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    VERFAHREN ZUR HERSTELLUNG VON SEMICARBAZONEN
    1.
    发明公开
    VERFAHREN ZUR HERSTELLUNG VON SEMICARBAZONEN 有权
    用于生产缩氨基脲

    公开(公告)号：EP1727792A1

    公开(公告)日：2006-12-06

    申请号：EP05716121.8

    申请日：2005-03-16

    申请人： BASF Aktiengesellschaft

    发明人： ZIERKE, Thomas ,  ENGEL, Stefan ,  OTTO, Peter

    IPC分类号： C07C281/04 ,  C07C281/14

    CPC分类号： C07C281/14

    摘要： The invention relates to a method for producing semicarbazone compounds of formula (I) wherein R1 and R2 independently represent hydrogen, halogen, CN, C1-C4 alkyl, C1-C4 alkoxy, C1-C4 haloalkyl or C1-C4 haloalkoxy, and R3 represents C1-C4 alkoxy, C1-C4 haloalkyl or C1-C4 haloalkoxy. According to said method, a hydrazone compound of general formula (II), wherein R represents C1-C4 alkoxy, amino, C1-C4 alkylamino or di-(C1-C4-alkyl)amino, and R1 and R2 have the above-mentioned designations, is reacted with an aniline compound of general formula (III) wherein R3 has the above-mentioned designation.

    PYRAZOLYLDIOXOTHIOCHROMANOYL-DERIVATE
    2.
    发明公开
    PYRAZOLYLDIOXOTHIOCHROMANOYL-DERIVATE 有权
    PYRAZOLYLDIOXOTHIOCHROMANOYL衍生物

    公开(公告)号：EP1080089A1

    公开(公告)日：2001-03-07

    申请号：EP99924925.3

    申请日：1999-05-10

    申请人： BASF AKTIENGESELLSCHAFT

    发明人： WITSCHEL, Matthias ,  LANGEMANN, Klaus ,  VON DEYN, Wolfgang ,  MISSLITZ, Ulf ,  BAUMANN, Ernst ,  ENGEL, Stefan ,  MAYER, Guido ,  NEIDLEIN, Ulf ,  WAGNER, Oliver ,  OTTEN, Martina ,  WESTPHALEN, Karl-Otto ,  WALTER, Helmut

    IPC分类号： C07D409/06 ,  C07D409/14 ,  A01N43/56

    CPC分类号： C07D409/06 ,  A01N43/56 ,  C07D409/14 ,  C07F9/65586

    摘要： The invention relates to pyrazolyldioxothiochromanoyl derivatives of formula (I) in which the variables have the following meanings: X represents oxygen, sulfur, S=O, S(=O)2, CR4R5, C=O or C=NR6; R1 hydrogen, nitro, halogen, cyano, alkyl, alkyl halide, alkoxy, alkoxy halide, alkyl thio, alkyl thio halide, alkyl sulfinyl, alkyl sulfinyl halide, alkyl sulfonyl, alkyl sulfonyl halide, optionally substituted amino sulfonyl or optionally substituted sulfonyl amino; R2 represents alkyl, alkyl halide, alkoxy or alkoxy halide; R3 represents hydrogen, alkyl or halogen; R4, R5 represent hydrogen, nitro, halogen, cyano, alkyl, alkyl halide, alkoxy, alkoxy halide, alkyl thio, alkyl thio halide, alkyl sulfinyl, alkyl sulfinyl halide, alkyl sulfonyl, alkyl sulfonyl halide or optionally substituted amino; or R?4 and R5¿ jointly construct a chain which can be substituted and/or discontinued by oxygen or sulfur; or an optionally substituted methylidene group; l represents 0 to 4; and R7 represents substituted pyrazole-4-yl-carbonyl or substituted pyrazole-4-yl-methylidene. The invention also relates to the salts of said derivatives which can be used for agricultural purposes, to a method for producing the pyrazolyldioxothiochromanoyl derivatives, to agents containing the same, and to the use of these derivatives or agents containing the same for controlling undesirable plants.

