Method for the preparation of polyesters of 1,4-butane diol
    11.
    发明授权
    Method for the preparation of polyesters of 1,4-butane diol 失效
    1,4-丁二醇聚酯的制备方法

    公开(公告)号:US3859257A

    公开(公告)日:1975-01-07

    申请号:US17065471

    申请日:1971-08-10

    CPC classification number: C08G63/181 C08G63/78

    Abstract: Improvements in the production of polyesters of dicarboxylic acid moieties and 1,4-butanediol moieties, where at least some of the acid moieties are aromatic, by catalytic direct or transesterification of the acids or esters thereof with a molar excess of 1,4- butanediol, whereby reducing the amount of excess 1,4-butanediol required to produce commercially acceptible polyesters, which comprises reacting the 1,4-butanediol with the dicarboxylic acid or an ester thereof in a mole ratio of 1.05 to 1.25:1 respectively at temperatures of less than 200*C while distilling off the volatile cleavage products including the 1,4butanediol until the flow of butanediol has been reduced to less than about 10 percent of its initial removal rate, and then polycondensing this product at temperatures above 200*C in the usual manner.

    Warhead
    12.
    发明授权
    Warhead 失效
    弹头

    公开(公告)号:US3857338A

    公开(公告)日:1974-12-31

    申请号:US30022672

    申请日:1972-10-24

    Inventor: BUCKLISCH L

    CPC classification number: F42B12/58

    Abstract: Warhead for bombs, projectiles, rockets and the like having a casing with several projectiles accommodated therein. The projectiles are disposed in launcher tubes which are connected with each other by a common central connecting component to form an independent unit in a symmetrical arrangement with respect to the axis of the component. The independent unit is equipped with a descent-retarding device on one side thereof positioned toward one direction of the axis, while the other side is provided with a stabilizing device toward the other direction of the axis to vertically position the axis during descent. Preferred embodiments use parachutes as descent-retarding devices and rigid stabilizer rods or flexible members to interconnect a stabilizing weight with the respective independent units. Accommodations are made to telescope the stabilizer rods into one another to limit the total space utilized in the stored position. In the embodiments utilizing flexible members, the weights are provided with a recess at the undersides thereof to accommodate the next adjacent parachute and independent unit when in the stored position in the warhead.

    Abstract translation: 弹头,弹头,火箭等具有容纳在其中的几个射弹的壳体。 抛射体设置在通过公共中心连接部件彼此连接的发射管中,以形成相对于部件的轴线对称布置的独立单元。 独立单元在其一侧沿轴线的一个方向配备有下降延迟装置,而另一侧在轴向的另一方向上设置有稳定装置,以在下降期间垂直定位轴。 优选实施例使用降落伞作为下降阻滞装置和刚性稳定杆或柔性构件将稳定重量与相应的独立单元相互连接。 住房将稳定杆望远镜放在一起,以限制在存储位置中使用的总空间。 在利用柔性构件的实施例中,重物在其下侧设置有凹部,以在处于弹头中的存储位置时容纳下一个相邻的降落伞和独立单元。

    Porous silicic acid and its production
    13.
    发明授权
    Porous silicic acid and its production 失效
    多孔硅酸及其生产

    公开(公告)号:US3850971A

    公开(公告)日:1974-11-26

    申请号:US9824470

    申请日:1970-12-15

    Inventor: BLEH O TERMIN E LENZ A

    CPC classification number: C01B33/163

    Abstract: 1. PROCESS FOR MAKING POROUS SILIC ACID GEL WHICH COMPRISES CONTACTING METHYL OR ETHYL SILICATE, OR POLYMETHYL OR POLYETHYL SILICATE IN THE PRESENCE OF A HYDROLYSIS ACTIVATING SUBSTANCE, WITH ABOUT 70 TO 120% OF THE STOICHIOMETRIC AMOUNT OF WATER WITH STIRRING UNDER CONDITIONS TO ACHIEVE HOMOGENEITY TO EFFECT HYDROLYSIS AND PRODUCE SOLID SILICIC ACID HAVING A SPECIFIC SURFACE OF ABOUT 50 TO 1000 M.2/G., SEPARATING THE SOLID SILICK ACID FROM THE LIQUID AND DRYING THE RESULTING POROUS SILICIC ACID.

    Polyamide shock absorber piston from terephthalic acid and branched diamine
    14.
    发明授权
    Polyamide shock absorber piston from terephthalic acid and branched diamine 失效
    来自三聚氰胺和分散二胺的聚酰亚胺防震活塞

    公开(公告)号:US3846379A

    公开(公告)日:1974-11-05

    申请号:US16012071

    申请日:1971-07-06

    Inventor: SCHNEIDER J PUNGS W

    CPC classification number: F16F9/3214 C08G69/26 F16F2224/00 F16F2228/00

    Abstract: A shock absorber piston especially suitable for use in automobiles and like vehicles wherein the piston is in contact with a damping fluid and is subject to repeated stresses under varying degrees of pressure and temperature; the piston is made of an amorphous polyamide characterized by a viscosity of about 100 to 200 in a 0.5 percent by weight solution in m-cresol at 25*C.

