摘要:
A method of purifying lithium hexafluorophosphate that allows to purify lithium hexafluorophosphate, useful as lithium secondary cell electrolyte, organic synthesis medium or the like, to an extremely high purity is provided. Lithium hexafluorophosphate containing harmful impurities such as oxyfluoride, lithium fluoride is purified by adding phosphoric chloride. The purification is performed in the presence of phosphoric chloride and hydrogen fluoride of the quantity equal or superior to the equivalent amount for reacting them, and then by converting lithium fluoride lithium hexafluorophosphate with generated phosphor pentafluoride.
摘要:
A method of purifying lithium hexafluorosphate that allows to purify lithium hexafluorophosphate, useful as lithium secondary cell electrolyte, organic synthesis medium or the like, to an extremely high purity is provided. Lithium hexafluorophosphate containing harmful impurities such as oxyfluoride, lithium fluoride is purified by adding phosphoric chloride. The purification is performed in the presence of phosphoric chloride and hydrogen fluoride of the quantity equal or superior to the equivalent amount for reacting them, and then by converting lithium fluoride to lithium hexafluorophosphate with generated phosphor pentafluoride.
摘要:
The present invention provides a method enabling the high purification of a niobium compound and/or tantalum compound in a simplified manner at a low cost. This is accomplished by providing a method enabling the high purification of a niobium compound and/or tantalum compound comprising the steps of preparing a solution containing niobium and/or tantalum, allowing a precipitate comprising niobium and/or tantalum to develop, separating the precipitate by filtration from the filtrate, converting the precipitate to a liquid melt or taking the filtrate, and separating a niobium compound from a tantalum compound or vice versa by utilizing the difference in solubility to the solvent between the niobium compound and the tantalum compound.
摘要:
An object of the present invention is to provide a method for purifying a highly pure niobium compound and/or tantalum compound, the method enabling the purification of a highly pure niobium compound and tantalum compound in a simplified manner at a low cost. The object is met by providing a method comprising adding an organic solvent to an aqueous solution containing a niobium compound and/or tantalum compound together with impurities, and then performing extraction via the solution. A niobium compound and/or tantalum compound dissolved in a solution is allowed to precipitate, and said aqueous solution is obtained by dissolving the precipitate in water.
摘要:
The present invention provides a method enabling the high purification of a niobium compound and/or tantalum compound in a simplified manner at a low cost. This is accomplished by providing a method enabling the high purification of a niobium compound and/or tantalum compound comprising the steps of preparing a solution containing niobium and/or tantalum, allowing a precipitate comprising niobium and/or tantalum to develop, separating the precipitate by filtration from the filtrate, converting the precipitate to a liquid melt or taking the filtrate, and separating a niobium compound from a tantalum compound or vice versa by utilizing the difference in solubility to the solvent between the niobium compound and the tantalum compound.
摘要:
The present invention provides a method for purifying a niobium compound and/or tantalum compound in a simplified manner at a low cost. This is accomplished by providing a method for purifying a niobium compound and/or tantalum compound whereby a niobium compound and/or tantalum compound dissolved in a solvent is allowed to precipitate to be isolated.
摘要:
An object of the present invention is to provide a method for purifying a highly pure niobium compound and/or tantalum compound, the method enabling the purification of a highly pure niobium compound and tantalum compound in a simplified manner at a low cost. The object is met by providing a method comprising adding an organic solvent to an aqueous solution containing a niobium compound and/or tantalum compound together with impurities, and then performing extraction via the solution. A niobium compound and/or tantalum compound dissolved in a solution is allowed to precipitate, and said aqueous solution is obtained by dissolving the precipitate in water.
摘要:
A method for reducing oxygen and carbon components in high-purity fluoride such as calcium fluoride and barium fluoride (a high-purity fluoride that is not limited to calcium fluoride and barium fluoride), or in rare-earth fluorides such as ytterbium fluoride and cerium fluoride used for an optical fiber, a coating material, and so on. The oxygen and carbon components contained in the high-purity fluoride are reduced by a fluorine gas treatment.
摘要:
A humor sampling implement includes a detection unit having a main frame part possessing a blood transfer channel to collect blood through a blood inflow port and transfer the blood to a blood outflow port, and a test paper for detecting glucose in the blood transferred through the blood transfer channel. The main frame part is furnished with a projection protruding in the blood transfer channel toward the blood outflow port. The blood transfer channel can be configured to include a first blood transfer channel opening to the blood inflow port and a second blood transfer channel connected to the first blood transfer channel, wherein the direction of blood transfer is different from that in the first blood transfer channel, and the projection is provided at an end portion of the first blood transfer channel on blood outflow port side so as to protrude in the second blood transfer channel.
摘要:
A lancet instrument detachably fitted to a lancing apparatus, comprising a lancet having a lancet body with a sharp lancet tip at its tip, a lancet hub fixed to the lancet body so that the lancet tip is exposed, and an elastic deformation part extended from the lancet hub in the tip direction and elastically deformable so that the distance thereof from the lancet body can be changed, a ring-like member fitted to the outer periphery of the elastic deformation part and releasable in the tip direction by changing the distance between the elastic deformation part and the lancet body, and a casing having a ring-like member contact part storing the lancet so as to be movable in the longitudinal direction and formed in the inner peripheral part thereof so that the ring-like member is brought into contact therewith and stopped to move in the tip direction and a tip opening through which the lancet tip can be projected. The lancet instrument thus obtained is so formed that the projection of the lancet tip through the tip opening of the casing is blocked by moving the ring-like member released from the elastic deformation part in the tip direction between the tip of the elastic deformation part and the ring-like member contact part to restrict the movement of the lancet.