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公开(公告)号：US5763148A
公开(公告)日：1998-06-09
申请号：US682354
申请日：1996-07-17
IPC分类号： G03C5/16 , G03C1/00 , G03C1/035 , G03C1/04 , G03C1/42 , G03C1/76 , G03C1/91 , G03C5/26 , G03C5/29
CPC分类号： G03C1/7614 , G03C1/42 , G03C5/262
摘要： A silver halide photographic activation material is disclosed comprising a film support, on one or both sides thereof at least one gelatino silver halide emulsion layer and between said emulsion layer and said support a hydrophilic undercoat layer comprising as a binder at least 50% of a loaded latex polymer, said latex polymer being loaded with at least one developing agent, further characterised in that water absorption during activation processing is not higher than 2.5 g per gram of binder present in said material.
摘要翻译： 公开了一种卤化银照相活化材料，其包括膜载体，其一侧或两侧上至少有一个明胶卤化银乳剂层，并且在所述乳剂层和所述载体之间，包含作为粘合剂的至少50％的负载的亲水底涂层 胶乳聚合物，所述胶乳聚合物装载有至少一种显影剂，其特征还在于，活化处理期间的吸水性不高于所述材料中每克粘结剂2.5克。
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公开(公告)号：US5660966A
公开(公告)日：1997-08-26
申请号：US680405
申请日：1996-07-15
申请人： Peter Willems , Freddy Henderickx
发明人： Peter Willems , Freddy Henderickx
摘要： A silver halide photographic material for industrial radiography is disclosed comprising a film support and on one or both sides thereof at least one silver halide emulsion layer which is characterized in that each gelatino silver halide emulsion layer comprises as silver halide silver chloride or silver chlorobromide wherein the amount of bromide is not more than 10 mole %; has a gelatin to silver halide (expressed as silver nitrate) ratio from 0.2 to 0.6 and a total amount of silver halide corresponding to from 11 g to 35 g of silver/m.sup.2 and in that the photographic material has been fore-hardened to such an extent that when it is immersed in demineralized water of 25.degree. C. for 3 minutes there is not absorbed more than 3.0 g of water per gram of gelatin, and wherein said material further comprises a dihydroxybenzene compound and a 3-pyrazolidine-1-one compound as developing agents. Moreover a method for developing a radiographically exposed photographic material is disclosed comprising the step of contacting the exposed photographic material with an aqueous alkaline liquid, called activator liquid, being initially substantially free from developing agent(s), having a pH value of at least 10 and containing a primary and/or secondary amine.
摘要翻译： 公开了一种用于工业射线照相术的卤化银照相材料，其包括膜载体，并且其一侧或两侧上至少有一个卤化银乳剂层，其特征在于每个明胶卤化银乳剂层包含卤化银氯化银或氯溴化银，其中 溴的含量不超过10摩尔％; 具有明胶至卤化银（表示为硝酸银）的比例为0.2至0.6，卤化银的总量相当于11g至35g的银/ m2，并且照相材料已经硬化到这种 其程度是当其浸入25℃的软化水中3分钟时，每克明胶不吸收3.0克以上的水，其中所述材料还包含二羟基苯化合物和3-吡唑烷-1-酮 化合物作为显影剂。 此外，公开了一种用于显影放射照相曝光的照相材料的方法，其包括使曝光的照相材料与称为活化剂液体的碱性水溶液接触的步骤，其最初基本上不含显影剂，其pH值至少为10 并含有伯胺和/或仲胺。
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13.发明授权Processing of radiographic materials having emulsion grains rich in silver chloride 失效具有富含氯化银乳剂颗粒的射线照相材料的加工
公开(公告)号：US06066441A
公开(公告)日：2000-05-23
申请号：US303545
申请日：1999-05-03
IPC分类号： G03C5/26 , C03C1/06 , G03C1/005 , G03C1/035 , G03C1/06 , G03C1/09 , G03C1/74 , G03C5/16 , G03C5/30 , G03C5/31
CPC分类号： C03C1/06 , G03C1/06 , G03C1/005 , G03C1/0051 , G03C1/0053 , G03C1/035 , G03C1/09 , G03C2001/03517 , G03C2001/03541 , G03C2001/091 , G03C2001/095 , G03C2001/097 , G03C2005/168 , G03C2005/3007 , G03C2200/01 , G03C2200/03 , G03C5/16 , G03C5/30
摘要： A method is disclosed of processing an exposed black-and-white light-sensitive silver halide photographic material having silver halide, coated in an amount, expressed as an equivalent amount of silver nitrate of less than 6 g/m.sup.2 comprising the steps of developing, fixing, rinsing and drying, making use in the developing step of an ascorbic acid type developer and of an equivalent developer replenisher providing a regeneration amount of less than 150 ml/m.sup.2, characterized in that the said material has a buffering capacity of less than 6 mmole/m.sup.2, wherein said buffering capacity is defined as the amount of alkali, expressed in mmole/square meter, required to bridge across pH differences between the material and the developer.
