Diamond cutting tool and method of manufacturing the same
    3.
    发明授权
    Diamond cutting tool and method of manufacturing the same 失效
    金刚石切割工具及其制造方法

    公开(公告)号:US5567522A

    公开(公告)日:1996-10-22

    申请号:US318188

    申请日:1994-10-05

    摘要: A diamond cutting tool has a rake face (5) of a cutting edge member (2) consisting essentially of a (111) plane of diamond. The cutting edge member (2) of diamond is vapor-deposited by CVD or the like on an independently prepared base material. In this vapor deposition, the diamond is deposited while controlling and periodically varying the carbon to hydrogen ratio of the supplied raw material gas, in such a manner that a (111) crystal plane is oriented with a prescribed fluctuation or non-uniformity, but is substantially parallel to the base material surface. The as-formed diamond material is separated from the base material and cut into a desired shape, and then bonded as a cutting edge member (2) to a tool base (1) through a metallization layer (4) and a brazing layer (3), in such an orientation that the (111) plane defines the rake face (5). The tool having such a rake face (5) consisting essentially of the (111) plane, with a prescribed fluctuation of its orientation, is excellent in wear resistance and is resistant to cleavage damage.

    摘要翻译: 金刚石切割工具具有基本上由(111)钻石平面组成的切削刃部件(2)的前刀面(5)。 通过CVD等将金刚石的切削刃部件(2)以独立制备的基材气相沉积。 在这种气相沉积中,以(111)晶面以规定的波动或非均匀性取向的方式,控制和周期性地改变供给的原料气体的碳/氢比,沉积金刚石,但是 基本平行于基材表面。 将形成的金刚石材料与基材分离并切割成所需的形状,然后通过金属化层(4)和钎焊层(3)作为切割边缘部件(2)粘合到工具基体(1) ),以(111)面限定前刀面(5)的方向。 具有基本上由(111)面形成的具有规定的取向波动的这样的前刀面(5)的刀具具有优异的耐磨性并且耐裂纹损伤。

    Bonding tool having diamond head and method of manufacturing the same
    4.
    发明授权
    Bonding tool having diamond head and method of manufacturing the same 失效
    具有金刚石头的接合工具及其制造方法

    公开(公告)号:US5370299A

    公开(公告)日:1994-12-06

    申请号:US41545

    申请日:1993-04-02

    摘要: A bonding tool has a head portion made essentially of vapor-deposited diamond, wherein a principal diamond crystal plane forming a head face is a (111) plane. Such a head face has high hardness and a good wear resistance. In order to improve the toughness of a bonding head which is mainly made of vapor-deposited diamond, a portion or ply forming the head face consists essentially of high-purity diamond, and another portion or ply supporting the head face consists essentially of low-purity diamond. The head face has a high rigidity, while the portion supporting the head face has a high toughness. In order to provide a bonding head portion which is mainly made of vapor-deposited diamond with electrical conductivity, a first portion or ply forming a head face consists essentially of polycrystalline diamond containing a relatively small amount of dopant, and another portion or ply supporting the first portion or ply contains a large amount of dopant. The head portion having electrical conductivity can be heated by energization. In a tool employing a coating containing vapor-deposited diamond as a bonding head portion, the coating is formed by a compound of a metal or ceramics and vapor-deposited diamond, in order to improve the strength of the coating and adhesion to a tool substrate.

    摘要翻译: 接合工具具有基本上由气相沉积金刚石制成的头部,其中形成头部面的主要金刚石晶体平面是(111)面。 这种头面具有高硬度和良好的耐磨性。 为了提高主要由气相沉积金刚石制成的接合头的韧性,形成头部面的部分或层基本上由高纯度的金刚石组成,并且支撑头部面的另一部分或层基本上由低熔点金刚石构成, 纯度钻石。 头部表面具有高刚性,而支撑头部面的部分具有高韧性。 为了提供主要由具有导电性的气相沉积金刚石制成的接合头部分,形成头部面的第一部分或第一部分基本上由含有相对少量掺杂剂的多晶金刚石组成,另一部分或层叠支撑 第一部分或第二部分含有大量的掺杂剂。 可以通过通电来加热具有导电性的头部。 在使用包含气相沉积金刚石作为粘合头部分的涂层的工具中,涂层由金属或陶瓷和气相沉积金刚石的化合物形成,以便提高涂层的强度和对工具基材的粘附 。

    Bonding tool having a diamond head and method of manufacturing the same
    5.
    发明授权
    Bonding tool having a diamond head and method of manufacturing the same 失效
    具有金刚石头的接合工具及其制造方法

