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    Conjugated diene block polymer and process for preparing the same
    12.
    发明授权
    Conjugated diene block polymer and process for preparing the same 失效
    共轭二烯嵌段聚合物及其制备方法

    公开(公告)号：US4436873A

    公开(公告)日：1984-03-13

    申请号：US477583

    申请日：1983-03-21

    Applicant: Hiroshi Furukawa ,  Yuichi Saito ,  Akio Imai ,  Keisaku Yamamoto ,  Hiroyoshi Takao ,  Nobuyuki Yoshida

    Inventor： Hiroshi Furukawa ,  Yuichi Saito ,  Akio Imai ,  Keisaku Yamamoto ,  Hiroyoshi Takao ,  Nobuyuki Yoshida

    IPC: C08F297/00 ,  C08F136/04 ,  C08F297/02

    CPC classification number: C08F297/02 ,  C08F136/04

    Abstract: A conjugated diene block polymer composed of blocks having a different microstructure from each other such that one block contains 20 to 60% by mole of 1,2- and/or 3,4-bonding, the other block contains 50 to 90% by mole of 1,2- and/or 3,4-bonding, the difference in the 1,2- and/or 3,4-bonding content between the both blocks is from 20 to 50% mole and the average content of 1,2- and/or 3,4-bonding in the polymer is from 50 to 85% by mole. The block polymer has a high wet skid resistance and a low dynamic heat generating property, and is very useful as a material for automobile tires.

    Abstract translation: 共轭二烯嵌段聚合物由具有彼此不同微结构的嵌段组成，使得一个嵌段含有20至60摩尔％的1,2-和/或3,4-键，另一个嵌段含有50至90摩尔％ 的1,2-和/或3,4-键，两个嵌段之间的1,2-和/或3,4-键含量的差异为20-50％摩尔，平均含量为1,2 - 和/或3,4-键在聚合物中为50-85摩尔％。 嵌段聚合物具有高的抗湿滑性和低动态发热性，并且作为汽车轮胎的材料是非常有用的。

    Processes for producing 1-benzyl-4-[(5,6-dimethoxy-1indanon)-2-yl]methylpiperidine and hydrochloride thereof
    14.
    发明申请
    Processes for producing 1-benzyl-4-[(5,6-dimethoxy-1indanon)-2-yl]methylpiperidine and hydrochloride thereof 有权
    1-苄基-4 - [（5,6-二甲氧基-1茚满酮）-2-基]甲基哌啶及其盐酸盐的制备方法

    公开(公告)号：US20070117846A1

    公开(公告)日：2007-05-24

    申请号：US10580908

    申请日：2005-04-27

    Applicant: Akio Imai ,  Hiroshi Nishimura

    Inventor： Akio Imai ,  Hiroshi Nishimura

    IPC: C07D211/06 ,  A61K31/445

    CPC classification number: C07D211/32 ,  B01J25/02

    Abstract: Processes for preparing 1-benzyl-4-[(5,6-dimethoxy-lindanon)-2-yl]methylpiperidine (donepezil), which is useful as an intermediate for medicines, and for producing 1-benzyl-4-[(5,6-dimethoxy-1-indanon)-2-yl]methylpiperidine hydrochloride (donepezil hydrochloride), which is useful as a medicine. The process for donepezil hydrochloride production comprises catalytically hydrogenating the compound represented by the structural formula (III) [1-benzyl-4-[(5,6-dimethoxy-lindanon)-2-ylidene]methylpiperidine] with a Raney nickel catalyst under mild conditions and subsequently treating it with hydrochloric acid. Thus, impurities are further diminished. The operations are simple and the process is suitable for industrial production.

    Abstract translation: 用于制备1-苄基-4 - [（5,6-二甲氧基 - 茚满酮）-2-基]甲基哌啶（多奈哌齐）的方法，其可用作药物的中间体，并用于制备1-苄基-4 - [（5 ，6-二甲氧基-1-茚满酮）-2-基]甲基哌啶盐酸盐（盐酸多奈哌齐），其可用作药物。 盐酸多奈哌齐的方法包括用温和的阮内镍催化剂催化氢化由结构式（III）[1-苄基-4 - [（5,6-二甲氧基 - 茚满酮）-2-亚基]甲基哌啶]代表的化合物 然后用盐酸处理。 因此，杂质进一步减少。 操作简单，适用于工业生产。

    Alpha-olefin polymerization catalyst and process for producing alpha-olefin polymer
    15.
    发明申请
    Alpha-olefin polymerization catalyst and process for producing alpha-olefin polymer 审中-公开
    α-烯烃聚合催化剂和α-烯烃聚合物的制备方法

