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    Post-treatment of deboronated MWW zeolite
    11.
    发明授权
    Post-treatment of deboronated MWW zeolite 有权

    公开(公告)号：US10099933B2

    公开(公告)日：2018-10-16

    申请号：US14435588

    申请日：2013-10-09

    Applicant: BASF SE

    Inventor： Andrei-Nicolae Parvulescu ,  Jeff Yang ,  Stefan Maurer ,  Manuela Gaab ,  Karsten Seidel ,  Olga Gerlach ,  Ulrich Mueller

    IPC: C01B39/48 ,  B01J35/00 ,  C01B39/02 ,  B01J29/70

    Abstract: A process for the post-treatment of a zeolitic material having an MWW framework structure, the process comprising (i) providing a zeolitic material having an MWW framework structure, wherein the framework structure of the zeolitic material comprises X2O3 and YO2, wherein Y is a tetravalent element and X is a trivalent element and wherein the molar ratio X2O3:YO2 is greater than 0.02:1; (ii) treating the zeolitic material provided in (i) with a liquid solvent system thereby obtaining a zeolitic material having a molar ratio X2O3:YO2 of at most 0.02:1, and at least partially separating the zeolitic material from the liquid solvent system; (iii) treating the zeolitic material obtained from (ii) with a liquid aqueous system having a pH in the range of 5.5 to 8 and a temperature of at least 75° C.

    Process for the conversion of oxygenates to olefins
    12.
    发明授权
    Process for the conversion of oxygenates to olefins 有权

    公开(公告)号：US09598326B2

    公开(公告)日：2017-03-21

    申请号：US14076723

    申请日：2013-11-11

    Applicant: BASF SE

    Inventor： Manuela Gaab ,  Ulrich Müller ,  Milan Kostur ,  Kirsten Spannhoff ,  Kerem Bay ,  Andrei-Nicolae Parvulescu

    IPC: C07C1/22 ,  C07C1/20

    CPC classification number: C07C1/20 ,  C07C2529/40 ,  C07C11/02

    Abstract: The present invention relates to a process for the conversion of oxygenates to olefins comprising (i) providing a gas stream comprising one or more oxygenates; and (ii) contacting the gas stream with a catalyst; wherein the catalyst comprises a zeolitic material having an MFI, MEL, and/or MWW-type framework structure comprising YO2 and X2O3, wherein Y is a tetravalent element, and X is a trivalent element, said zeolitic material being obtainable and/or obtained according to a method comprising (1) preparing a mixture comprising one or more sources for YO2, one or more sources for X2O3, and one or more solvents; and (2) crystallizing the mixture obtained in step (1) to obtain a zeolitic material having an MFI, MEL and/or MWW-type framework structure; wherein the mixture crystallized in step (2) contains 3 wt.-% or less of the one or more elements M based on 100 wt.-% of YO2, wherein M stands for sodium.

    Production and Use of a Zeolitic Material in a Process for the Conversion of Oxygenates to Olefins
    15.
    发明申请
    Production and Use of a Zeolitic Material in a Process for the Conversion of Oxygenates to Olefins 有权
    在将氧化物转化为烯烃的方法中的沸石材料的生产和使用

    公开(公告)号：US20140135556A1

    公开(公告)日：2014-05-15

    申请号：US14076651

    申请日：2013-11-11

    Applicant: BASF SE

    Inventor： Manuela Gaab ,  Ulrich Müller ,  Milan Kostur ,  Kirsten Spannhoff ,  Kerem Bay ,  Andrei-Nicolae Parvulescu

    IPC: B01J29/70 ,  C07C1/22

    CPC classification number: B01J29/7038 ,  B01J23/02 ,  B01J29/40 ,  B01J29/7034 ,  B01J37/0009 ,  B01J37/0201 ,  C07C1/20 ,  C07C2523/02 ,  C07C2529/035 ,  C07C2529/40 ,  C07C2529/70 ,  Y02P20/52 ,  C07C11/06 ,  C07C11/08

    Abstract: Described is a process for the production of a zeolitic material having an MFI, MEL, and/or MWW-type framework structure comprising YO2 and X2O3. The process comprises (1) preparing a mixture comprising one or more sources for YO2, one or more sources for X2O3, and one or more solvents; (2) crystallizing the mixture obtained in step (1) to obtain a zeolitic material having an MFI, MEL and/or MWW-type framework structure; and (3) impregnating the zeolitic material obtained in step (2) with one or more elements selected from the group of alkaline earth metals. Y is a tetravalent element, and X is a trivalent element. The mixture crystallized in step (2) contains 3 wt.-% or less of one or more elements M based on 100 wt-% of YO2, wherein M stands for sodium.

    Abstract translation: 描述了一种生产具有包含YO 2和X 2 O 3的MFI，MEL和/或MWW型骨架结构的沸石材料的方法。 该方法包括（1）制备包含一种或多种YO源的混合物，一种或多种X 2 O 3源和一种或多种溶剂的混合物; （2）使步骤（1）中获得的混合物结晶，得到具有MFI，MEL和/或MWW型骨架结构的沸石材料; 和（3）用一种或多种选自碱土金属的元素浸渍步骤（2）中获得的沸石材料。 Y是四价元素，X是三价元素。 在步骤（2）中结晶的混合物含有3重量％或更少的一种或多种基于100重量％YO 2的元素M，其中M代表钠。

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