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公开(公告)号:US20170362348A1
公开(公告)日:2017-12-21
申请号:US15529661
申请日:2015-12-01
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Stefan H. Gryska , Hae-Seung Lee , Sung-Won Ha , Jenny B. Werness , Erick I. Soto Cantu , Babu N. Gaddam
IPC: C08F2/38 , C08F220/20 , C08F220/30 , C08F220/34 , C09J151/00 , C08F2/50 , C08F265/06 , C08F220/06 , C08F222/10 , C09J4/06 , C08F220/18
CPC classification number: C08F2/38 , C08F2/50 , C08F220/06 , C08F220/20 , C08F220/30 , C08F220/34 , C08F222/1006 , C08F265/06 , C08F2220/1858 , C08F2220/1875 , C08F2400/02 , C08F2500/01 , C08F2800/20 , C09J4/06 , C09J133/02 , C09J133/04 , C09J133/08 , C09J133/12 , C09J151/003
Abstract: Acrylic syrup polymer composition are provided by partially polymerizing a (meth)acrylic monomer mixture in the presence of a thiol chain transfer agent to produce a first syrup polymer composition comprising a low molecular weight solute (meth)acrylic copolymer and solvent monomers, quenching the chain transfer agent, further polymerizing the first syrup polymer composition to produce a second syrup polymer composition comprising the low molecular weight solute acrylic copolymer, a high molecular weight solute acrylic copolymer and optionally unreacted solvent monomers, optionally adding a crosslinker and photoinitiator; and further photopolymerizing the syrup polymer composition to produce a pressure-sensitive adhesive.
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公开(公告)号:US09803114B2
公开(公告)日:2017-10-31
申请号:US15311224
申请日:2015-05-26
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Sung-Won Ha , Babu N. Gaddam , Mark F. Ellis , Hae-Seung Lee , John R. Jacobsen
IPC: C08F2/46 , C08F2/50 , C08G61/04 , C09J133/08 , C08F2/38 , C08F220/18 , C09J4/00 , C08F265/06 , C09J4/06 , C09J151/00 , C09J7/02 , C08F220/06
CPC classification number: C09J133/08 , C08F2/38 , C08F2/50 , C08F220/06 , C08F220/18 , C08F265/06 , C08L2312/00 , C09J4/00 , C09J4/06 , C09J7/385 , C09J151/003 , C09J2433/00 , C08F2220/1858 , C08F2220/1841
Abstract: A method for preparing an acrylate adhesive is provided by the steps of partially polymerizing a monomer mixture to provide a syrup polymer composition having a high molecular weight solute copolymer. This first syrup composition is again polymerized to provide a second syrup polymer composition having a low molecular weight copolymer. The second syrup polymer composition is provided with a crosslinking agent and further polymerized to provide the adhesive composition.
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公开(公告)号:US10093753B2
公开(公告)日:2018-10-09
申请号:US15529661
申请日:2015-12-01
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Stefan H. Gryska , Hae-Seung Lee , Sung-Won Ha , Jenny B. Werness , Erick I. Soto Cantu , Babu N. Gaddam
IPC: C09J4/06 , C08F2/38 , C08F2/50 , C08F265/06 , C09J151/00 , C08F220/06 , C08F220/20 , C08F220/30 , C08F220/34 , C08F222/10 , C09J133/02 , C09J133/08 , C09J133/04 , C09J133/12 , C08F220/18
Abstract: Acrylic syrup polymer composition are provided by partially polymerizing a (meth)acrylic monomer mixture in the presence of a thiol chain transfer agent to produce a first syrup polymer composition comprising a low molecular weight solute (meth)acrylic copolymer and solvent monomers, quenching the chain transfer agent, further polymerizing the first syrup polymer composition to produce a second syrup polymer composition comprising the low molecular weight solute acrylic copolymer, a high molecular weight solute acrylic copolymer and optionally unreacted solvent monomers, optionally adding a crosslinker and photoinitiator; and further photopolymerizing the syrup polymer composition to produce a pressure-sensitive adhesive.
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公开(公告)号:US20170081567A1
公开(公告)日:2017-03-23
申请号:US15311224
申请日:2015-05-26
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Sung-Won Ha , Babu N. Gaddam , Mark F. Ellis , Hae-Seung Lee , John R. Jacobsen
IPC: C09J133/08 , C08F220/18 , C09J7/02
CPC classification number: C09J133/08 , C08F2/38 , C08F2/50 , C08F220/06 , C08F220/18 , C08F265/06 , C08L2312/00 , C09J4/00 , C09J4/06 , C09J7/385 , C09J151/003 , C09J2433/00 , C08F2220/1858 , C08F2220/1841
Abstract: A method for preparing an acrylate adhesive is provided by the steps of partially polymerizing a monomer mixture to provide a syrup polymer composition having a high molecular weight solute copolymer. This first syrup composition is again polymerized to provide a second syrup polymer composition having a low molecular weight copolymer. The second syrup polymer composition is provided with a crosslinking agent and further polymerized to provide the adhesive composition.
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