    公开(公告)号：US20050059542A1

    公开(公告)日：2005-03-17

    申请号：US10975814

    申请日：2004-10-29

    Applicant: Makoto Satoh ,  Yasuki Fujiwara ,  Akio Imai

    Inventor： Makoto Satoh ,  Yasuki Fujiwara ,  Akio Imai

    IPC: C08F4/658 ,  C08F4/60 ,  C08F4/642 ,  C08F10/00 ,  B01J31/00 ,  C08F4/44

    CPC classification number: C08F10/00 ,  C08F4/6565

    Abstract: An α-olefin polymerization catalyst comprising (A) a solid catalyst component containing a titanium compound obtained by treating a solid product having a titanium content of 1.5% by weight or less obtained by reducing Ti(OR1)aX4-a (R1 represents a hydrocarbon group having 1 to 20 carbon atoms, X represents a halogen atom and a represents a number satisfying 0

    Abstract translation: 一种α-烯烃聚合催化剂，其包含（A）含有钛化合物的固体催化剂组分，所述钛化合物通过将通过还原Ti（OR 1）aX 4-a（R 2）获得的钛含量为1.5重量％以下的固体产物 在具有Si-O键的有机硅化合物的存在下，使用有机镁化合物与式（1）表示碳原子数1〜20的烃基，X表示卤素原子，a表示满足0

    Catalyst for &agr;-olefin polymerization and process for producing &agr;-olefin polymer
    16.
    发明授权
    Catalyst for &agr;-olefin polymerization and process for producing &agr;-olefin polymer 有权
    用于α-烯烃聚合的催化剂和用于生产α-烯烃聚合物的方法

    公开(公告)号：US06331501B1

    公开(公告)日：2001-12-18

    申请号：US09250286

    申请日：1999-02-16

    Applicant: Makoto Satoh ,  Yasuki Fujiwara ,  Akio Imai

    Inventor： Makoto Satoh ,  Yasuki Fujiwara ,  Akio Imai

    IPC: B01J3100

    CPC classification number: C08F10/00 ,  C08F4/651 ,  C08F4/6565

    Abstract: A catalyst for &agr;-olefin polymerization obtained by contacting (A) a solid catalyst component containing a titanium compound which is obtained by treating a solid product obtained by contacting an organosilicon compound having an Si—O bond, an ester compound and an organomagnesium compound, with an ether compound, titanium tetrachloride and an acyl halide, and successively treating said treated solid with an mixture of an ether compound and titanium tetrachloride, or a mixture of an ether compound, titanium tetrachloride and an ester compound, (B) an organoaluminum compound and (C) an electron-donative compound, and a process for producing an &agr;-olefin polymer with the catalyst.

    Abstract translation: 通过使（A）含有钛化合物的固体催化剂成分与通过使通过使具有Si-O键的有机硅化合物接触而得到的固体产物，酯化合物和有机镁化合物接触而获得的α-烯烃聚合反应， 与醚化合物，四氯化钛和酰基卤反应，并用醚化合物和四氯化钛的混合物或醚化合物，四氯化钛和酯化合物的混合物连续处理所述处理的固体，（B）有机铝化合物 和（C）电子给体化合物，以及使用该催化剂生产α-烯烃聚合物的方法。

    Transition metal complex, catalyst for olefin polymerization, and process for producing olefin polymers
    18.
    发明授权
    Transition metal complex, catalyst for olefin polymerization, and process for producing olefin polymers 失效
    过渡金属络合物，用于烯烃聚合的催化剂，以及用于生产烯烃聚合物的方法

    公开(公告)号：US6066704A

    公开(公告)日：2000-05-23

    申请号：US29887

    申请日：1998-06-26

    Applicant: Hiroaki Katayama ,  Akio Imai ,  Hidenori Hanaoka ,  Norio Kawamura ,  Akira Miyashita

    Inventor： Hiroaki Katayama ,  Akio Imai ,  Hidenori Hanaoka ,  Norio Kawamura ,  Akira Miyashita

    IPC: C07F9/53 ,  C07F17/00 ,  C08F4/642 ,  C08F4/646 ,  C08F4/659 ,  C08F4/6592 ,  C08F10/00 ,  C08F210/16 ,  C08F4/44 ,  B01J31/00 ,  B01J37/00 ,  C07F7/00 ,  C07F7/28

    CPC classification number: C07F17/00 ,  C07F9/532 ,  C08F10/00 ,  C08F210/16 ,  C08F4/65908 ,  C08F4/65912 ,  C08F4/6592 ,  Y10S526/943

