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41.发明公开Process for the preparation of diphenlyamine or nucleus-substituted derivative thereof 失效Verfahren zur Herstellung von Diphenylamin oder kernsubstituierten Derivaten
公开(公告)号：EP0803496A1
公开(公告)日：1997-10-29
申请号：EP97111438.4
申请日：1993-10-28
发明人： Nagata, Teruyuki , Kusuda, Chiyuki , Wada, Masaru
IPC分类号： C07C209/60 , C07C209/68
CPC分类号： C07C209/18 , C07C209/28
摘要： Described are processes for the preparation of diphenylamine or a nucleus-substituted derivative thereof, which comprise, upon feeding into a reaction system a phenol compound and reacting in the reaction system a cyclohexanone compound with an aniline compound in the presence of a hydrogen transfer catalyst and a catalytic amount of the cyclohexanone compound corresponding to the phenol compound while using the phenol compound as a hydrogen acceptor and forming the cyclohexanone compound in the reaction system, employing a hydroxide, carbonate or bicarbonate of an alkali metal and/or an alkaline earth metal when the hydrogen transfer catalyst is one of noble metals of Group VIII of the periodic table, respectively.
摘要翻译： 描述了制备二苯胺或其核取代衍生物的方法，其包括在将反应体系中加入酚化合物并在反应体系中在氢转移催化剂存在下使环己酮化合物与苯胺化合物反应，和 催化量的对应于酚化合物的环己酮化合物，同时使用酚化合物作为氢受体并在反应体系中形成环己酮化合物，使用碱金属和/或碱土金属的氢氧化物，碳酸盐或碳酸氢盐，当 氢转移催化剂分别是周期表第VIII族的贵金属之一。
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公开(公告)号：EP0753505A3
公开(公告)日：1997-03-26
申请号：EP96114159.5
申请日：1993-08-11
IPC分类号： C07C209/68 , C07C209/52
CPC分类号： C07C209/00 , C07C209/28 , C07C209/52 , C07C209/68
摘要： Disclosed are (1) a method for preparing an aromatic secondary amino compound which comprises reacting an N-cyclohexylideneamino compound in the presence of a hydrogen moving catalyst and a hydrogen acceptor by the use of a sulfur-free polar solvent and/or a cocatalyst, and (2) a method for preparing an aromatic secondary amino compound which comprises reacting cyclohexanone or a nucleus-substituted cyclohexanone, an amine and a nitro compound corresponding to the amine in a sulfur-free polar solvent in the presence of a hydrogen moving catalyst, a cocatalyst being added or not added.
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公开(公告)号：EP0476404B1
公开(公告)日：1995-06-21
申请号：EP91114715.5
申请日：1991-09-01
发明人： Nagata, Teruyuki , Watanabe, Katsuji , Kono, Yoshitsugu , Tamaki, Akihiro, Mitsui Toatsu Kosugaya Apt. 2-302 , Kobayashi, Takashi
IPC分类号： C07C209/36 , C07C211/46
CPC分类号： C07C209/36
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公开(公告)号：EP0435659B1
公开(公告)日：1995-02-22
申请号：EP90314290.9
申请日：1990-12-24
IPC分类号： C07C201/12 , C07C205/38 , C07C319/20 , C07C315/04 , C07C323/20 , C07C317/22
CPC分类号： C07C201/12 , C07C315/04 , C07C319/20 , C07C317/22 , C07C323/20 , C07C205/38
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公开(公告)号：EP0384463B1
公开(公告)日：1994-08-10
申请号：EP90103454.6
申请日：1990-02-22
发明人： Nagata, Teruyuki , Wada, Masaru , Mizuta, Hideki
IPC分类号： C07C265/14 , C07C263/10
CPC分类号： C07C263/10 , C07C265/14
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公开(公告)号：EP0588060A3
公开(公告)日：1994-04-13
申请号：EP93112886.2
申请日：1993-08-11
IPC分类号： C07C209/28 , C07C209/52 , C07C209/68 , C07C213/02
CPC分类号： C07C209/00 , C07C209/28 , C07C209/52 , C07C209/68
摘要： [Constitution] A method for preparing diphenylamine from cyclohexanone and aniline by adding dropwise nitrobenzene and cyclohexanone to a reaction system in which a hydrogen transfer catalyst and a sulfur-free polar solvent are present and aniline is being formed from nitrobenzene as a hydrogen acceptor. [Effect] Diphenylamine can be obtained in a high yield under moderate reaction conditions.
