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    PROCESS FOR THE MANUFACTURE OF THIAZOLE DERIVATIVES WITH PESTICIDAL ACTIVITY
    4.
    发明授权
    PROCESS FOR THE MANUFACTURE OF THIAZOLE DERIVATIVES WITH PESTICIDAL ACTIVITY 有权
    生产具有杀虫效果的噻唑衍生物

    公开(公告)号：EP1330446B1

    公开(公告)日：2010-04-07

    申请号：EP01988714.0

    申请日：2001-10-25

    申请人： Syngenta Participations AG

    发明人： RAPOLD, Thomas ,  SEIFERT, Gottfried ,  SENN, Marcel

    IPC分类号： C07D277/32 ,  C07D417/06 ,  A01N43/78 ,  A01N43/88

    CPC分类号： C07D277/32 ,  C07D417/06

    摘要： A process for the preparation of a compound of the formula (I) in which Q, Y, Z, R1, R2 are as defined in claim 1; in which a) a compound of the formula (II), in which X is a leaving group, is reacted with a halogenating agent to give a compound of the formula (III), in which W is a halogen atom; and b) the resulting compound of the formula (III) is reacted with a compound of the formula (IV), in which R1, R2, Y, Z and Q are as defined in claim 1; wherein the preparation of the compound of the formula (III) according to process stage a) involves a purification step in which the reaction mass which has formed is treated with water in the acidic pH range; a process for the preparation of a compound of the formula (III) according to the abovementioned process a), and the use of the compounds of the formulae (II), (III) and (IV) in a process as detailed above are described.

    PROCESS FOR THE SYNTHESIS OF MANDIPROPAMID AND DERIVATIVES THEREOF
    5.
    发明公开
    PROCESS FOR THE SYNTHESIS OF MANDIPROPAMID AND DERIVATIVES THEREOF 有权
    用于生产双炔酰菌及其衍生物的

    公开(公告)号：EP1919857A2

    公开(公告)日：2008-05-14

    申请号：EP06765248.7

    申请日：2006-08-08

    申请人： Syngenta Participations AG

    发明人： BOWDEN, Martin, Charles ,  CLARK, Thomas, Aitcheson ,  GIORDANO, Fanny, Delphine, Brigtte ,  JAU, Beat ,  SCHNEIDER, Hans-Dieter ,  SEIFERT, Gottfried ,  WISS, Juerg ,  ZELLER, Martin ,  FABER, Dominik

    IPC分类号： C07C231/02 ,  C07C235/34 ,  C07C59/70 ,  C07C43/174 ,  C07C43/313

    CPC分类号： C07C231/12 ,  C07C33/46 ,  C07C59/70 ,  C07C69/734 ,  C07C213/02 ,  C07C235/34 ,  C07C251/16 ,  C07C255/37 ,  C07C315/04 ,  C07C319/20 ,  C07C317/46 ,  C07C323/62

