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    2-MERCAPTOBENZOTHIAZOLE MANGANESE ZINC, PREPARATION METHOD THEREFOR AND APPLICATION THEREOF
    1.
    发明公开
    2-MERCAPTOBENZOTHIAZOLE MANGANESE ZINC, PREPARATION METHOD THEREFOR AND APPLICATION THEREOF 有权
    2-MERCAPTOBENZOTHIAZOL-MANGAN-ZINK，HERSTELLUNGSVERFAHRENDAFÜRUND ANWENDUNG DAVON

    公开(公告)号：EP2937340A1

    公开(公告)日：2015-10-28

    申请号：EP13865389.4

    申请日：2013-11-30

    申请人： Henan Xinxiang Academy of Agriculture Sciences

    发明人： WANG, Zhenjun ,  ZHANG, Xu ,  WANG, Limin ,  LIU, Hongyan ,  LI, Mengjiao ,  CHENG, Senxiang

    IPC分类号： C07D277/70 ,  A01N43/48 ,  A01P3/00

    CPC分类号： C07D277/72 ,  A01N43/78 ,  A01N59/16 ,  C07D277/70 ,  Y02A50/359 ,  A01N2300/00

    摘要： The present invention belongs to the technical field of agricultural fungicides and discloses a 2-mercaptobenzothiazole manganese zinc, preparation method therefor and application thereof. The chemical structure of the 2-mercaptobenzothiazole manganese zinc is shown as the above formula. Wherein m, n and n' are positive integers, m = 2 (n + n'), n≥n', n: n' = 1: 1 ~ 9: 1. Materials are prepared according to the stoichiometric ratio of the target products; 2-mercaptobenzothiazole is dissolved in sodium hydroxide solution. The aqueous solution of water-soluble manganese salts and water-soluble zinc salts solution are successively added to 2-mercaptobenzothiazole sodium solution under stirring, followed by stirring for mixing well, then the solution being allowed to stand, filtered and washed with water to obtain filter cake, and then dried in vacuum to obtain 2-mercaptobenzothiazole manganese zinc. The present 2-mercaptobenzothiazole manganese zinc may be used as an agricultural fungicide. The present invention coordinates the surface of solid particles of 2-mercaptobenzothiazole manganese with zinc to form a stable clathrate of 2-mercaptobenzothiazole manganese and zinc. Tests show that the clathrate has excellent effect for controlling a plurality of diseases including apple alternaria leaf spot, pear scab, apple ring rot, apple anthracnose and the like.

    摘要翻译： 本发明属于农药杀菌剂的技术领域，公开了2-巯基苯并噻唑锰锌，其制备方法及应用。 2-巯基苯并噻唑锰锌的化学结构如上式所示。 其中m，n和n'为正整数，m = 2（n + n'），n‰¥n'，n：n'= 1：1〜9：1材料根据化学计量比 目标产品; 将2-巯基苯并噻唑溶解在氢氧化钠溶液中。 将水溶性锰盐和水溶性锌盐溶液水溶液在搅拌下依次加入到2-巯基苯并噻唑钠溶液中，搅拌均匀，然后静置，过滤并用水洗涤，得到 滤饼，然后真空干燥，得到2-巯基苯并噻唑锰锌。 本发明的2-巯基苯并噻唑锰锌可用作农业杀真菌剂。 本发明利用锌将2-巯基苯并噻唑锰的固体颗粒表面配位，形成稳定的2-巯基苯并噻唑锰和锌的包合物。 试验表明，包合物对于控制苹果花斑病，梨痂病，苹果腐烂，苹果炭疽病等多种疾病具有优异的效果。

    Silver halide photographic material
    3.
    发明公开
    Silver halide photographic material 失效
    卤化银照相材料

    公开(公告)号：EP0189840A3

    公开(公告)日：1989-09-27

    申请号：EP86100855.5

    申请日：1986-01-23

    申请人： FUJI PHOTO FILM CO., LTD.