    SUBSTITUIERTE 4-BENZOYL-PYRAZOLE
    4.
    发明公开
    SUBSTITUIERTE 4-BENZOYL-PYRAZOLE 失效
    SUBSTITUIERTE 4-苯甲酰基 - 吡唑

    公开(公告)号：EP0984962A1

    公开(公告)日：2000-03-15

    申请号：EP98922797.0

    申请日：1998-05-04

    申请人： BASF AKTIENGESELLSCHAFT

    发明人： ENGEL, Stefan ,  BAUMANN, Ernst ,  VON DEYN, Wolfgang ,  HILL, Regina, Luise ,  KARDORFF, Uwe ,  MAYER, Guido ,  OTTEN, Martina ,  RHEINHEIMER, Joachim ,  WAGNER, Oliver ,  WITSCHEL, Matthias ,  MISSLITZ, Ulf ,  WALTER, Helmut ,  WESTPHALEN, Karl-Otto

    IPC分类号： C07D405/10 ,  A01N43/56 ,  C07D493/04 ,  C07D303/38 ,  C07D305/06

    CPC分类号： C07D405/10 ,  C07D493/04

    摘要： 4-benzoyl-pyrazoles having the formula (I) are disclosed, in which the substituents have the following meanings: R1, R2 stand for hydrogen, mercapto, nitro, halogen, cyano, rhodano, C¿1?-C6-alkyl, halogenated C1-C6-alkyl, C1-C6-alkoxy, C2-C6-alkenyl, C2-C6-alkinyl, -OR?10, -OCOR10¿, -OSO¿2R?10, -S(O)¿n?R?10, -SO¿2OR10, -SO2NR?3OR10, -NR10SO¿2R?10 or -NR10¿COR; Q stands for a pyrazol linked at position 4 and having formula (II), in which R11 stands for C¿1?-C6-alkyl, halogenated C1-C6-alkyl, phenyl or phenyl which is partially or entirely halogenated and/or bears one to three of the following radicals: nitro, cyano, C1-C4-alkyl, halogenated C1-C4-alkyl, C1-C4-alkoxy, halogenated C1-C4-alkoxy; R?12¿ stands for hydrogen, C¿1?-C6-alkyl, halogenated C1-C6-alkyl, C1-C6-alkylcarbonyl, halogenated C1-C6-alkylcarbonyl, C1-C6-alkoxycarbonyl, C1-C6-alkylsulfonyl, halogenated C1-C6-alkylsulfonyl, phenylcarbonyl, phenylcarbonylmethyl, phenoxycarbonyl or phenylsulfonyl, the last four substituents being unsubstituted or the phenyl ring being partially or entirely halogenated and/or bearing one to three of the following radicals: nitro, cyano, C1-C4-alkyl, halogenated C1-C4-alkyl, C1-C4-alkoxy, halogenated C1-C4-alkoxy; R?13¿ stands for hydrogen, C¿1?-C6-alkyl or halogenated C1-C6-alkyl; A stands for a group of formulas (IIIa), (IIIb) or (IV), in which the substituents have the meanings indicated in the first claim. Also disclosed are the salts of these compounds useful in agriculture.