    公开(公告)号:US5516027A

    公开(公告)日:1996-05-14

    申请号:US309842

    申请日:1994-09-20

    摘要: A bonding tool has a head portion made essentially of vapor-deposited diamond, wherein a principal diamond crystal plane forming a head face is a (111) plane. Such a head face has high hardness and a good wear resistance. In order to improve the toughness of a bonding head which is mainly made of vapor-deposited diamond, a portion or ply forming the head face consists essentially of high-purity diamond, and another portion or ply supporting the head face consists essentially of low-purity diamond. The head face has a high rigidity, while the portion supporting the head face has a high toughness. In order to provide a bonding head portion which is mainly made of vapor-deposited diamond with electrical conductivity, a first portion or ply forming a head face consists essentially of polycrystalline diamond containing a relatively small amount of dopant, and another portion or ply supporting the first portion or ply contains a large amount of dopant. The head portion having electrical conductivity can be heated by energization. In a tool employing a coating containing vapor-deposited diamond as a bonding head portion, the coating is formed by a compound of a metal or ceramics and vapor-deposited diamond, in order to improve the strength of the coating and adhesion to a tool substrate.

    摘要翻译: 接合工具具有基本上由气相沉积金刚石制成的头部,其中形成头部面的主要金刚石晶体平面是(111)面。 这种头面具有高硬度和良好的耐磨性。 为了提高主要由气相沉积金刚石制成的接合头的韧性,形成头部面的部分或层基本上由高纯度的金刚石组成,并且支撑头部面的另一部分或层基本上由低熔点金刚石构成, 纯度钻石。 头部表面具有高刚性,而支撑头部面的部分具有高韧性。 为了提供主要由具有导电性的气相沉积金刚石制成的接合头部分,形成头部面的第一部分或第一部分基本上由含有相对少量掺杂剂的多晶金刚石组成,另一部分或层叠支撑 第一部分或第二部分含有大量的掺杂剂。 可以通过通电来加热具有导电性的头部。 在使用包含气相沉积金刚石作为粘合头部分的涂层的工具中,涂层由金属或陶瓷和气相沉积金刚石的化合物形成,以便提高涂层的强度和对工具基材的粘附 。

    Cutting tool employing vapor-deposited polycrystalline diamond for
cutting edge and method of manufacturing the same
    6.
    发明授权
    Cutting tool employing vapor-deposited polycrystalline diamond for cutting edge and method of manufacturing the same 失效
    使用气相沉积多晶金刚石切割刃的切割工具及其制造方法

    公开(公告)号:US5435815A

    公开(公告)日:1995-07-25

    申请号:US84298

    申请日:1993-06-29

    摘要: A diamond cutting tool has a tool substrate and a cutting edge member. The cutting edge member is formed of a material having a three-layer structure or a diamond composite material. When the material having a three-layer structure is employed, the cutting edge member is formed by a vapor-deposited diamond layer defining a rake face, a layer of a composite material of vapor-deposited diamond and a metal or ceramics, and a layer of the metal or ceramics. The metal is prepared from Mo, W, Cr, V, Nb, Ta, Co, Ni or Fe, while the ceramics is prepared from cBN, SiC, Si.sub.3 N.sub.4, WC, TiC, TaC, NbC, Cr.sub.3 C.sub.2, Mo.sub.2 C, VC, TiN or BN. The cutting edge member is brazed to the tool substrate through the metal or ceramics layer. When the diamond composite material is employed, on the other hand, the cutting edge member is formed of a composite material of particles or fibers of AlN, cBN or SiC and vapor-deposited diamond. The diamond cutting tool is excellent in heat resistance and durability.

    摘要翻译: 金刚石切削工具具有工具基板和切削刃部件。 切削刃部件由具有三层结构的材料或金刚石复合材料形成。 当采用具有三层结构的材料时,切割边缘部件由形成前刀面的气相沉积金刚石层,气相沉积金刚石和金属或陶瓷的复合材料层以及层 的金属或陶瓷。 该金属由Mo,W,Cr,V,Nb,Ta,Co,Ni或Fe制成,而陶瓷由cBN,SiC,Si3N4,WC,TiC,TaC,NbC,Cr3C2,Mo2C,VC,TiN 或BN。 切削刃部件通过金属或陶瓷层钎焊到工具基板上。 另一方面,当使用金刚石复合材料时,切削刃部件由AlN,cBN或SiC的颗粒或纤维的复合材料和气相沉积金刚石形成。 金刚石切割工具耐热性和耐久性优异。