    发明人： Miyasaka, Nobuaki ,  Suga, Shuzo

    IPC分类号： G03C1/46 ,  G03C1/02 ,  G03C1/34

    CPC分类号： C07D263/58 ,  C07D235/28 ,  C07D277/72 ,  G03C1/035 ,  G03C1/346 ,  G03C1/46 ,  G03C2001/03558 ,  Y10S430/162

    摘要： A silver halide photographic material is described, comprising a support bearing at least one silver halide photographic emulsion layer and at least one auxiliary layer on one side or both sides thereof, wherein the silver halide photographic emulsion layer is a layer made of a light-sensitive silver halide emulsion containing silver iodide and an internally fogged silver halide emulsion, or is composed of a layer made of the light-sensitive silver halide emulsion containing silver iodide and a layer made of the internally fogged silver halide emulsion, and the auxiliary layer contains substantially non-light-sensitive silver halide grains having an average grain size of not more than 0.5 µm.

    摘要翻译： 描述了一种卤化银照相材料，该材料包括载体，该载体带有至少一层卤化银照相乳剂层和在其一侧或两侧上的至少一层辅助层，其中卤化银照相乳剂层是由光敏感的 含有碘化银和内部雾化卤化银乳剂的卤化银乳剂，或者由含有碘化银的光敏卤化银乳剂和由内部雾化卤化银乳剂构成的层构成的层组成，辅助层基本上含有 平均粒度不大于0.5μm的非感光卤化银颗粒。

    Silver halide photographic light-sensitive materials
    4.
    发明公开
    Silver halide photographic light-sensitive materials 失效
    光敏感的卤化银照相材料。

    公开(公告)号：EP0175148A2

    公开(公告)日：1986-03-26

    申请号：EP85110265.7

    申请日：1985-08-16

    申请人： FUJI PHOTO FILM CO., LTD.

    发明人： Ikeda, Hideo ,  Ohno, Shigeru ,  Nakamura, Koki ,  Miyasaka, Nobuaki

    IPC分类号： G03C1/34

    CPC分类号： C07D263/58 ,  C07D235/28 ,  C07D277/72 ,  G03C1/346

    摘要： A silver halide photographic light-sensitive material comprising a support having coated thereon at least one silver halide emulsion layer and a surface protecting layer, said silver halide photographic light-sensitive material comprising photosensitive silver halide grains and internally fogged silver halide grains, said intemally fogged silver halide grains having adsorbed thereon at least one compound represented by the formula (I):
    wherein X represents -0-, -NH- or -S-, R 1 , R 2 , R 3 and R 4 represent hydrogen atom or a substituent, and at least one of R,, R 2 , R, and R. is substituted or unsubstituted alkyl or aryl group having up to 13 carbon atoms, which is bonded directly or through a divalent linkage group, to the aromatic nucleus.

    Korrosionsschutzüberzugsmittel
    5.
    发明公开
    Korrosionsschutzüberzugsmittel 失效
    防腐蚀保护涂层剂。

    公开(公告)号：EP0003817A1

    公开(公告)日：1979-09-05

    申请号：EP79100481.5

    申请日：1979-02-19

    申请人： Henkel Kommanditgesellschaft auf Aktien

    发明人： Eschwey, Helmut, Dr. ,  Galinke, Joachim, Dr. ,  Linden, Heinrich ,  Wegemund, Bernd, Dr. ,  Wiemers, Norbert, Dr.

    IPC分类号： C23F11/14 ,  C23F11/16 ,  C09D5/08

    CPC分类号： C09D5/086 ,  C07D277/72 ,  C09D7/45

    摘要： Korrosionsschutzüberzugsmittel für Metalloberflächen, enthaltend als Korrosionsinhibitor Zink- oder Bleisalze von mit mindestens einer Hydroxyl- oder Mercaptogruppe substituierten fünf- oder sechsgliedrigen Heterocyclen, die im Ring mindestens ein Stickstoffatom und konjugierte Doppelbindungen aufweisen, von denen mindestens eine in einer Gruppierung der Formel
    vorliegt. Besonders geeignet sind die Salze des Mercaptobenzthiazols, des Mercaptopyridins sowie der entsprechenden s-Triazinderivate, beispielsweise der Cyanursäure und der Thiocyanursaure.