    Abstract: A transition metal complex represented by the formula [1] ##STR1## wherein M is a transition metal atom of the group 4 of the periodic table of elements; Cp is a group having a cyclopentadiene type anionic skeleton; A and G are each a divalent residue containing an atom of the group 15 or 16 of the periodic table of elements and may be the same with or different from each other; X.sup.1, X.sup.2, R.sup.1, R.sup.2, R.sup.3 and R.sup.4 are each independently a hydrogen atom, halogen atom, alkyl group with the number of carbon atoms of 1-20 optionally substituted with at least one halogen atom, aralkyl group with the number of carbon atoms of 7-20 optionally substituted with at least one halogen atom, aryl group with the number of carbon atoms of 6-20 optionally substituted with at least one halogen atom, substituted silyl group with the number of carbon atoms of 1-20 optionally substituted with at least one halogen atom, alkoxy group with the number of carbon atoms of 1-20 optionally substituted with at least one halogen atom, aralkyloxy group with the number of carbon atoms of 7-20 optionally substituted with at least one halogen atom, aryloxy group with the number of carbon atoms of 6-20 optionally substituted with at least one halogen atom or a di-substituted amino group with the number of carbon atoms of 2-20, provided that R.sup.1, R.sup.2, R.sup.3 and R.sup.4 may optionally combine with each other to form a ring; L is a Lewis base and w is an integer of 0-2, an olefin polymerization catalyst and a process for producing olefin polymers which uses the catalyst.

    Abstract translation: PCT No.PCT / JP96 / 02439 Sec。 371日期：1998年6月26日 102（e）日期1998年6月26日PCT 1996年8月30日PCT PCT。 公开号WO97 / 08179 日期：1997年3月6日由式[1]表示的过渡金属络合物，其中M是元素周期表第4族的过渡金属原子; Cp是具有环戊二烯型阴离子骨架的基团; A和G各自是含有元素周期表第15或16族的原子的二价残基，并且可以彼此相同或不同; X1，X2，R1，R2，R3和R4各自独立地为氢原子，卤素原子，任选被至少一个卤素原子取代的碳原子数为1-20的烷基，具有碳原子数的芳烷基 任选被至少一个卤素原子取代的，任选被至少一个卤素原子取代的碳原子数为6-20的芳基，任选被至少一个卤素原子取代的碳原子数为1-20的取代甲硅烷基，任选被 至少一个卤素原子，任选被至少一个卤素原子取代的碳原子数为1-20的烷氧基，任选被至少一个卤素原子取代的碳原子数为7-20的芳烷氧基，芳氧基 碳原子数为6-20个，任选被至少一个卤素原子取代或碳原子数为2-20的二取代氨基，条件是R1，R2，R3和R4可以任选地与每个 其他形式 戒指; L是路易斯碱，w是0-2的整数，烯烃聚合催化剂和使用该催化剂的烯烃聚合物的制造方法。

    .alpha.-olefin polymerization catalyst system and process for producing .alpha.-olefin catalyst
    20.
    发明授权
    .alpha.-olefin polymerization catalyst system and process for producing .alpha.-olefin catalyst 失效
    α-烯烃聚合催化剂体系和α-烯烃催化剂生产方法

    公开(公告)号：US5608018A

    公开(公告)日：1997-03-04

    申请号：US350158

    申请日：1994-11-30

    Applicant: Takeshi Ebara ,  Teruyosi Kiyota ,  Akio Imai

    Inventor： Takeshi Ebara ,  Teruyosi Kiyota ,  Akio Imai

    IPC: C08F4/654 ,  C08F4/656 ,  C08F10/00 ,  C08F4/651

    CPC classification number: C08F10/00

    Abstract: An .alpha.-olefin polymerization catalyst system having so high a catalytic activity and stereoregularity that the catalyst residue and amorphous polymer need not be removed and a process for producing an.alpha.-olefin polymer using the catalyst system, said catalyst system consisting essentially of:(A) a trivalent titanium compound-containing solid catalyst component prepared by reducing a titanium compound, represented by the general formula Ti(OR.sup.1).sub.a X.sub.4-a in which R.sup.1 represents a hydrocarbon group having 1 to 20 carbon atoms; X represents a halogen atom; and a represents a numeral satisfying 0

    Abstract translation: 具有如此高的催化活性和立构规整性的催化剂残余物和无定形聚合物不需要除去的α-烯烃聚合催化剂体系和使用该催化剂体系生产α-烯烃聚合物的方法，所述催化剂体系基本上由以下组成：（A ）通过还原由通式Ti（OR 1）a X 4-a表示的钛化合物制备的含三价钛化合物的固体催化剂组分，其中R 1表示具有1至20个碳原子的烃基; X表示卤原子; 和a表示满足0

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