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    A process for treatment of polymers using a spouted bed mixer
    6.
    发明公开
    A process for treatment of polymers using a spouted bed mixer 审中-公开
    Verfahren zur Behandlung von Polymeren mithilfe eines Strahlschichtmischers

    公开(公告)号：EP2949688A1

    公开(公告)日：2015-12-02

    申请号：EP14169934.8

    申请日：2014-05-27

    Applicant: Borealis AG

    Inventor： Vavizos, Nikolaos ,  Kanellopoulos, Vasileios ,  Krallis, Apostolos

    IPC: C08J3/20 ,  C08L23/10 ,  B01J8/24 ,  C08L23/26 ,  C08L23/12 ,  C08K5/14 ,  C08K5/01 ,  C08F8/00 ,  C08F255/02 ,  C08F236/06

    CPC classification number: B01J8/386 ,  B01J8/10 ,  B01J8/245 ,  B01J2208/00274 ,  B01J2208/00557 ,  C08F8/00 ,  C08F255/02 ,  C08F2810/10 ,  C08J3/203 ,  C08J2323/12 ,  C08K5/14 ,  C08L23/12 ,  C08K5/01 ,  C08F110/06 ,  C08F236/06

    Abstract: The present invention relates to a process for the chemical treatment of polymers comprising the following steps:
    i) providing a polymer P);
    ii) introducing the polymer P) into a spouted bed mixer;
    iii) keeping the polymer P) within the spouted bed mixer such that the mean residence time τ of the polymer P) in the spouted bed mixer is at least 1 minute;
    iv) optionally, contacting the polymer P) with a chemical substance B) in the spouted bed mixer during step iii);
    v) withdrawing the polymer from the spouted bed mixer whereby a chemical substance A) is added to the polymer P) during the course of steps i) to iii) or, in case step iv) is present during the course of steps i) to iv).
    The present invention furthermore relates to a spouted bed mixer for the chemical treatment of polymers comprising feeding means for feeding polymer to the spouted bed mixer whereby the feeding means are equipped with means for contacting the polymer with a chemical substance A) prior to feeding to the spouted bed mixer.
    The present invention furthermore, relates to the use of a spouted bed mixer in the production of high melt strength polypropylene and to a polymer obtainable by the process according to the invention.

    Abstract translation: 本发明涉及一种化学处理聚合物的方法，包括以下步骤：i）提供聚合物P）; ii）将聚合物P引入喷射床混合器中; iii）将聚合物P保持在喷射床混合器内，使得喷射床混合器中聚合物P）的平均停留时间Ä至少为1分钟; iv）任选地，在步骤iii）期间在喷射床混合器中使聚合物P）与化学物质B）接触; v）从喷射床混合器中取出聚合物，其中在步骤i）至iii）过程中将化学物质A）加入到聚合物P）中，或者在步骤i）过程中存在步骤i）至 ⅳ）。 本发明还涉及一种用于化学处理聚合物的喷射床混合器，其包括用于将聚合物进料到喷射床混合器的进料装置，由此进料装置装备有用于使聚合物与化学物质A）接触的装置， 喷出式搅拌机 本发明还涉及喷射床混合器在生产高熔体强度聚丙烯和通过本发明方法获得的聚合物中的用途。

    INTEGRATED SYSTEM TECHNIQUE FOR COUPLING FIXED BED AND JET FLUIDIZED BED TO SEPARATOR UNIT
    8.
    发明公开
    INTEGRATED SYSTEM TECHNIQUE FOR COUPLING FIXED BED AND JET FLUIDIZED BED TO SEPARATOR UNIT 有权
    集成系统及方法硬床的交联和流化床分离器

    公开(公告)号：EP2745924A4

    公开(公告)日：2015-06-17

    申请号：EP12807318

    申请日：2012-05-25

    Applicant: UNIV NANJING

    Inventor： ZHOU ZHENG ,  ZHANG ZHIBING ,  YANG GAODONG ,  GONG XIONGHUI ,  WU PINGKENG

    IPC: B01J8/00

    CPC classification number: B01D3/009 ,  B01J8/005 ,  B01J8/02 ,  B01J8/08 ,  B01J8/20 ,  B01J19/18 ,  B01J2208/00557 ,  B01J2219/00006 ,  B01J2219/0004 ,  C07C29/04 ,  C07C29/48 ,  C07C67/08 ,  C07C67/297 ,  C07C2101/16 ,  C07C2601/16 ,  Y02P20/582 ,  C07C33/025 ,  C07C33/14 ,  C07C69/14

