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公开(公告)号：EP1282587A1
公开(公告)日：2003-02-12
申请号：EP01929076.6
申请日：2001-04-19
申请人： Solutia Inc.
CPC分类号： C07C37/60 , B01J29/06 , B01J29/40 , B01J29/46 , B01J29/90 , B01J2229/36 , B01J2229/40 , B01J2229/42 , Y02P20/52 , Y02P20/584 , C07C39/04
摘要： A method for catalytic production of hydroxylated aromatics by exposing zeolite catalyst to a reducing atmosphere to activate said catalyst, and reacting an aromatic with nitrous oxide in the preanence of said activated catalyst.
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32.发明公开
公开(公告)号：EP1204625A1
公开(公告)日：2002-05-15
申请号：EP00950693.2
申请日：2000-07-26
IPC分类号： C07C39/12 , C07C37/00 , C07C39/215
CPC分类号： C07C43/23 , C07C37/001 , C07C39/12 , C07C39/215
摘要： The present invention relates to the preparation of substituted or unsubstituted 1,2-bis(4-hydroxyphenyl)-hydroxyaliphatics such as 1,2-bis(4-hydroxyphenyl)-2-hydroxypropanes by reacting substituted or unsubstituted 1,2-bis(4-hydroxyphenyl)-halogen substituted aliphatics such as 1,2-bis(4-hydroxyphenyl)-2-chloropropanes in the presence of a base and water.
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公开(公告)号：EP0925270B1
公开(公告)日：2001-01-10
申请号：EP96931586.0
申请日：1996-09-13
发明人： SABAHI, Mahmood
CPC分类号： C07C37/00 , C07C49/255 , C07C39/38
摘要： A mixture of water and a glycol, such as ethylene glycol, is employed as the solvent for the reaction between 1,6-dibromo-2-naphthol and an alkali metal sulfite in the preparation of 6-bromo-2-naphthol and its derivatives to effect a substantial reduction in reaction time. The glycol/water mol ratio is ordinarily in the range of 0.1-0.5/l, preferably 0.3-0.5/l.
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34.发明公开METHOD OF MAKING 1,1-BIS-(4-HYDROXYPHENYL)-3,3,5-TRIMETHYLCYCLOHEXANE 失效用于生产1,1-双（4-羟基苯基）-3,3,5-三甲基环己烷
公开(公告)号：EP0729447A4
公开(公告)日：1998-06-10
申请号：EP95932375
申请日：1995-09-05
发明人： RUBINO MARK R , SALEK JEFFREY S
IPC分类号： C07D317/72 , B01J27/10 , B01J31/02 , C07C37/11 , C07C37/14 , C07C39/17 , C07C319/14 , C07C323/61 , C07D319/08 , C07D327/04 , C07D327/06 , C07C37/00
CPC分类号： C07C37/115 , C07C37/14 , C07C37/20 , C07C319/14 , Y02P20/582 , C07C323/61 , C07C39/17
摘要： This invention provides a unique method of producing 1,1-bis-(4-hydroxyphenyl)-3,3,5-trimethylcyclohexane ('BPTMC'). The disclosed method manufactures BPTMC from ketals and hemithioketals of 3,3,5-trimethylcyclohexanone ('TMC'). The reaction takes place in the presence of an acid catalyst, and optionally added co-catalysts. Additionally, applicants have disclosed a particularly useful method of manufacturing BPTMC from TMC and alcohol and/or thiol starting materials. These starting materials react to form the TMC ketal or thioketal materials. This method is particularly useful in that it allows recovery and recycling of the alcohol and/or thiol.
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公开(公告)号：EP0458965A4
公开(公告)日：1993-07-28
申请号：EP91903105
申请日：1990-12-12
发明人： SCHAAP, ARTHUR, PAUL
IPC分类号： C07B37/04 , A01N1/02 , A61B5/154 , A61F6/04 , A61J1/05 , A61K31/12 , A61K31/13 , A61K31/16 , A61K31/215 , A61K31/35 , A61K35/14 , A61K45/00 , A61K45/06 , A61L2/00 , A61L2/18 , A61L2/26 , A61L15/00 , A61M1/02 , A61P31/12 , A61P37/04 , C07B61/00 , C07C37/00 , C07C37/62 , C07C39/38 , C07C41/01 , C07C41/18 , C07C43/178 , C07C43/23 , C07C51/15 , C07C305/24 , C07D207/46 , C07D307/87 , C07D311/58 , C07D311/82 , C07D321/00 , C07D405/12 , C07D407/10 , C07D407/12 , C07D417/12 , C07D493/10 , C07D495/04 , C07F7/18 , C07F9/6541 , C07F9/655 , C07F9/6558 , C07F9/6561 , C07H15/203 , C07C41/30 , C07C67/28 , C07C67/293 , C07C303/24 , C07F9/117
CPC分类号： A61L2/18 , A61K31/12 , A61L2/0088 , C07C41/01 , C07C51/15 , C07C2603/18 , C07C2603/74 , C07D207/46 , C07D311/82 , C07D321/00 , C07D405/12 , C07D407/10 , C07D407/12 , C07D417/12 , C07D493/10 , C07D495/04 , C07F7/1852 , C07F7/1856 , C07F9/6541 , C07F9/65512 , C07F9/65522 , C07F9/65586 , C07F9/6561 , C07H15/203 , Y02P20/55 , C07C65/11 , C07C43/1788
摘要： An improved process for the preparation of vinyl ethers by the coupling reaction of an ester of formula (I), with a carbonyl containing compound of formula (II), wherein A and R are passive organic groups and OY is a hydroxyl group or OP where P is a protecting group is described. The ester and the carbonyl containing compound are reacted in an organic solvent with a titanium salt, a metallic reducing agent and an amine base to provide the vinyl ether. The reaction is safe and produces high yields. The vinyl ethers are useful for producing dioxetanes which produce light upon triggering.
