Abstract:
A method for forming a dispersion-strengthened material containing nanoparticles that are uniformly dispersed in a matrix phase. The method includes adding nanoparticles and a molten material to a container to form a pool within the container and rotating the container to create a convection vortex in the pool. The convection vortex is sufficient to cause the nanoparticles to be incorporated into the molten material so as to yield a molten composite material, and further causes the molten composite material to be ejected from the container. The molten composite material is then cooled to form a solid composite body comprising a uniform dispersion of the nanoparticles.
Abstract:
A process for repairing a turbine component comprises overlaying a preform of a brazing material onto a surface of the turbine component, wherein the surface comprises a damaged portion; securing the preform of a brazing material to the surface; and heating the turbine component to a temperature effective to form a brazed joint between the brazing material and the turbine component. Also disclosed is a repaired turbine component repaired by the process.
Abstract:
Methods for casting a metallic material to form a component are described. The component can be a superalloy-containing turbine part, for example. The general method includes the step of pouring the metallic material, in molten form, into an investment mold; and then rapidly immersing the entire investment mold into a bath that contains a low-melting liquid coolant metal, so as to achieve substantially uniform, multi-directional heat transfer out of the molten material. The molten material that solidifies to form the component is characterized by a fine-grained, equiaxed grain structure. Related embodiments include the use of two ingots that constitute the superalloy material. One ingot includes the oxygen-reactive elements, and is prepared by a vacuum-melting technique. The other ingot includes the remainder of the elements, and can be prepared by a number of techniques, such as air-melting processes.
Abstract:
A coating suitable for use as protective oxide-forming coatings on Nb-based substrates, and particularly monolithic niobium-based alloys, exposed to high temperatures and oxidative environments. The coating contains aluminum, may further contain silicon, and optionally contains niobium, titanium, hafnium, and/or chromium, which in combination form one or more intermetallic phases that promote the formation of a slow-growing oxide scale. The intermetallic phases may be M(Al,Si)3, M5(Al,Si)3, and/or M3Si5Al2 where M is niobium, titanium, hafnium, and/or chromium.
Abstract:
The present invention provides methods for manufacturing an article having a wetting-resistant surface. The method includes providing a substrate. The method further includes disposing a coating mixture on a surface of the substrate, wherein the coating mixture comprises a braze material and a texture-providing material. The method further includes heating the braze material to bond the texture-providing material to the surface of the substrate to form the article having the wetting-resistant surface.
Abstract:
The present invention provides a friction stir welding apparatus operable for welding one or more metals, metal alloys, or other materials, and a method for friction stir welding. The friction stir welding apparatus includes a pin tool holder, a shoulder having a surface coupled to the pin tool holder, and a pin tool coupled to the pin tool holder, the pin tool at least partially protruding from the surface of the shoulder, wherein the pin tool is made of a consumable pin tool material. The method includes introducing the pin tool into a workpiece; traversing the pin tool along a joint to be welded on the workpiece; and substantially continuously feeding the pin tool into the weld joint as it is traversed along the joint, thereby incorporating at least a portion of the consumable pin tool material into the volume of the joint to be welded.
Abstract:
The present invention provides methods for manufacturing an article having a wetting-resistant surface. The method includes providing a substrate. The method further includes disposing a coating mixture on a surface of the substrate, wherein the coating mixture comprises a braze material and a texture-providing material. The method further includes heating the braze material to bond the texture-providing material to the surface of the substrate to form the article having the wetting-resistant surface.
Abstract:
Niobium silicide articles are described. They include a surface region enriched with at least about 25 atom % germanium, which can enhance the properties of the article. Methods for preparing these articles are described as well. According to one method, an article is formed from a niobium silicide composite material which contains a selected amount of germanium. The article is then heat-treated under conditions sufficient to increase the level of germanium in the surface region to at least about 25 atom %, based on the total composition of the surface region. In another embodiment, a germanium-containing material is applied over a niobium-silicide article, and then diffused into the surface region of the article by way of a heat treatment.
Abstract:
A method for creating a solid state joint is disclosed. The method includes providing an adjoining apparatus that includes a pin tool, a backing plate and a thermal control plate disposed below the backing plate. The method also includes rotating the pin tool and traversing the pin tool relative to a workpiece along a joint to be welded on the workpiece. The method further includes manipulating the temperature of the pin tool and the backing plate in order to control the temperature and rate of change of temperature experienced by the workpiece at a weld affected zone at the joint. The method also includes maintaining a user chosen temperature differential between the weld affected zone and the backing plate via the thermal control plate.
Abstract:
Articles that include a material that has L12-structured gamma-prime phase precipitates within a matrix phase at a concentration of at least 20% by volume are disclosed. The gamma-prime phase precipitates are less than 1 micrometer in size. The material also has A3-structured eta phase precipitates distributed within the matrix phase at a concentration in the range from about 1% to about 25% by volume. The articles may be formed by mechanically working a workpiece that has at least about 40% nickel, about 1.5% to about 8% titanium, and about 1.5% to about 4.5% aluminum. The workpiece may be worked at a temperature below a solvus temperature of the eta phase; and then heat treated at a temperature sufficient to dissolve any gamma prime phase present in the workpiece but below the solvus temperature of the eta phase.