    Process for producing fine polyphenylene sulfide resin particles, fine polyphenylene sulfide resin particles, and dispersion thereof
    8.
    发明授权
    Process for producing fine polyphenylene sulfide resin particles, fine polyphenylene sulfide resin particles, and dispersion thereof 有权
    微聚苯硫醚树脂颗粒的制造方法,聚苯硫醚树脂微粒及其分散体

    公开(公告)号:US08563681B2

    公开(公告)日:2013-10-22

    申请号:US12933635

    申请日:2009-03-23

    IPC分类号: C08G64/00 C08G63/02

    摘要: This invention provides a process for producing fine PPS resin particles and dispersion thereof by industrially applicable simple operation. This invention further provides very fine PPS resin particles, and furthermore provides fine PPS resin particles uniform in particle size. This invention is a process for producing fine polyphenylene sulfide resin particles comprising the following steps (a) and (b); (a) a step of heating a polyphenylene sulfide resin in an organic solvent, for obtaining a solution with the polyphenylene sulfide resin dissolved therein (dissolution step) (b) a step of flushing-cooling the aforementioned solution, for precipitating the fine particles of the polyphenylene sulfide resin (precipitation step).

    摘要翻译: 本发明提供通过工业上简单的操作制造PPS树脂微粒及其分散体的方法。 本发明还提供非常细的PPS树脂颗粒,并且还提供粒度均匀的PPS树脂颗粒。 本发明是一种生产精细聚苯硫醚树脂颗粒的方法,包括以下步骤(a)和(b)。 (a)在有机溶剂中加热聚苯硫醚树脂以获得溶解有聚苯硫醚树脂的溶液的步骤(溶解步骤)(b)将上述溶液冲洗冷却的步骤,使 聚苯硫醚树脂(沉淀步骤)。

    PROCESS FOR PRODUCTION OF POLYAMIDEIMIDE RESIN MICROPARTICLES, AND POLYAMIDEIMIDE RESIN MICROPARTICLES
    9.
    发明申请
    PROCESS FOR PRODUCTION OF POLYAMIDEIMIDE RESIN MICROPARTICLES, AND POLYAMIDEIMIDE RESIN MICROPARTICLES 有权
    聚酰胺树脂微生物生产工艺和聚酰胺树脂微生物

    公开(公告)号:US20120237771A1

    公开(公告)日:2012-09-20

    申请号:US13508200

    申请日:2010-10-06

    IPC分类号: C08G73/14

    摘要: A process for producing fine particles of polyamide-imide resin includes a dissolution step and a precipitation step wherein the dissolution step is selected from steps (a1) and (b1); (a1) polyamide-imide resin is dissolved in an organic solvent to prepare a polyamide-imide resin solution A1 having a polyamide-imide resin content of less than 5 mass %; and (b1) polyamide-imide resin is dissolved in an organic solvent to prepare a polyamide-imide resin solution B1 having a polyamide-imide resin content of less than 10 mass %, and the precipitation step is selected from (a2) the polyamide-imide resin solution A1 is added to a solvent that is virtually free from surface active agents and able to precipitate fine particles of the polyamide-imide resin to cause precipitation of fine particles of the polyamide-imide resin, and (b2) the polyamide-imide resin solution B1 is subjected to flash crystallization to cause precipitation of fine particles of the polyamide-imide resin.

    摘要翻译: 制备聚酰胺酰亚胺树脂微粒的方法包括溶解步骤和沉淀步骤,其中溶解步骤选自步骤(a1)和(b1); (a1)聚酰胺酰亚胺树脂溶解在有机溶剂中,制备聚酰胺 - 酰亚胺树脂含量小于5质量%的聚酰胺 - 酰亚胺树脂溶液A1; 和(b1)聚酰胺酰亚胺树脂溶解在有机溶剂中,制备聚酰胺 - 酰亚胺树脂含量小于10质量%的聚酰胺 - 酰亚胺树脂溶液B1,沉淀步骤选自(a2)聚酰胺 - 将酰亚胺树脂溶液A1加入到基本上不含表面活性剂的溶剂中,并能够使聚酰胺 - 酰亚胺树脂的细颗粒沉淀,使聚酰胺 - 酰亚胺树脂的细颗粒沉淀,和(b2)聚酰胺 - 酰亚胺 树脂溶液B1进行闪光结晶,使聚酰胺 - 酰亚胺树脂的微粒析出。