    Abstract translation: 特别适合用于汽车和类似车辆的减震器活塞,其中活塞与阻尼流体接触并且在不同程度的压力和温度下经受重复的应力; 活塞由无定形聚酰胺制成,其特征在于在25℃的间甲酚中的0.5重量%溶液中粘度为约100至200。

    Process for the manufacture of lowdensity nitrocellulose granules
    17.
    发明授权
    Process for the manufacture of lowdensity nitrocellulose granules 失效
    低密度纳米纤维素颗粒的制造工艺

    公开(公告)号:US3824108A

    公开(公告)日:1974-07-16

    申请号:US82353569

    申请日:1969-05-05

    CPC classification number: C09D101/18 C06B21/0066 C08B5/04

    Abstract: PROCESS OF PREPARING NITROCELLULOSE GRANULES HAVING A BULK DENSITY OF BETWEEN 0.4 AND 0.6 G./CM3 FROM A NITROCELLULOSE LACQUER PREPARED BY STIRRING UNDER WATER NITROCELLULOSE STABILIZERS AND A NITROCELLULOSE SOLVENT INSOLUBLE IN THE WATER, ADDING TO THE LACQUER STILL BEING STIRRED A PROTECTIVE COLLOID AND A WATER-SOLUBLE ALKALI METAL OR ALKALINE EARTH METAL SALT, THEREAFTER REDUCING THE STIRRING SPEED WHEREUPON THE LACQUER BREAKS UP INTO DROP-LIKE PARTICLES, FURTHER REDUCING THE STIRRING SPEED AS TO CAUSE THE PARTICLES, OF LACQUER TO FLOW TOGETHER AGAIN,MAKING A SECOND ADDITION OF PROTECTIVE COLLOID AND SALT, THEN INCREASING THE STIRRING SPEED CAUSING THE LACQUER TO BREAK UP AND FORM THE DESIRED PARTICLES AND THEREAFTER DISTILLING OFF THE SOLVENT.

    Process for the preparation of pure sodium benzoate
    18.
    发明授权
    Process for the preparation of pure sodium benzoate 失效
    制备纯正辛酸钠的方法

    公开(公告)号:US3821292A

    公开(公告)日:1974-06-28

    申请号:US11660571

    申请日:1971-02-18

    CPC classification number: C07C51/412 C07C63/08

    Abstract: The present disclosure is directed to a process for the preparation of substantially pure sodium benzoate which comprises treating commercial grade methyl benzoate with acidic bleaching clay, of the montmorillonite type fractionally distilling the methyl benzoate to obtain a constant boiling-point, substantially pure fraction of methyl benzoate and saponifying the mixture with sodium hydroxide to obtain substantially pure sodium benzoate.

    Cross-linked shaped objects of vinyl chloride polymers
    19.
    发明授权
    Cross-linked shaped objects of vinyl chloride polymers 失效
    氯乙烯聚合物的交联成型对象

    公开(公告)号:US3821174A

    公开(公告)日:1974-06-28

    申请号:US29412372

    申请日:1972-10-02

    Inventor: BUNING R

    CPC classification number: C08F8/00 D01F6/32 C08F30/04

    Abstract: Cross-linked vinyl chloride polymers are produced by employing as the linear vinyl chloride polymer a copolymer of vinyl chloride and a silane and effecting the cross-linking by contacting the linear polymer with hydrochloric or nitric acid. Premature cross-linking, i.e. cross-linking before final shaping of the desired article such as filament or sheet, can be avoided by use of the process of the invention.

    Apparatus for forming tube end sockets
    20.
    发明授权
    Apparatus for forming tube end sockets 失效
    用于形成管端塞的装置

    公开(公告)号:US3806301A

    公开(公告)日:1974-04-23

    申请号:US12034171

    申请日:1971-03-02

    CPC classification number: B29C57/02 B29D1/00 B29L2023/22 Y10S425/218

    Abstract: A process for forming, at the end of a pipe fabricated from a synthetic resin material, a socket having external ribs, beads, projections, or the like, extending in cross-sectional planes or helically, and apparatus for implementing the novel process, wherein the process contemplates the insertion of a temperaturecontrolled mandrel in the end of an initially-heated pipe, simultaneously imparting a rotary motion to the mandrel as it is axially advanced and, upon cooling of the pipe end, withdrawal of the mandrel with further rotary motion thereof.

    Abstract translation: 在由合成树脂材料制成的管的端部处形成具有在横截面或螺旋状延伸的外部肋,珠,突起等的插座以及用于实现新方法的装置的方法,其中 该方法考虑将温度受控的心轴插入初始加热的管的端部,同时在心轴轴向前进时给心轴提供旋转运动,并且在冷却管端时,心轴以进一步的旋转 其运动。

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