摘要翻译： 公开了一种处理具有卤化银的暴露的黑白感光卤化银照相材料的方法，其涂布量以等于数量的硝酸银表示，小于6g / m 2，其包括显影， 固定，漂洗和干燥，用于抗坏血酸型显影剂的显影步骤和提供小于150ml / m 2的再生量的等效显影剂补充液，其特征在于所述材料具有小于6的缓冲能力 mmole / m2，其中所述缓冲能力定义为桥接跨材料和显影剂之间的pH差异所需的碱量（以毫摩尔/平方米表示）。
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公开(公告)号：US5998083A
公开(公告)日：1999-12-07
申请号：US028758
申请日：1998-02-24
摘要： An image-forming system for radiological imaging is disclosed said system consisting of an intensifying screen comprising on a support at least one layer of a green-light emitting phosphor and, in operative association therewith, a prehardened light-sensitive photographic silver halide film material, comprising a support and on both sides thereof one or more hydrophilic colloid layers, said layers being hardened to such an extent that their swelling degree is reduced to less than 200% after immersing said material for 2 minutes in demineralised water of 35.degree. C.; further comprising in at least one of said hydrophilic layers chemically ripened, monodisperse essentially cubic silver chloroiodide grains having a mean crystal diameter of from 0.40 mm up to 0.65 mm; wherein said grains have been spectrally sensitised in the wavelength range between 520 and 580 nm, have a maximum absorption between 540 and 500 nm and have been coated in a total amount of silver per sq.m. of from 6 g up to 8 g, wherein said amount is expressed as an equivalent amount of silver nitrate per sq.m.; said image-forming system being characterised in that said silver chloroiodide grains have been doped with a complex ion compound satisfying the formula[ML.sub.6 ].sup.n- (I)whereinM represents a filled frontier orbital polyvalent metal ion;L.sub.6 represents six coordination complex ligands which are independently selected, provided that at least three, more preferred four, of the said ligands are more electronegative than any halide ligand and at least four of the said ligands are anionic ligands; n=1, 2, 3 or 4;and wherein the energetic distance between filled higher occupied (HOMO) and lower unoccupied (LUMO) molecular orbital is more than 27000 cm.sup.-1.
摘要翻译： 公开了一种用于放射成像的图像形成系统，所述系统由增强屏幕组成，所述增强屏幕包括在至少一层绿光发射荧光体的支撑件上，并且与其可操作地相关联的预硬化的感光照相卤化银膜材料， 其包含支撑体，并且在其两侧上具有一个或多个亲水胶体层，所述层被硬化至使其在35℃的软化水中浸渍2分钟后其溶胀度降低至小于200％的程度。 还包括在所述亲水层中的至少一个化学成熟，单分散基本上具有0.40mm至0.65mm的平均晶体直径的立方体氯化银银晶粒; 其中所述晶粒已经在520和580nm之间的波长范围内被光谱增感，在540和500nm之间具有最大吸收，并且已经以每平方米的总量涂覆银。 为6g至8g，其中所述量表示为每平方米当量的硝酸银。 所述成像系统的特征在于所述氯代碘化银颗粒已经掺杂满足式[ML6] n-n（I）的复合离子化合物，其中M表示填充的边界轨道多价金属离子; L6表示独立选择的六个配位络合配体，只要至少三个，更优选的四个所述配体比任何卤化物配体更具有电负性，并且至少四个所述配体是阴离子配体; n = 1,2,3或4; 并且其中填充的较高占据（HOMO）和较低未占据（LUMO）分子轨道之间的能量距离大于27000cm -1。
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15.发明授权
公开(公告)号：US5593817A
公开(公告)日：1997-01-14
申请号：US594144
申请日：1996-01-31