    Abstract: This invention relates to a process of integrated system formed by coupling of fixed bed, jetting floating bed, and separating unit, aimed to provide a new process and equipment of higher efficiency, which integrates multi-type reactors and separation. In this invention, reaction materials will undergo preliminary reaction in fixed bed reactor and intensified reaction in jetting floating bed reactor, and then separation in the subsequent separation system. Unreacted materials will be returned to the raw material intermediate storage tank for mixing with fresh materials, as raw materials for continued reaction. During this process, materials first pass the fixed bed reactor once to achieve certain conversion rate, and then enter the jetting floating bed reactor for intensified reaction. When the product reaches required concentration, the materials will enter subsequent separation equipment for separation. During the whole process, fixed bed reactor, jetting floating bed reactor, and subsequent separation system are coupled, so that the flow path is more integrated, reaction time is greatly shortened, and process energy consumption is further lowered.

    Abstract translation: 本发明涉及通过固定床的耦合，喷射浮床，和分离单元上综合系统，目的在于提供高效率，它集成了多类型的反应器和分离的新工艺和设备的处理。 在本发明中，反应材料将发生固定床反应器预反应并加剧了在随后的分离系统的喷射浮床反应器中，然后分离反应，未反应的材料将被返回到原料中间储罐与新鲜材料混合， 作为用于持续反应的原料。 在此过程中，材料先通过固定床反应器一旦达到一定的转化率，然后进入喷射浮床反应器，用于增强反应。 当产物达到所需的浓度，该材料将进入随后的分离设备进行分离。 在整个过程中，固定床反应器，喷射浮床反应器中，和随后的分离系统被耦合，所以没有流动路径是集成度更高，反应时间大大缩短，而且过程的能量消耗进一步降低。

    Multistage process for the polymerization of olefins
    9.
    发明公开
    Multistage process for the polymerization of olefins 审中-公开
    烯烃聚合的多阶段过程

    公开(公告)号：EP2803680A1

    公开(公告)日：2014-11-19

    申请号：EP13168101.7

    申请日：2013-05-16

    Applicant: Basell Polyolefine GmbH

    Inventor： Penzo, Giuseppe ,  Mei, Gabriele ,  Meier, Gerhardus ,  Schueller, Ulf ,  Ciarrocchi, Antonio

    IPC: C08F210/00 ,  C08F2/00 ,  C08F2/34

    CPC classification number: C08F110/02 ,  B01J8/0025 ,  B01J8/1863 ,  B01J8/1872 ,  B01J8/26 ,  B01J19/245 ,  B01J2208/00274 ,  B01J2208/00292 ,  B01J2208/00557 ,  B01J2208/00752 ,  B01J2208/00761 ,  B01J2208/00769 ,  B01J2208/00991 ,  B01J2219/24 ,  C08F10/00 ,  C08F2/001 ,  C08F2/34 ,  C08F2/01 ,  C08F2500/12 ,  C08F2500/07 ,  C08F2500/24 ,  C08F2500/18

    Abstract: A process for polymerizing olefins at temperatures of from 30°C to 140°C and pressures of from 1.0 MPa to 10 MPa in the presence of a polymerization catalyst in a multistage polymerization of olefins in at least two serially connected gas-phase polymerization reactors, the process for transferring polyolefin particles from a first gas-phase polymerization reactor to a second gas-phase polymerization reactor comprising the steps of
    a) discharging polyolefin particles from the first gas-phase polymerization reactor into a separation chamber in which the polyolefin particles are separated from concomitantly discharged reaction gas, the separation chamber being at a lower pressure than the pressure in the first gas-phase polymerization reactor;
    b) transferring the polyolefin particles within the separation chamber into a lower part of the separation chamber which contains a bed of polyolefin particles which moves from top to bottom of this part of the separation chamber and into which a fluid is introduced in an amount that an upward stream of the fluid in the bed of polyolefin particles above the fluid introduction point is induced,
    c) withdrawing polyolefin particles from the lower end of said lower part and transferring them to one of at least two lock hoppers working intermittently in parallel; and
    d) simultaneously pressurizing another of the at least two lock hoppers working intermittently by means of a gas comprising reaction gas coming from the second gas-phase polymerization reactor, and
    apparatus for the multistage polymerization of olefins, comprising at least two serially connected gas-phase polymerization reactors and a device for transferring polyolefin particles from an upstream gas-phase polymerization reactor to a downstream gas-phase polymerization reactor, the transferring device comprising
    - a gas/solid separation chamber placed downstream of the upstream gas-phase polymerization which gas/solid separation chamber is equipped at a lower part with an inlet for introducing a fluid, and
    - connected to the gas/solid separation chamber at least two lock hoppers, placed in a parallel arrangement, each connected to the downstream gas-phase polymerization reactor.