    摘要翻译： 公开了具有式（I）的4-苯甲酰基吡唑，其中取代基具有以下含义：R 1，R 2代表氢，巯基，硝基，卤素，氰基，rhodano，C 1 -C 6烷基，卤代 C 1 -C 6烷基，C 1 -C 6烷氧基，C 2 -C 6烯基，C 2 -C 6炔基，-OR 10，-OCOR 10，-OSO 2 R 10，-S（O） 10，-SO 2 OR 10，-SO 2 NR 3 OR 10，-NR 10 SO 2 R 10或-NR 10 COR; Q代表在4位连接且具有式（II）的吡唑，其中R 11代表部分或完全被卤代的C 1 -C 6烷基，卤代C 1 -C 6烷基，苯基或苯基和/或 硝基，氰基，C 1 -C 4烷基，卤代C 1 -C 4烷基，C 1 -C 4烷氧基，卤代C 1 -C 4烷氧基; R 12代表氢，C 1 -C 6烷基，卤代C 1 -C 6烷基，C 1 -C 6烷基羰基，卤代C 1 -C 6烷基羰基，C 1 -C 6烷氧基羰基，C 1 -C 6烷基磺酰基，卤代 C1-C6-烷基磺酰基，苯基羰基，苯基羰基甲基，苯氧基羰基或苯基磺酰基，最后四个取代基是未取代的或苯环部分或完全被卤代和/或带有1-3个下列基团：硝基，氰基，C1- ，卤代C 1 -C 4烷基，C 1 -C 4烷氧基，卤代C 1 -C 4烷氧基; R 13代表氢，C 1 -C 6烷基或卤代C 1 -C 6烷基; A代表式（IIIa），（IIIb）或（IV）的基团，其中取代基具有第一项权利要求中所示的含义。 还公开了用于农业的这些化合物的盐。

    SUBSTITUIERTE 2-BENZOYL-CYCLOHEXAN-1,3-DIONE MIT HERBIZIDER WIRKUNG
    7.
    发明公开
    SUBSTITUIERTE 2-BENZOYL-CYCLOHEXAN-1,3-DIONE MIT HERBIZIDER WIRKUNG 失效
    替代二-2-苯甲酰基环己烷-1,3二酮麻醉剂治疗剂WIRKUNG

    公开(公告)号：EP0958276A1

    公开(公告)日：1999-11-24

    申请号：EP97953895.0

    申请日：1997-12-19

    申请人： BASF AKTIENGESELLSCHAFT

    发明人： HILL, Regina, Luise ,  KARDORFF, Uwe ,  RACK, Michael ,  BAUMANN, Ernst ,  VON DEYN, Wolfgang ,  ENGEL, Stefan ,  MAYER, Guido ,  OTTEN, Martina ,  RHEINHEIMER, Joachim ,  WITSCHEL, Matthias ,  MISSLITZ, Ulf ,  WALTER, Helmut ,  WESTPHALEN, Karl-Otto

    IPC分类号： C07D333 ,  A01N35 ,  A01N37 ,  A01N41 ,  C07C251 ,  C07C257 ,  C07C259 ,  C07C317

    CPC分类号： A01N41/10 ,  A01N35/10 ,  A01N37/52 ,  C07C251/48 ,  C07C259/10 ,  C07C317/32 ,  C07C317/44 ,  C07C2601/16

    摘要： The invention concerns 2-benzoyl-cyclohexan-1,3-diones of formula (I), in which R1, R2 stand for hydrogen, nitro, halogen, cyano, rhodano, alkyl, halogen alkyl, alkoxyalkyl, alkenyl, alkinyl, -OR?5, -OCOR6¿, -OSO¿2R?6, -SH, -S(O)¿n?R?7, -SO¿2OR5, -SO2NR?5R8, -NR8SO¿2R?6 or -NR8COR6; R3¿ stands for hydrogen, cyano, alkyl, halogen alkyl, -OR?7, -SR7 or -NR7R10; R4¿ stands for hydrogen, optionally substituted alkyl, cycloalkyl, alkenyl, cycloalkenyl, alkinyl, -COR9, -CO2R?9, -COSR9¿ or -CONR8R9; X stands for oxygen or NR8; n equals 0, 1 or 2; R5 stands for hydrogen, alkyl, halogen alkyl, alkoxyalkyl, alkenyl or alkinyl; R6 stands for alkyl or halogen alkyl; R7 stands for alkyl, halogen alkyl, alkoxyalkyl, alkenyl or alkinyl; R8 stands for hydrogen or alkyl; R9 stands for alkyl, alkenyl, alkinyl, phenyl or benzyl; R10 stands for alkyl, halogen alkyl, alkenyl or alkinyl; Q stands for an optionally substituted cyclohexan-1,3-dione ring linked in position 2. Also disclosed are the salts of these compounds useful in agriculture; processes and intermediate products for preparing the compounds of formula (I), agents containing the same and the use of these derivatives or agents containing the same for controlling undesirable plants.