摘要翻译： 一种改进的制备乙烯基醚的方法，其通过下式的酯与含有羰基的式（IMAGE）化合物的偶联反应，其中A和R是无源有机基团，OY是羟基或OP， P是一个保护组。 酯和含羰基化合物在有机溶剂中与钛盐，金属还原剂和胺碱反应以提供乙烯基醚。 反应安全，产量高。 乙烯基醚可用于产生在触发时产生光的二氧杂环丁烷。
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36.发明公开Procédé de débromation de dérivés dibromés du naphtol 失效Verfahren zur Debromierung von Dibromnaphtholderivaten。
公开(公告)号：EP0536012A1
公开(公告)日：1993-04-07
申请号：EP92402327.8
申请日：1992-08-24
发明人： Jacquot, Roland
CPC分类号： C07C49/255 , C07C37/00 , C07C39/38
摘要： L'invention concerne un procédé permettant de monodébromer sélectivement en position 1 le dibromo-1,6 hydroxy-2 naphtaléne.
Selon ce procédé, on fait réagir, dans un solvant organique acide et en présence d'un catalyseur à base de carbure de tungstène, (i) ledit dérivé dibromé du naphtaléne avec (ii) de l'hydrogène moléculaire ou un composé susceptible de générer, dans le milieu de réaction, de l'hydrogène naissant.
On receuille ainsi principalement du bromo-6 hydroxy-2 naphtalène.摘要翻译： 本发明涉及一种使得有可能在1位上选择性地单取1,6-二溴-2-羟基萘的方法。根据该方法，在酸性有机溶剂中和存在下进行反应 基于碳化钨的催化剂之间，（i）所述二溴萘和（ii）分子氢或能够在反应介质中产生新生氢的化合物。 因此，主要得到6-溴-2-羟基萘。
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37.发明公开
公开(公告)号：EP0373668A3
公开(公告)日：1991-01-16
申请号：EP89123230.8
申请日：1989-12-15
发明人： Pan, Yuh-Guo , Hochman, Lana L.
IPC分类号： C07C213/08 , C07C37/00 , C07D317/64 , C07C215/76 , C07C215/86 , C07C39/14 , C07C233/43
CPC分类号： C07D317/64 , C07C37/002 , C07C37/50 , C07C213/08 , C07C39/14
摘要： The conversion of ortho-hydroxylated Mannich bases to the corresponding methylated compounds, e.g., cresols, can be effectively carried out using a novel hydrogenation technique.
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公开(公告)号：EP0275528B1
公开(公告)日：1990-07-25
申请号：EP87118965.0
申请日：1987-12-21
发明人： Torii, Shigeru , Taniguchi, Masatoshi , Sasaoka, Michio , Tomotaki, Yoshihisa , Akada, Mitsuo , Tanaka, Hideo , Suzuki, Akira , Yamashita, Shiro
IPC分类号： C07C37/00 , C07C39/373 , C07B35/02
CPC分类号： C07C255/00 , C07C17/00 , C07C17/363 , C07C29/58 , C07C37/001 , C07C37/002 , C07C41/24 , C07C45/65 , C07C49/687 , C07C49/80 , C07C51/09 , C07C67/327 , C07C2601/16 , C07C2601/18 , C07D317/52 , C07C57/52 , C07C33/423 , C07C69/743 , C07C69/65 , C07C39/373 , C07C43/225
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40.发明公开Process for producing bis-hydroxyphenyl-n-alkanes, bis-hydroxyphenyl-n-alkanes and alkane diones 失效生产双羟基苯基-N-烷烃，双羟基苯基-N-烷烃和烷基二醇的方法
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