    摘要翻译： 腐蚀保护性涂层材料的金属表面，含有作为缓蚀剂锌或至少一个羟基或巯基的铅盐取代的五元或六元杂环，其在环中含有至少一个氮原子和共轭双键，其中至少一个存在于所述式的部分 ， 特别合适的是巯基苯的盐，所述Mercaptopyridins和相应的s-三嗪衍生物，如氰尿酸和硫氰酸。

    METHOD OF OBTAINING 2-MERCAPTOBENZOTHIAZOLE
    7.
    发明公开
    METHOD OF OBTAINING 2-MERCAPTOBENZOTHIAZOLE 有权
    一种获得2-巯基苯

    公开(公告)号：EP1699769A1

    公开(公告)日：2006-09-13

    申请号：EP04809258.9

    申请日：2004-12-23

    申请人： DUSLO, a.s.

    发明人： KRIZANOVIC, Karol ,  MUNTAGOVA, Lubica

    IPC分类号： C07D277/72

    CPC分类号： C07D277/72

    摘要： 2-Mercaptobenzothiazole is obtained from a melt of the raw product prepared by the reaction of aniline, carbon disulphide and sulphur by pressure synthesis in a reactor, where the melt contains 2-mercaptobenzothiazole, unreacted raw materials, intermediate products and pitches, so that after reaching a stationary state of the reaction medium it includes the following steps: a) crystallization of the 2-mercaptobenzothiazole raw product from an aniline solution, b) dividing the liquid phase (FK) from crystallization from step a) in three parts, c) removing one part of the liquid phase (FK1) from crystallization from step a) out of the process, d) returning the second part of the liquid phase (FK2) from crystallization from step a) into the reactor for preparation of the raw product and supplementing it with sulphur and carbon disulphide with respect to aniline, e) final purification of the crystallized 2-mercaptobenzothiazole from step a) in the aniline liquid phase and separation of pure 2-mercaptobenzothiazole, f) using the third part of the liquid phase (FK3) from crystallization from step a), supplemented with the liquid phase (FR) from final purification from step e) and possibly with aniline for crystallization of a further batch of the 2­-mercaptobenzothiazole raw product, g) using the liquid phase (FR) from final purification from step f), together with a part of the liquid phase (FK3) from step e), possibly with aniline, for crystallization of the 2-mercaptobenzothiazole raw product, wherein the steps a) to g) are repeated.

    Verfahren zur Herstellung von 2-Chlor-benzothiazolen oder 2-Chlor-benzoxazolen
    9.
    发明公开
    Verfahren zur Herstellung von 2-Chlor-benzothiazolen oder 2-Chlor-benzoxazolen 失效
    一种用于2-氯苯并噻唑或2-氯恶唑的制备方法。

    公开(公告)号：EP0626379A3

    公开(公告)日：1995-08-30

    申请号：EP94105776.2

    申请日：1994-04-14

    申请人： BAYER AG

    发明人： Käss, Volker, Dr.

    IPC分类号： C07D277/68 ,  C07D263/58

    CPC分类号： C07D263/58 ,  C01B17/0253 ,  C07D277/68 ,  C07D277/70 ,  C07D277/72

    摘要： Die Titelverbindungen der Formel

    in der
    R¹ und R² unabhängig voneinander Wasserstoff, geradkettiges oder verzweigtes C₁-C₄-Alkyl, geradkettiges oder verzweigtes C₁-C₄-Alkoxy, Nitro, Fluor, Chlor, Brom, SO₂Cl, Cyano oder SO₂-C₁-C₄-alkyl bedeuten, und X für Schwefel oder Sauerstoff steht, können aus den zugehörigen 2-Mercapto-benzothiazolen oder 2-Mercapto-benzoxazolen durch Chlorierung mit Thionylchlorid in Gegenwart von Phosphorigsäure-Verbindungen der Formel
            YP(OR⁵)₂   (III)
    hergestellt werden, in der
    R⁵ Wasserstoff, geradkettiges oder verzweigtes, substituiertes oder unsubstituiertes C₁-C₁₂-Alkyl, Phenyl oder C₇-C₁₀-Aralkyl bedeutet und Y für Wasserstoff oder OR⁵ steht.