摘要： A photographic developing solution and a method of developing silver halide materials in the said developing solution is disclosed, the said developing solution comprising hydroquinone in an amount from 0 to 30 g per litre, an auxiliary developer, and silver halide complexing agents in an amount from 0 to 50 g per litre, characterized in that said developer further comprisesin amounts from 0.1 to 5 g per litre a compound corresponding to the formula (I), accompanied by charge compensating anions,Z'N.sup.+ --R--N.sup.+ Z" (I)wherein at least divalent group R contains at least one oxyethylene group and wherein Z' and Z", being the same or different, are composed of enough atoms to form a heterocyclic aromatic 5- or 6-ring;andat least 1 g of a compound corresponding to the formula (II), a precursor thereof, a derivative thereof and/or a metal salt thereof ##STR1## wherein each of A, B and D independently represents an oxygen atom or NR.sup.1 ;X represents an oxygen atom, a sulphur atom, NR.sup.2 ; CR.sup.3 R.sup.4 ;C=O; C=NR.sup.5 or C=S;Y represents an oxygen atom, a sulphur atom, NR.sup.'2 ; CR.sup.'3 R.sup.'4 ; C=O, C=NR.sup.'5 or C=S;Z represents an oxygen atom, a sulphur atom, NR.sup."2 ; CR.sup."3 R.sup."4 ; C=O; C=NR.sup."5 or C=S;n equals 0, 1 or 2;each of R.sup.1 to R.sup.5, R.sup.'1 to R.sup.'5 and R.sup."1 to R.sup."5 independently represents hydrogen, alkyl, aralkyl, hydroxyalkyl, carboxyalkyl; alkenyl, alkynyl, cycloalkyl, cycloalkenyl, aryl or heterocyclyl;and whereinR.sup.3 and R.sup.4, R.sup.'3 and R.sup.'4, R.sup."3 and R.sup."4, may further form together a ring; andwherein in the case that X=CR.sup.3 R.sup.4 and Y=CR.sup.'3 R.sup.'4, R.sup.3 and R.sup.'3 and/or R.sup.4 and R.sup.'4 may form a ring and wherein in the case that Y=CR.sup.'3 R.sup.'4 and Z=CR.sup."3 R.sup."4 with n=1 or 2, R.sup.'3 and R.sup."3 and/or R.sup.'4 and R.sup."4 may form a ring.
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公开(公告)号：US5447817A
公开(公告)日：1995-09-05
申请号：US222911
申请日：1994-04-05
CPC分类号： G03C5/3056 , G03C1/30 , G03C5/16 , G03C5/38 , Y10S430/168
摘要： To eliminate the "pi-line" artefact after processing a method of image formation in a silver halide industrial X-ray photographic material is disclosed wherein said material comprises on at least one side of a support, at least one gelatino silver halide emulsion layer and a total amount of silver halide, corresponding to from 6 to 20 g of silver nitrate per square meter and per side, and at least one non-sensitive protective antistress coating and wherein said method proceeds by the steps of exposing said material to direct X-rays and processing the material in an automatic processing machine by development, fixing, rinsing and drying, characterized in that said material further comprises at least one vinyl sulphone compound as a hardening agent in at least one of its hydrophilic layers, that development occurs in a developer comprising as a surfactant at least one anionic alkylphenoxy and/or alkoxy polyalkyleneoxy phosphate ester, sulphate ester, alkyl carboxylic, sulphonic or phosphonic acid and/or a salt thereof and that fixing occurs in a fixer which may comprise at least one alpha-ketocarboxylic acid.