摘要翻译： [组成]通过将硝基苯和环己酮滴加到其中存在氢转移催化剂和不含硫的极性溶剂的反应体系中由环己酮和苯胺制备二苯胺的方法，并且由硝基苯作为氢受体形成苯胺。 [效果]二苯胺可以在中等反应条件下以高收率获得。
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公开(公告)号：EP0553801A1
公开(公告)日：1993-08-04
申请号：EP93101236.3
申请日：1993-01-28
CPC分类号： C08K5/5398 , B29C33/60
摘要： An internal release agent comprises a sulfur-containing acid phosphoric esters selected from the group consisting of thiophosphoric acid esters and dithiophosphoric acid esters of the formula,
where X and Y are independently selected from the group consisting of an oxygen atom and a sulfur atom, at least one of X and Y is a sulfur atom, and R₁ and R₂ are independently alkyl groups.摘要翻译： 一种内部脱模剂包括选自硫代磷酸酯和下式的二硫代磷酸酯的含硫酸性磷酸酯，其中X和Y独立地选自氧原子和硫原子 原子，X和Y中的至少一个是硫原子，并且R 1和R 2独立地是烷基。
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公开(公告)号：EP0329389A3
公开(公告)日：1990-03-28
申请号：EP89301399.5
申请日：1989-02-15
发明人： Nagata, Teruyuki , Okazaki, Koju , Kajimoto, Nobuyuki , Miura, Tohru , Kanemura, Yoshinobu , Sasagawa, Katsuyoshi
CPC分类号： C08G18/775 , B29C33/60 , B29K2075/00 , B29L2011/0016 , C08G18/3863 , G02B1/041 , C08L75/00
摘要： Polyurethane base lens resins obtained by reacting one or more of sulfur-containing polyisocyanates compound with one or more of sulfur-containing polyols, and polyurethane base lenses comprising these resins are disclosed. A method for preparing polyurethane base lenses which comprises adding internal mold releasing agents to the mixture of the above polyisocyanates and polyols prior to casting polymerization is also disclosed.
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公开(公告)号：EP0212823B1
公开(公告)日：1990-02-07
申请号：EP86305281.7
申请日：1986-07-09
发明人： Yamaguchi, Keizaburo , Sugimoto, Kenichi , Tanabe, Yoshimitsu , Nagata, Teruyuki , Yamaguchi, Akihiro
IPC分类号： C07C315/06 , C07C201/00 , C07C205/00
CPC分类号： C07C201/16 , C07C315/04 , C07C315/06 , C07C205/45 , C07C317/14
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50.发明公开Preparation process of N-substituted monochlorosuccinimide 失效Verfahren zur Herstellung von N-substitutioniertem Monochlorosuccinimid。
公开(公告)号：EP0349259A1
公开(公告)日：1990-01-03
申请号：EP89306498.0
申请日：1989-06-27
IPC分类号： C07D207/40
CPC分类号： C07D207/416
摘要： N-substituted monochlorosuccinimides e.g., N-phenylmonochlorosuccinimide, can be prepared in a high yield by reacting a maleamic acid, e.g., N-phenylmaleamic acid, with phosgene in the presence of a catalyst,e.g., dimethylformamide .
摘要翻译： N-取代的一氯代琥珀酰亚胺例如N-苯基一氯代琥珀酰亚胺可以通过马来酰胺酸例如N-苯基马来酰胺酸与光气在催化剂例如二甲基甲酰胺的存在下以高收率制备。
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