    Abstract translation: 在至少两个串联连接的气相聚合反应器中，在聚合催化剂存在下，在烯烃的多级聚合反应中，在30℃至140℃的温度和1.0MPa至10MPa的压力下聚合烯烃的方法， 将聚烯烃颗粒从第一气相聚合反应器转移到第二气相聚合反应器的方法包括以下步骤：a）将聚烯烃颗粒从第一气相聚合反应器排出到其中分离聚烯烃颗粒的分离室中 来自伴随排出的反应气体，分离室的压力低于第一气相聚合反应器中的压力; b）将分离室内的聚烯烃颗粒转移到分离室的下部，该分离室包含聚烯烃颗粒床，所述聚烯烃颗粒床从该分离室的该部分的顶部移动到底部并且以这样的量引入流体， 诱导在流体引入点之上的聚烯烃颗粒床中的流体的向上流，c）从所述下部的下端抽出聚烯烃颗粒，并将它们传送到并行间歇工作的至少两个闭锁料斗中的一个; 和d）同时通过包含来自第二气相聚合反应器的反应气体的气体对间歇工作的至少两个闭锁料斗中的另一个进行加压，以及用于烯烃多级聚合的设备，其包括至少两个串联连接的气 - 以及将聚烯烃颗粒从上游气相聚合反应器转移到下游气相聚合反应器的装置，所述转移装置包括：气/固分离室，其置于上游气相聚合的下游，气/ 固体分离室在下部装备有用于引入流体的入口，并且 - 与气体/固体分离室连接至少两个平行布置的锁定料斗，每个锁定料斗连接到下游气相聚合反应器。

    REGENERATION DE CATALYSEUR EN CONTINU DANS UN REACTEUR A LIT FLUIDISE
    10.
    发明公开
    REGENERATION DE CATALYSEUR EN CONTINU DANS UN REACTEUR A LIT FLUIDISE 有权
    与反应区和连续催化剂再生区的流化床反应器流化床反应器

    公开(公告)号：EP2731703A2

    公开(公告)日：2014-05-21

    申请号：EP12744067.5

    申请日：2012-07-09

    Applicant: Arkema France

    Inventor： DUBOIS, Jean-Luc ,  PATIENCE, Grégory

    IPC: B01J8/00 ,  B01J8/18 ,  B01J8/38 ,  B01J8/22 ,  B01J38/22

    CPC classification number: B01J8/24 ,  B01J8/0055 ,  B01J8/1818 ,  B01J8/1827 ,  B01J8/1836 ,  B01J8/226 ,  B01J8/386 ,  B01J23/92 ,  B01J27/285 ,  B01J38/30 ,  B01J2208/00141 ,  B01J2208/00203 ,  B01J2208/00557 ,  B01J2208/0084 ,  C07C45/38 ,  C07C45/52 ,  C07C51/215 ,  C07C51/235 ,  C07C51/265 ,  C07C51/313 ,  C07C51/377 ,  Y02P20/584 ,  C07C47/22 ,  C07C57/04 ,  C07C63/26 ,  C07C63/16 ,  C07C57/145 ,  C07C47/06

    Abstract: The invention relates to a catalytic reactor including a chamber (1) and separation means (2) arranged inside the chamber (1), said separation means defining at least one reaction area (3) and at least one regeneration area (4), the reaction area (3) being supplied by a reaction flow supply device (15, 16) and connected, at the outlet thereof, to a first gas tapping device (13), the regeneration area (4) being supplied by a regeneration flow supply device (17) and connected, at the outlet thereof, to a second gas tapping device (10), the reactor being suitable for comprising a fluidized bed of catalyst particles (5) in the reaction area (3), the separation means (2) being suitable for enabling the catalyst particles to pass from the reaction area (3) to the regeneration area (4), and the reactor being suitable for comprising a device for feeding catalyst particles into the regeneration area (4), thereby enabling the return thereof to the reaction area (3).

    Abstract translation: 的催化反应器包括腔室（1）和分离装置（2）布置在所述腔室（1）的内部在所述分离装置限定的至少一个反应区域（3）和至少一个再生区域（4）中，反应区（3 ）被提供有反应流（15，16）并连接，在其出口，在第一自攻气体装置（13），所述再生区域（4）被提供有一个再生流（17）和连接，在 它们的出口，在第二自攻气装置（10），该反应器适合于包含催化剂颗粒的流化床（5）在所述反应区域（3），所述分离装置（2）使所述催化剂颗粒从传 反应区（3）到再生区（4），并使得有可能的催化剂颗粒移动到再生区域（4），以使它们在反应区（3）的返回反应器中。

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