    摘要翻译： 本发明涉及式I的2-苯甲酰基环己烷-1,3-二酮，其中R1，R2各自为氢，硝基，卤素，氰基，氰硫基，烷基，卤代烷基，烷氧基烷基，烯基，炔基，-OR5，-OCOR6，-OSO2R6， -SH，-S（O）nR7，-SO2OR5，-SO2NR5R8，-NR8SO2R6或-NR8COR6; R3是氢，氰基，烷基，卤代烷基，-OR7，-SR7或-NR7R10; R4是氢，取代或未取代的烷基， 环烷基，烯基，环烯基，炔基，-COR 9，-CO 2 R 9，-COSR 9或-CONR 8 R 9; X是氧或NR 8; n是0,1或2; R 5是氢，烷基，卤代烷基，烷氧基烷基，烯基或炔基; 烷基或卤代烷基; R 7是烷基，卤代烷基，烷氧基烷基，烯基或炔基; R 8是氢或烷基; R 9是烷基，烯基，炔基，苯基或苄基; R 10是烷基，卤代烷基，链烯基或炔基; Q是环己烷-1 具有或不具有取代基的2-二酮环，其位置2;及其农业上有用的盐;制备式I化合物的方法和中间体; 包含它们的组合物; 以及使用这些衍生物或包含它们的组合物来控制不期望的植物。

    HERBIZIDE BENZOYLDERIVATE
    8.
    发明公开
    HERBIZIDE BENZOYLDERIVATE 失效
    除草剂苯甲酰

    公开(公告)号：EP0811005A1

    公开(公告)日：1997-12-10

    申请号：EP96904761.0

    申请日：1996-02-13

    申请人： BASF AKTIENGESELLSCHAFT

    发明人： VON DEYN, Wolfgang ,  HILL, Regina, Luise ,  KARDORFF, Uwe ,  ENGEL, Stefan ,  OTTEN, Martina ,  VOSSEN, Marcus ,  PLATH, Peter ,  RANG, Harald ,  HARREUS, Albrecht ,  RÖHL, Franz ,  WALTER, Helmut ,  WESTPHALEN, Karl-Otto ,  MISSLITZ, Ulf

    IPC分类号： C07D239 ,  A01N43 ,  C07D207 ,  C07D213 ,  C07D215 ,  C07D231 ,  C07D235 ,  C07D261 ,  C07D263 ,  C07D271 ,  C07D275 ,  C07D277 ,  C07D279 ,  C07D285 ,  C07D307 ,  C07D317 ,  C07D319 ,  C07D327 ,  C07D333 ,  C07D335 ,  C07D339 ,  C07D405 ,  C07D407 ,  C07D409 ,  C07D413 ,  C07D417

    CPC分类号： C07D271/06 ,  A01N43/08 ,  A01N43/10 ,  A01N43/74 ,  A01N43/80 ,  C07D261/04 ,  C07D261/08 ,  C07D263/14 ,  C07D263/32 ,  C07D277/26 ,  C07D307/46 ,  C07D333/22

