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    METHOD FOR PREPARING Y-TYPE MOLECULAR SIEVE HAVING HIGH SILICA-ALUMINA RATIO
    13.
    发明公开
    METHOD FOR PREPARING Y-TYPE MOLECULAR SIEVE HAVING HIGH SILICA-ALUMINA RATIO 审中-公开
    制备具有高硅铝比的Y型分子筛的方法

    公开(公告)号：EP3187463A1

    公开(公告)日：2017-07-05

    申请号：EP14900724.7

    申请日：2014-12-05

    申请人： Dalian Institute Of Chemical Physics Chinese Academy of Sciences

    发明人： YUAN, Danhua ,  HE, Dawei ,  SONG, Zhijia ,  XU, Yunpeng ,  LIU, Zhongmin

    IPC分类号： C01B39/24

    CPC分类号： C01B39/24 ,  C01B39/205 ,  C01P2002/72 ,  C01P2002/86 ,  C01P2004/03

    摘要： Provided is a method for preparing a Y type molecular sieve having a high silica-to-alumina ratio, comprising: mixing deionized water, a silicon source, an aluminum source, an alkali source, and a tetraalkylammoniumcation source as a template agent to obtain an initial gel mixture; after aging the initial gel mixture at an appropriate temperature, feeding the gel mixture into a high pressure synthesis kettle for crystallization; separating a solid product, and drying to obtain the Y type molecular sieve having a high silica-to-alumina ratio. The method provides a phase-pure Y type molecular sieve having a high crystallinity, the SiO 2 /Al 2 O 3 thereof being not less than 6.

    摘要翻译： 本发明提供一种制备氧化硅铝比高的Y型分子筛的方法，包括将去离子水，硅源，铝源，碱源和四烷基铵阳离子源作为模板剂混合，得到 初始凝胶混合物; 将初始凝胶混合物在适当温度下老化后，将凝胶混合物加入高压合成釜中进行结晶; 分离固体产物，并干燥以获得具有高氧化硅/氧化铝比的Y型分子筛。 该方法提供了结晶度高的纯相Y型分子筛，其SiO2 / Al2O3不小于6。

    METHOD FOR PREPARING POLYOXYMETHYLENE DIMETHYL ETHER CARBONYL COMPOUND AND METHYL METHOXYACETATE
    14.
    发明公开
    METHOD FOR PREPARING POLYOXYMETHYLENE DIMETHYL ETHER CARBONYL COMPOUND AND METHYL METHOXYACETATE 审中-公开
    制造方法聚甲醛二甲醚羰基化合物和甲氧基乙酸甲酯的

    公开(公告)号：EP3088381A1

    公开(公告)日：2016-11-02

    申请号：EP13900195.2

    申请日：2013-12-23

    申请人： Dalian Institute Of Chemical Physics Chinese Academy of Sciences

    发明人： NI, Youming ,  ZHU, Wenliang ,  LIU, Hongchao ,  LIU, Yong ,  LIU, Zhongmin ,  MENG, Shuanghe ,  LI, Lina ,  LIU, Shiping ,  ZHOU, Hui

    IPC分类号： C07C67/37 ,  C07C69/708

    CPC分类号： C07C67/37 ,  C07C67/38 ,  C07C69/708

    摘要： This invention provides a method for preparing a polyoxymethylene dimethyl ether carbonyl compound and/or methyl methoxyacetate as intermediates for producing ethylene glycol, which comprises passing a raw material: polyoxymethylene dimethyl ether or methylal together with carbon monoxide and hydrogen gas through a reactor carrying an acidic molecular sieve catalyst, and performing a reaction to prepare a corresponding product under an appropriate condition where no other solvent is added, wherein the process of the reaction is a gas-liquid-solid three-phase reaction. In the method of this invention, the raw material of polyoxymethylene dimethyl ether or methylal has a high conversion rate, each product has a high selectivity, the catalyst has a long service life, additional solvents are not required to be used, and reaction conditions are relatively mild. The method of this invention enables continuous production and has the potential for industrial application. Also, ethylene glycol may be produced by subjecting the resultant product to hydrolysis after hydrogenation or hydrogenation after hydrolysis.