摘要翻译： 公开了在卤化银工业X射线照相材料中处理图像形成方法之后消除“pi线”人造物，其中所述材料在载体的至少一侧包含至少一个明胶卤化银乳剂层和 相当于每平方米和每侧6至20g硝酸银的总量的卤化银和至少一种不敏感的保护性抗静电涂层，其中所述方法通过以下步骤进行：将所述材料暴露于直接X- 通过显影，定影，漂洗和干燥在自动加工机中处理该材料，其特征在于，所述材料还包含至少一种乙烯基砜化合物作为其至少一个亲水层中的硬化剂，所述发展发生在 包含至少一种阴离子烷基苯氧基和/或烷氧基聚亚烷基氧基磷酸酯，硫酸酯，烷基羧酸，磺酸或磷酸的表面活性剂 甲酸和/或其盐，并且固定发生在可以包含至少一种α-酮羧酸的定影剂中。
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17.发明授权Radiographic film material exhibiting increased covering power and “colder” blue-black image tone 失效显示增加覆盖力和“较冷”的蓝黑色图像色调的放射照相胶片材料公开(公告)号：US06346360B1
公开(公告)日：2002-02-12
申请号：US09706835
申请日：2000-11-07
申请人： Ann Verbeeck , Freddy Henderickx
发明人： Ann Verbeeck , Freddy Henderickx
IPC分类号： G03C517
CPC分类号： G03C5/16 , G03C1/0051 , G03C1/12 , G03C1/122 , G03C1/7614 , G03C5/17 , G03C2001/03511 , G03C2001/03535 , G03C2001/7635 , G03C2005/168 , G03C2007/3025 , G03C2200/03 , G03C2200/40 , G21K4/00 , G21K2004/06 , Y10S430/166 , Y10S430/167
摘要： A radiographic film material has been provided, comprising a transparent film support having first and second major surfaces coated, apart from a subbing layer and, optionally, a non-light-sensitive hydrophilic layer thereupon, with at least one light-sensitive silver halide emulsion layer overcoated with a protective antistress layer, said emulsion layer(s) having chemically and spectrally sensitized {111} tabular hexagonal core-shell emulsion grains or crystals in an amount of at least 50% of the total projective grain surface of all grains, said grains being composed of a silver bromide core and a silver bromoiodide shell having an average amount over the whole crystal volume of more than 90 mole % of silver bromide, said grains further having a mean equivalent volume diameter of from 0.3 &mgr;m up to 1.0 &mgr;m and an average grain thickness of less than 0.30 &mgr;m, wherein said film material is coated with a total amount of silver, expressed as an equivalent amount of silver nitrate of less than 7 g/m2, characterized in that all silver iodide is present in an outermost shell corresponding with at most 20% of all silver halide precipitated in order to provide silver iodide to be present in the whole grain volume of said tabular grains in an average amount of less than 1 mole % of iodide, based on silver and in that said protective antistress layer, said non-light-sensitive hydrophilic layer or both said protective antistress layer and said non-light-sensitive hydrophilic layer comprise a mercapto-tetrazole compound as in general formula (I), presented in the claims and in the detailed description, said compound being present in high amounts of at least 0.5 mmole per mole of silver halide coated.
摘要翻译： 已经提供了一种放射照相胶片材料，其包括透明膜支撑体，其具有第一和第二主表面，除了底层和任选的非光敏亲水层之外，还包括至少一种感光卤化银乳剂 所述乳剂层具有化学和光谱增感的{111}平板状六角形核 - 壳乳剂颗粒或晶体，其量为所有颗粒的总投射颗粒表面的至少50％，所述颗粒表面 颗粒由溴化银核和银溴碘化银壳组成，其平均量超过90％以上溴化银的整体结晶体积，所述颗粒的平均当量体积直径为0.3μm至1.0μm， 平均颗粒厚度小于0.30μm，其中所述薄膜材料涂覆有总量的银，其表示为当量的硝酸银 其特征在于，所有碘化银存在于最外壳中，对应于所有卤化银沉淀的至多20％，以便提供碘化银存在于所述片状颗粒的整个颗粒体积中 平均量小于1摩尔％的碘化物，基于银，并且在所述保护性抗静电层中，所述非感光亲水层或所述保护性抗过敏层和所述非感光亲水层均包含巯基四唑 所述化合物如权利要求书和详细描述中所述的通式（I）所示的化合物，所述化合物以每摩尔涂覆的卤化银至少0.5毫摩尔的量存在。
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18.发明授权Silver halide photographic material exhibiting increased covering power and “colder” blue-black image tone 失效卤化银照相材料表现出增加的覆盖力和“较冷”的蓝黑色图像色调公开(公告)号：US06342338B1
公开(公告)日：2002-01-29
申请号：US09710838
申请日：2000-11-14
IPC分类号： G03C135
CPC分类号： G03C1/7614 , G03C1/0051 , G03C1/122 , G03C5/17 , G03C2001/0055 , G03C2200/03 , Y10S430/166 , Y10S430/167 , Y10S430/168
摘要： A black-and-white silver halide photographic film material, particularly suitable for use in radiography, has been disclosed, said material comprising a transparent film support having first and second major surfaces coated with a subbing layer, further coated adjacent thereto on one side (for a single-side coated material) or on both sides (for a duplitized material) of said film support and overcoated with a protective antistress layer, a light-sensitive silver halide emulsion layer having chemically and spectrally sensitized {111} tabular hexagonal grains, accounting for at least 50% of the total projective surface of all grains, wherein said film material is coated with a low amount of silver and wherein said protective antistress layer(s)and/or another hydrophilic non-light-sensitive layer comprise(s) a compound according to general formula (I) in an amount of at least 0.5 mmole per mole of coated silver halide, as claimed. A radiographic screen/film combination has also been disclosed, said combination comprising a duplitized film as described herein sandwiched between a pair of supported or self-supporting X-ray intensifying screens emitting radiation in the wavelength range for which said material has been made spectrally sensitive in order to obtain a black-and-white image after exposure of said screen/film combination, followed by processing of the film material.
