SYSTEMS FOR PRODUCING ULTRA HIGH PURITY TITANIUM TETRAIODIDE (TiI4) AND ULTRA HIGH PURITY TITANIUM METAL 审中-公开
    用于生产超高钛酸四铁（TiI4）和超高纯度钛金属的方法和系统

    公开(公告)号：WO1996020892A1

    公开(公告)日：1996-07-11

    申请号：PCT/US1995004870

    申请日：1995-04-24

    Applicant: MATERIALS RESEARCH CORPORATION

    Inventor： MATERIALS RESEARCH CORPORATION ,  LAM, Raymond, K., F.

    IPC: C01G23/02

    CPC classification number: C22B34/1263 ,  C01G23/02 ,  C22B34/1222 ,  C22B34/1277 ,  Y02P10/23

    Abstract: Systems and methods are provided for producing ultra high purity titanium tetraiodide, on the order of at least 99.998 % pure, and for producing ultra high purity titanium metal having a purity of greater than 99.998 % pure. The system includes a titanium tetraiodide generating subsystem; a titanium tetraiodide purification subsystem wherein titanium tetraiodide is refined to ultra high purity by a double distillation process at reduced pressure; and a titanium tetraiodide decomposition subsystem wherein titanium tetraiodide is decomposed and ultra high purity titanium metal is deposited on a deposition substrate. The ultra high purity titanium tetraiodide can be used as a precursor for the titanium metal production, or it may be utilized in other semiconductor applications. Also contemplated are methods of making ultra high purity metal halides wherein the halide is selected from the group consisting of bromides, chlorides, iodides and fluorides.

    Abstract translation: 提供了用于生产纯度高达99.998％的超高纯度四碘化钛的系统和方法，以及用于生产纯度高于99.998％纯度的超高纯钛金属。 该系统包括四碘化钛生成子系统; 四碘化钛净化子系统，其中通过双蒸馏方法在减压下将四碘化钛精制成超高纯度; 和四碘化钛分解的四碘化钛分解子系统，并且在沉积基板上沉积超高纯度钛金属。 超高纯钛四碘化钛可用作钛金属生产的前体，或者可用于其它半导体应用。 还考虑制备超高纯度金属卤化物的方法，其中卤化物选自溴化物，氯化物，碘化物和氟化物。

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