    摘要： A process for the preparation of a compound of formula (I) wherein: R is an alkynyl group; R1 is alkyl, alkenyl, alkynyl, cycloalkyl, cycloalkyl-alkyl, phenyl and phenylalkyl, it being possible in turn for all of the receding groups to carry one or more identical or different halogen atoms; alkoxy; alkenyloxy; alkynyloxy; alkoxyalkyl; haloalkoxy; alkylthio; haloalkylthio; alkysulfonyl; formyl; alkanoyl; hydroxy; halogen; cyano; nitro; amino; alkylamino; dialkylamino; carboxyl; alkoxycarbonyl; alkenyloxycarbonyl; or alkynyloxycarbonyl; and n is an integer from 0 to 3, said process comprising: (i) the reaction of a compound of formula (III) wherein R, R1 and n are as hereinbefore defined; m and m' are independently 0 or 1; when m and m' are both 0, A is an alkyl, alkenyl or alkynyl group (suitably having up to eight carbon atoms), optionally substituted by one or more groups independently selected from halogen, hydroxy, alkoxy, C1-4 dialkylamino or cyano; when one of m and m' is 0 and the other is 1, A is an alkanediyl, alkenediyl or alkynediyl group containing at least two carbon atoms (and suitably having up to eight carbon atoms), optionally substituted by one or more groups independently selected from halogen, hydroxy, alkoxy, C1-4 dialkylamino or cyano; when m and m' are both 1, A is an alkanetriyl, alkenetriyl or alkynetriyl group containing at least three carbon atoms (and suitably having up to eight carbon atoms), optionally substituted by one or more groups independently selected from halogen, hydroxy, alkoxy, C1-4 dialkylamino or cyano; and wherein if the group A contains three or more carbon atoms, one or more of the carbon atoms may each optionally be replaced with an oxygen atom, provided that there is at least one carbon atom between any two oxygen atoms in the molecule, with a compound of formula (IV) to give a compound of formula (II) wherein R, R1 and n are as hereinbefore defined, and (ii) the reaction of a compound of formula (II) with , wherein L is a leaving group, to give the compound of formula (I) as hereinbefore defined, is disclosed.

    PROCESS FOR THE PREPARATION OF THIOPHENOLS
    6.
    发明授权
    PROCESS FOR THE PREPARATION OF THIOPHENOLS 有权
    用于生产苯硫酚

    公开(公告)号：EP1330434B1

    公开(公告)日：2007-12-12

    申请号：EP01986676.3

    申请日：2001-10-09

    申请人： Syngenta Participations AG

    发明人： SEIFERT, Gottfried ,  URWYLER, Bernhard

    IPC分类号： C07C319/02 ,  C07C321/26

    CPC分类号： C07C319/02 ,  C07C323/62

    摘要： A process for the preparation of thiophenols of formula (I) wherein n is an integer from 1 to 5 and R is hydrogen, alkyl, hydroxyalkyl, alkylamino, dialkylamino, alkenyl, alkynyl, alkoxy, alkylthio, phenyl, naphthyl, phenoxy, phenylthio, halogen, hydroxy, mercapto, carboxyl, sulfo or heterocyclyl, by reacting phenyldiazonium salts of formula (II) wherein n and R are as defined and X is halogen or hydrogen sulfate, with sulfur at elevated temperature in the presence of an aqueous base and isolating the compounds of formula (I).

    PROCESS FOR THE MANUFACTURE OF THIAZOLE DERIVATIVES WITH PESTICIDAL ACTIVITY
    10.
    发明公开
    PROCESS FOR THE MANUFACTURE OF THIAZOLE DERIVATIVES WITH PESTICIDAL ACTIVITY 有权
    生产具有杀虫效果的噻唑衍生物

    公开(公告)号：EP1330446A1

    公开(公告)日：2003-07-30

    申请号：EP01988714.0

    申请日：2001-10-25

    申请人： Syngenta Participations AG

    发明人： RAPOLD, Thomas ,  SEIFERT, Gottfried ,  SENN, Marcel

    IPC分类号： C07D277/32 ,  C07D417/06 ,  A01N43/78 ,  A01N43/88

    CPC分类号： C07D277/32 ,  C07D417/06

    摘要： A process for the preparation of a compound of the formula (I) in which Q, Y, Z, R1, R2 are as defined in claim 1; in which a) a compound of the formula (II), in which X is a leaving group, is reacted with a halogenating agent to give a compound of the formula (III), in which W is a halogen atom; and b) the resulting compound of the formula (III) is reacted with a compound of the formula (IV), in which R1, R2, Y, Z and Q are as defined in claim 1; wherein the preparation of the compound of the formula (III) according to process stage a) involves a purification step in which the reaction mass which has formed is treated with water in the acidic pH range; a process for the preparation of a compound of the formula (III) according to the abovementioned process a), and the use of the compounds of the formulae (II), (III) and (IV) in a process as detailed above are described.