摘要翻译： 已经公开了特别适合用于放射照相术的黑白卤化银照相胶片材料，所述材料包括透明膜支撑体，所述透明膜支撑体具有涂覆有底层的第一和第二主表面，其一侧进一步涂覆在其上 对于单面涂层材料）或在所述膜支撑体的两侧（用于双面照射材料）并用保护性抗阻层覆盖，具有化学和光谱增感{111}片状六边形晶粒的感光卤化银乳剂层， 占所有颗粒的总投影表面的至少50％，其中所述膜材料涂覆有少量的银，并且其中所述保护抗静电层和/或另一亲水性非感光层包含（s ）根据通式（I）的化合物，其量为每摩尔涂覆的卤化银至少为0.5毫摩尔，如所要求保护的.A射线照相屏/膜组合也已经被 所述组合包括如本文所述的双面胶片夹在一对支撑的或自支撑的X射线增强屏幕之间，所述X射线增强屏幕在所述材料已被制成光谱敏感的波长范围内发射辐射，以获得黑 - 所述屏幕/胶片组合曝光后的白色图像，随后加工薄膜材料。
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公开(公告)号：US6048096A
公开(公告)日：2000-04-11
申请号：US28451
申请日：1998-02-24
IPC分类号： G03C1/005 , G03C1/035 , G03C1/09 , G03C1/18 , G03C1/29 , G03C1/30 , G03C5/17 , G03C5/30 , G03B42/04
CPC分类号： G03C5/17 , G03C1/0053 , G03C1/035 , G03C1/09 , G03C1/30 , G03C1/18 , G03C1/29 , G03C2001/0055 , G03C2001/03517 , G03C2001/03541 , G03C2001/03558 , G03C2001/03594 , G03C2001/095 , G03C2001/097 , G03C2005/3007 , G03C2200/03 , G03C5/30 , Y10S430/167
摘要： An image-forming system for radiological imaging is described consisting of an intensifying screen comprising on a support at least one layer of a green-light emitting phosphor and, in operative association therewith, a prehardened light-sensitive photographic silver halide film material, comprising a support and on both sides thereof one or more hydrophilic colloid layers having monodisperse cubic silver chloroiodide grains with a mean crystal diameter of from 0.40 .mu.m up to 0.65 .mu.m or {111} tabular silver chloroiodide grains having an aspect ratio of from 5 to 20 and a tabularity from 20 to 200; wherein said grains have been spectrally sensitized in the green wavelength range and have been coated in a total amount of silver per sq.m. of from 6 g up to 8 g, expressed as an equivalent amount of silver nitrate per sq.m.; wherein in the image-forming system silver chloroiodide grains have been chemically sensitized with one or more selenide compound(s) generating silver selenide.
摘要翻译： 一种用于放射成像的图像形成系统被描述为由增强屏幕组成，该增强屏幕包括在至少一层绿色发光荧光体的支撑体上，并与其有关的预硬化的感光照相卤化银膜材料，包括 并且在其两侧上具有一个或多个具有平均晶体直径为0.40μm至0.65μm的单分散立方体氯化银颗粒或具有纵横比为5至20的{111}片状氯银银颗粒的亲水胶体层 从20到200的表格; 其中所述晶粒已经在绿色波长范围内被光谱增感，并且已经以每平方米的总量涂覆银。 为6g至8g，表示为每平方米当量的硝酸银。 其中在成像系统中，氯化银颗粒已经用一种或多种产生硒化银的硒化物化学增感。
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