    METHOD FOR PREPARING NAY MOLECULAR SIEVE OF HIGH SILICA-ALUMINA RATIO AND PRODUCT THEREOF
    15.
    发明公开
    METHOD FOR PREPARING NAY MOLECULAR SIEVE OF HIGH SILICA-ALUMINA RATIO AND PRODUCT THEREOF 审中-公开
    用于生产的NaY分子筛具有高硅铝-SHARE及其产品

    公开(公告)号：EP3081532A1

    公开(公告)日：2016-10-19

    申请号：EP13899055.1

    申请日：2013-12-09

    申请人： Dalian Institute Of Chemical Physics, Chinese Academy of Sciences

    发明人： YUAN, Danhua ,  DONG, Xinglong ,  XU, Yunpeng ,  LIU, Zhongmin ,  WANG, Kunyuan ,  HUANG, Wei

    IPC分类号： C01B39/24

    CPC分类号： C01B39/24

    摘要： The present invention relates to a method for preparing a NaY molecular sieve having a high silica-to-alumina ratio, wherein deionized water, a silicon source, an aluminum source, an alkali source, and ILs as a template agent are mixed to obtain an initial gel mixture; the initial gel mixture is maintained at a proper temperature and aged, then fed into a high pressure synthesis kettle for crystallization; the solid product is separated and dried, to obtain the NaY molecular sieve having a high silica-to-alumina ratio, wherein the ILs is a short-chain alkylimidazolium ionic liquid. The template agent used in the method of the invention is less volatile, and the resultant high-silicon Y molecular sieve has a high crystallinity and a silica-to-alumina ratio of 6 or more.

    METAL SILICOALUMINOPHOSPHATE MOLECULAR SIEVE HAVING RHO SKELETON STRUCTURE AND PREPARATION PROCESS THEREFOR
    19.
    发明公开
    METAL SILICOALUMINOPHOSPHATE MOLECULAR SIEVE HAVING RHO SKELETON STRUCTURE AND PREPARATION PROCESS THEREFOR 有权
    金属化学硅酸盐微生物 - 麦芽糖酵母

    公开(公告)号：EP2860158A1

    公开(公告)日：2015-04-15

    申请号：EP12878414.7

    申请日：2012-06-08

    申请人： Dalian Institute Of Chemical Physics, Chinese Academy of Sciences

    发明人： TIAN, Peng ,  SU, Xiong ,  LIU, Zhongmin ,  FAN, Dong ,  ZHANG, Ying ,  YANG, Yue

    IPC分类号： C01B39/54

    CPC分类号： C01B39/54 ,  B01J20/18 ,  B01J20/3078 ,  B01J29/85 ,  B01J37/082

    摘要： The present invention relates to a metal silicoaluminophosphate molecular sieve MeAPSO with a RHO framework structure and a preparation method thereof. The metal silicoaluminophosphate molecular sieve is characterized in that: the metal atoms are at least one of vanadium, copper, molybdenum, zirconium, cobalt, manganese, magnesium, iron, nickel and zinc. The chemical composition of said metal silicoaluminophosphate molecular sieve in anhydrous state is expressed as: mR•nMe•(SixAlyPz)O 2 , where R represents template existed in molecular sieve micropores, m is the molar number of said template per one molar of (SixAlyPz)O 2 , m=0.1∼0.5; Me represents metal atom entering into said metal silicoaluminophosphate molecular sieve framework, n is the molar number of Me per one molar of (SixAlyPz)O 2 , n=0.001∼0.30. Said metal silicoaluminophosphate molecular sieve has ion exchange performance and adsorption performance. The catalyst prepared from said metal silicoaluminophosphate molecular sieve can be applicable to multiple hydrocarbon reactions, such as catalytic cracking, reforming, polymerization, alkylation, transalkylation, isomerization, dehydrogenation, hydrogenation and the like.

    摘要翻译： 本发明涉及具有RHO骨架结构的金属硅铝磷酸盐分子筛MeAPSO及其制备方法。 金属硅铝磷酸盐分子筛的特征在于：金属原子是钒，铜，钼，锆，钴，锰，镁，铁，镍和锌中的至少一种。 所述金属硅铝磷酸盐分子筛的无水状态的化学成分表示为：mR¢nMe¢（SixAlyPz）O 2，其中R表示模板存在于分子筛微孔中，m是每一摩尔的所述模板的摩尔数 （SixAlyPz）O 2，m = 0.1〜0.5; Me表示进入所述金属硅铝磷酸盐分子筛框架的金属原子，n是每摩尔（SixAlyPz）O 2的Me的摩尔数，n = 0.001 / 0.30。 所述金属硅铝磷酸盐分子筛具有离子交换性能和吸附性能。 由所述金属硅铝磷酸盐分子筛制备的催化剂可适用于多个烃反应，如催化裂化，重整，聚合，烷基化，烷基转移，异构化，脱氢，氢化等。