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    ROHRBÜNDELREAKTOR FÜR UNKATALYSIERTE ODER HOMOGENKATALYSIERTE REAKTIONEN
    2.
    发明公开
    ROHRBÜNDELREAKTOR FÜR UNKATALYSIERTE ODER HOMOGENKATALYSIERTE REAKTIONEN 有权
    管式反应器非催化或均匀催化反应

    公开(公告)号：EP2389241A2

    公开(公告)日：2011-11-30

    申请号：EP10701318.7

    申请日：2010-01-19

    Applicant: BASF SE

    Inventor： TELES, Joaquim, Henrique ,  RESCH, Peter ,  RUPPEL, Wilhelm ,  WEGERLE, Ulrike ,  GERLINGER, Wolfgang ,  RÖSSLER-FEIGEL, Beatrice ,  MEIER, Anton ,  MÜLLER, Christian

    IPC: B01J19/24

    CPC classification number: B01J19/2425 ,  B01J4/001 ,  B01J19/006 ,  B01J2219/00085 ,  B01J2219/00166 ,  F28D7/16 ,  F28F9/0265 ,  F28F9/0275 ,  F28F9/0278 ,  Y02P20/582

    Abstract: The invention relates to a tube bundle reactor having a flat feed dome. Alternatively, the discharge dome can also be designed flat. The flat design reduces the reaction heat developing in the hood in reaction types that take place not only in the tube bundle (non-catalyzed reactions and reactions with homogenously distributed catalyst). Undesired reactions that already take place in the dome due to accumulated heat are thus heavily suppressed, whereby greater selectivity in temperature-sensitive reactions is achieved. Additionally, the temperature distribution within the domes can be precisely controlled. The tube bundle reactor comprises a tube bundle that has a feed end connected to a feed dome of the tube bundle reactor, wherein the feed dome is designed in a flat shape having a cross-sectional surface at the feed end and an inner volume, and the ratio of the inner volume to the cross-sectional surface is less than 0.35 m. The invention is furthermore implemented by a method for operating a tube bundle reactor, comprising: introducing a reactant mixture into a tube bundle and converting at least a portion of the reactant mixture into a product inside the tube bundle. The introduction step comprises: feeding the reactant mixture into an inner space of a feed dome of the tube bundle reactor and forwarding the reactant mixture into a feed end of the tube bundle in the form of a fluid flow. The fluid flow has a cross-sectional surface upon entering the feed end and the inner space of the feed dome through which the fluid flows has an inner volume; wherein the ratio of the inner volume to the cross-sectional surface is less than 0.35 m.

    PROCESS FOR PRODUCING PROPYLENE OXIDE
    7.
    发明公开
    PROCESS FOR PRODUCING PROPYLENE OXIDE 有权
    生产环氧丙烷的方法

    公开(公告)号：EP2430009A1

    公开(公告)日：2012-03-21

    申请号：EP10715902.2

    申请日：2010-05-05

    Applicant: BASF SE ,  The Dow Chemical Company

    Inventor： KAMPE, Philip ,  RESCH, Peter ,  CHIN, Soo, Yin ,  BAßLER, Peter ,  MÜLLER, Ulrich ,  SCHINDLER, Götz-Peter ,  GÖBBEL, Hans-Georg ,  TELES, Joaquim, Henrique ,  GUMLICH, Kai ,  GRAßLER, Thomas ,  BARTOSCH, Christian ,  JACUBINAS, Richard ,  WEIDENBACH, Meinolf

    IPC: C07D301/12

    CPC classification number: C07D301/12 ,  Y02P20/52

    Abstract: A process for producing propylene oxide comprising reacting propene with hydrogen peroxide in the presence of a catalyst to give a mixture (Gl) comprising propylene oxide, unreacted propene, and oxygen; separating propylene oxide from mixture (Gl) to give a mixture (GII) comprising propene and oxygen; and adding hydrogen to mixture (GII) and reducing the oxygen comprised in mixture (GII) at least partially by reaction with hydrogen in the presence of a catalyst comprising copper in elemental and/or oxidic form on a support, wherein copper is present on the support in an amount of 30 to 80 wt.-% based on the whole catalyst and calculated as CuO.

    Abstract translation: 一种生产环氧丙烷的方法，包括在催化剂存在下使丙烯与过氧化氢反应，得到包含环氧丙烷，未反应的丙烯和氧的混合物（G1） 从混合物（G1）分离环氧丙烷以得到包含丙烯和氧的混合物（GII）; 并且在包含元素和/或氧化物形式的铜的催化剂存在下，在混合物（GII）中加氢并至少部分地通过与氢反应来还原混合物（GII）中包含的氧，其中铜存在于 基于整个催化剂的30-80重量％的载体并且以CuO计算。

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