摘要:
For the production of a bubble-free vitreous material, and in particular bubble-free vitreous silica, bubbles-containing vitreous material is exposed in a furnace, at a temperature which reduces its viscosity to a value between 10.sup.13.5 and 10.sup.8 Pa.sec, to the omnidirectional pressure ranging from 100 to 3000 bars of a gas which is insoluble in the vitreous material for a period of not less than 10 minutes and is then cooled.
摘要:
A heat conductive ceramic substrate for semiconductor circuits, comprising polycrystalline aluminum nitride of high density containing as an additive boron nitride or oxides of calcium, magnesium, aluminum, titanium, zirconium, chrome, silicon, and/or rare earth metals. The boron nitride additive concentration ranges between 0.1 and 3% by weight, preferably between 0.5 and 2% by weight. The oxide additive concentration ranges between 0.1 and 5% by weight. The substrate has a significantly higher thermal conductivity than aluminum oxide substrates and is more economincal to manufacture than beryllium oxide substrates.
摘要:
The temperature stabilization body is made of pulverized aluminum nitride with a first additive of pulverized aluminum present between 0.05% to 2%, and a grain size of under 1 micrometer, and a second additive of from 0.1% to 10% of an oxide, preferably yttrium oxide, present at about 1%--all precentages by weight, in which the mixture is ground in a ceramic ball mill to a grain size of not over 0.1 mm, subjected to cold isostatic pressure in the order of 2500 bar to form a green, pressed body, and then sintered at a sintering temperature of between 1750.degree. C. to 2000.degree. C. The heat conductivity of the densely sintered aluminum nitride body will then be at least 140 W/m .degree.K., and a heat conductivity of twice as much can be obtained, the body being non-toxic and not subject to creep under temperatures up to at least 1700.degree. C.
摘要:
A low contamination crucible for pulling monocrystals of Group III and Group V elements of the Periodic Table, comprising particularly aluminum nitride with an additive of boron nitride or a rare earth oxide. The additive concentration is up to 5% by weight, but preferably 0.5% to 3% by weight. The hardness of the crucible of the invention is 300 to 400% greater than that of undoped material subjected to the same sintering conditions.
摘要:
In order to connect a tube of a more common material, such as stainless steel, to a tube of a highly corrosion-resistant metal such as tantalum, where the two tubes cannot be welded together by fussion technology, a connection piece is made of two closely fitting layers of the two materials telescoped into each other, which are exposed to hot compressed noble gas, such as argon, in a pressure vessel, with precautions against oxidation from residual oxygen in the noble gas. Then the ends are machined to remove any hard soldered portion used to make a gas-tight seal of the blank before pressure treatment, after which a longer ring-shaped section of the stainless part of the connection piece is removed at one end and likewise a section of the tantalum part of the connection piece at the other end, so that the projecting ends can be welded to the pipes to be joined. One method of protection against oxidation is to use a blank in which a tantalum tube is fitted between two stainless steel tubes, one of which is completely removed by machining after the pressure treatment.
摘要:
Optical-grade zinc sulfide bodies produced by the CVD technique and subjected to an aftertreatment under a high gas pressure and at elevated temperature possess improved optical properties. They are suited for use as infrared windows.
摘要:
The invention relates to a product (1), particularly a gas turbine blade that can be exposed to a hot aggressive gas (7). The product (1) has a metallic basic body (2), which is provided with a thermal barrier coating (4) having a spinel of the composition AB2O4.
摘要:
An article that is particularly well suited for use as a gas turbine engine component has a metallic substrate and a ceramic thermal barrier layer including a mixed metal oxide system comprising a compound selected from the group consisting of (i) a lanthanum aluminate and (ii) a calcium zirconate, the calcium in which is partially replaced by at least one calcium-substitute element, such as strontium (Sr) or barium (Ba). In addition, the lanthanum in the lanthanum aluminate can be partially replaced by a lanthanum-substitute element from the lanthanide group, particularly gadolinium (Gd). A process for producing such an article comprises providing a pre-reacted mixed metal oxide system as described above and applying it to the substrate by plasma spraying or an evaporation coating process.
摘要:
The invention relates to novel polysilazanes, the preparation thereof, the further processing thereof to form silicon nitride-containing ceramic material, and this material itself. In order to prepare the polysilazanes, dialkylaminoorganyldichlorosilanes of the formula RsiCl.sub.2 -Nr'R' are reacted with ammonia. The polysilazanes can then be pyrolyzed to form silicon nitride-containing ceramic material. The polysilazanes according to the invention dissolve in customary aprotic solvents.
摘要:
The invention relates to novel polymeric hydridosilazanes, processes for their preparation and their use for the preparation of ceramic material containing silicon nitride. To prepare the polymeric hydridosilazanes, polymeric hydridochlorosilazanes are reacted with NH.sub.3. To prepare the ceramic material containing silicon nitride, the polymeric hydridosilazanes are then pyrolyzed.