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    Process for the heterogeneous synthesis of chemical compounds
    1.
    发明授权
    Process for the heterogeneous synthesis of chemical compounds 有权

    公开(公告)号：EP1707259B1

    公开(公告)日：2018-06-06

    申请号：EP05007150.5

    申请日：2005-04-01

    申请人： CASALE SA

    发明人： Filippi, Ermanno ,  Tarozzo, Mirco ,  Rizzi, Enrico

    IPC分类号： B01J8/04 ,  B01J8/06

    CPC分类号： B01J8/0469 ,  B01J8/0496 ,  B01J8/067 ,  B01J2208/00194 ,  B01J2208/00371 ,  B01J2208/00522 ,  B01J2208/0053 ,  B01J2219/00024

    摘要： A reactor for heterogeneous synthesis of chemical compounds, in particular methanol, comprises: - a substantially cylindrical shell (12) closed at the opposite ends by respective bottoms (14, 16); - at least one first, adiabatic, catalytic bed (25, 26, 27) having a substantially annular section, coaxially supported inside the shell (12) in an upper portion (20) of the shell, the at least one catalytic bed (25, 26, 27) having an inlet side (25a, 26a, 27a) for the reagent gases or for a reaction mixture, and an outlet side (25b, 26b, 27b) for the reaction mixture, - a second, pseudo-isothermal, catalytic bed (31) having a substantially annular section, supported inside the shell (12) in a lower portion (21) of the shell, coaxially positioned with respect to the at least one first catalytic bed and at a pre-determined distance therefrom, said second catalytic bed having an inlet side for a reaction mixture coming from the at least one first catalytic bed (25, 26, 27) and an outlet side for gaseous reaction products; - a plurality of heat exchangers (45) supported and distributed in a respective annular portion of the second catalytic bed (31), the heat exchangers (45) being flown by a heat exchanger operating fluid.

    FASEROPTISCHE TEMPERATURMESSUNG IN EINER KATALYSATORSCHÜTTUNG
    3.
    发明公开
    FASEROPTISCHE TEMPERATURMESSUNG IN EINER KATALYSATORSCHÜTTUNG 审中-公开
    在EINERKATALYSATORSCHÜTTUNG的FASEROPTISCHE TEMPERATURMESSUNG

    公开(公告)号：EP3233261A1

    公开(公告)日：2017-10-25

    申请号：EP15819809.3

    申请日：2015-12-17

    申请人： MAN Diesel & Turbo SE

    发明人： EGNER, Franz ,  BANK, Rolf ,  BAUER, Andreas ,  LAINER, Martin ,  VERBEEK, Dieter

    IPC分类号： B01J8/06

    CPC分类号： B01J8/067 ,  B01J8/001 ,  B01J2208/00061 ,  B01J2208/00194 ,  B01J2208/00672 ,  B01J2208/065

    摘要： The invention relates to a tube reactor for carrying out heterogeneous catalysed gas phase reactions comprising a thermal tube (2), which contains a catalyst material (3) and around which a fluid heat transfer medium (5) flows on the outer face (25) during operation, the catalyst material (3) consisting of particles (4). The tube reactor also comprises a temperature-sensitive optical waveguide (9) which is surrounded by a capillary tube (8), extends into the catalyst material (3) of the thermal tube (2), has measuring points (35) having a predetermined spacing (a
    M ) between adjacent measurement points (35) in the axial direction of the thermal tube (2), and can be connected to a source for optical signals and to an evaluation unit (31) for optical signals reflected by the optical waveguide (9). At least in an axial thermal tube portion (34) of predetermined length containing at least a part of the catalyst material (3), the optical waveguide (9) has measuring points (35) having a spacing (a
    M ) between adjacent measuring points (35) in the axial direction of the thermal tube (2) which is 0.8 to 5 times the shortest edge length (l
    K ) of all imaginary cuboids which, having a minimum volume in the cases in which nominal external dimensions are associated with the particles (4) of the catalyst material (3), in each case delimit a particle (4) on the assumption that the particle (4) has the nominal external dimension thereof, and in all other cases in each case delimit said particles (4) which belong to a proportion by mass of a minimum of 70 % of the catalyst material (3) to which all the particles (4) having imaginary cuboids belong, wherein each edge length is longer than the shortest edge length (l
    K ).

    摘要翻译： 本发明涉及用于进行非均相催化气相反应的管式反应器，其包括含有催化剂材料（3）并且流体传热介质（5）在外表面（25）上流动的热管（2） 在操作期间，由颗粒（4）组成的催化剂材料（3）。 管式反应器还包括被毛细管（8）包围的温度敏感光波导（9），延伸到热管（2）的催化剂材料（3）中，具有预定的测量点（35） 在热管（2）的轴向上的相邻测量点（35）之间的间隔（a M），并且可以连接到光信号源和评估单元（31），用于光信号反射的光信号 （9）。 至少在包含催化剂材料（3）的至少一部分的预定长度的轴向热管部分（34）中，光波导（9）具有测量点（35），测量点（35）在相邻的测量点 （35）在热管（2）的轴向上的长度是所有假想长方体的最短边缘长度（l K）的0.8至5倍，在所有假想长方体中，具有最小体积的标称外部尺寸与 在假定颗粒（4）具有其标称外部尺寸的情况下，催化剂材料（3）的颗粒（4）在每种情况下限定颗粒（4），并且在所有其他情况下分别限定所述颗粒 ），其中每个边缘长度都比最短边缘长度（1K）长，所有这些具有虚拟立方体的粒子（4）所属的催化剂材料（3）的最小值为70％。

    A METHOD FOR REVAMPING AN AMMONIA CONVERTER
    6.
    发明公开
    A METHOD FOR REVAMPING AN AMMONIA CONVERTER 审中-公开
    VERFAHREN ZUR MODERNISIERUNG EINES AMMONIAKWANDLERS

    公开(公告)号：EP3115338A1

    公开(公告)日：2017-01-11

    申请号：EP15175687.1

    申请日：2015-07-07

    申请人： Casale SA

    发明人： Carrara, Davide

    IPC分类号： C01C1/04 ,  B01J8/04

    CPC分类号： C01C1/0417 ,  B01J8/0415 ,  B01J8/0496 ,  B01J2208/0015 ,  B01J2208/00194 ,  B01J2208/0053 ,  B01J2219/00024 ,  Y02P20/52

    摘要： Method for revamping a multi-bed ammonia converter, wherein said converter comprises a plurality of adiabatic catalytic beds including a first catalytic bed and one or more further catalytic bed(s), said catalytic beds being arranged in series so that the effluent of a bed is further reacted in the subsequent bed; at least a first inter-bed heat exchanger arranged between said first catalytic bed and a second catalytic bed to cool the effluent of said first bed before admission into said second bed, and optionally further inter-bed heat exchanger(s) arranged between consecutive beds; said method involves the conversion of said first catalytic bed into an isothermal catalytic bed.

    摘要翻译： 一种改进多床氨转化器的方法，其中所述转化器包括多个绝热催化床，包括第一催化床和一个或多个另外的催化床，所述催化床被串联排列，使得床的流出物 在随后的床中进一步反应; 布置在所述第一催化床和第二催化床之间的至少第一床间热交换器，以在进入所述第二床之前冷却所述第一床的流出物，以及任选地进一步布置在连续床之间的床间热交换器 ; 所述方法涉及将所述第一催化床转化为等温催化床。