    摘要： The invention concerns benzoyl derivatives of formula (I) in which the substituents have the following meanings: L and M represent hydrogen, C1-C6 alkyl, C2-C6 alkenyl, C2-C6 alkinyl, C1-C4 alkoxy (these groups being optionally substituted by one to five halogen atoms or C1-C4 alkoxy), halogen, cyano, nitro, a -(Y)n-S(O)mR7 or -(Y)¿n-CO-R?8 group; Z represents a five to six-membered heterocyclic saturated or unsaturated group containing one to three heteroatoms selected from the group comprising oxygen, sulphur and nitrogen and which can optionally be substituted by halogen, cyano, nitro, a -CO-R8 group, C¿1?-C4 alkyl, C1-C4 alkyl halide, C3-C8 cycloalkyl, C1-C4 alkoxy, C1-C4 alkoxy halide, C1-C4 alkyl thio, C1-C4 alkyl thio halide, di-C1-C4 alkyl amino, phenyl optionally substituted by halogen, cyano, nitro, C1-C4 alkyl or C1-C4 alkyl halide, or an oxo group which can be present in the tautomeric form as a hydroxy group, is substituted or, together with a condensation-bound phenyl ring which is optionally substituted by halogen or, cyano, nitro, C1-C4 alkyl or C1-C4 alkyl halide, with a condensation-bound carbocycle or with a condensation-bound second heterocycle which can optionally be substituted by halogen, cyano, nitro, C1-C4 alkyl, di-C1-C4 alkyl amino, C1-C4 alkoxy, C1-C4 alkoxy halide or a C1-C4 alkyl halide, forms a bicyclic system; Y represents O or NR?9¿; n is 0 or 1; m is 0, 1 or 2; R7 represents C¿1?-C4 alkyl, C1-C4 alkyl halide or NR?9R10; R8¿ represents C¿1?-C4 alkyl, C1-C4 alkyl halide, C1-C4 alkoxy or NR?9R10; R9¿ represents hydrogen or C¿1?-C4 alkyl; R?10¿ represents C¿1?-C4 alkyl; Q represents a cyclohexane-1,2-dione ring connected at position 2 and of formula (II) in which R?1, R2, R4 and R6¿ represent hydrogen or C¿1?-C4 alkyl, R?5¿ represents hydrogen, C¿1?-C4 alkyl or a -COOR?10¿ group, R3 represents hydrogen, C¿1?-C4 alkyl, C3-C6 cycloalkyl, these groups optionally including one to three of the following substituents: halogen, C1-C4 alkyl thio, C1-C4 alkoxy, or R?3¿ represents tetrahydropropanyl-3, tetrahydropropanyl-4 or tetrahydrothiopyranyl-3, or R?3 and R5¿ together form a bond or a three to six-membered carbocyclic ring. The invention also concerns standard agricultural salts of compounds of formula (I) usually utilized in agriculture.

    VERFAHREN ZUR HERSTELLUNG SUBSTITUIERTER BIPHENYLE
    10.
    发明公开
    VERFAHREN ZUR HERSTELLUNG SUBSTITUIERTER BIPHENYLE 有权
    用于生产取代BIPHENYLS

    公开(公告)号：EP1856024A1

    公开(公告)日：2007-11-21

    申请号：EP06708604.1

    申请日：2006-03-02

    申请人： BASF AKTIENGESELLSCHAFT

    发明人： ENGEL, Stefan ,  OBERDING, Tanja

    IPC分类号： C07C201/12 ,  C07C205/12

    CPC分类号： C07C209/68 ,  C07C201/12 ,  C07C211/52 ,  C07C205/11

    摘要： The invention relates to a method for producing substituted biphenyls (I) in which: R1 = nitro, amino or NHR3: R2 = CN, NO2, halogen, C1-C6 alkyl, C2-C6 alkenyl, C2-C6 alkynyl, C1-C6-alkoxy, C1-C6 alkyl halide, C1-C6 alkylcarbonyl or phenyl; R3 = C1-C4 alkyl, C2-C4 alkenyl or C2-C4 alkynyl; m = 1 or 2, and; n = 0 to 3. The invention is characterized in that a compound (II) is reacted with a diphenyl borinic acid (III) in the presence of a base and of a palladium catalyst selected from the group consisting of: a) palladium-trialkylphosphine or trialkylphosphine complex with palladium being zero in the oxidation state; b) salt of the palladium in the presence of triarylphosphine or trialkylphosphine serving as a complex ligand or; c) optionally, metallic palladium raised on substrates, in the presence of triarylphospine or trialkylphosphine in a solvent.