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    Transition metal hydroxy-anion electrode materials for lithium-ion battery cathodes
    12.
    发明授权
    Transition metal hydroxy-anion electrode materials for lithium-ion battery cathodes 有权
    用于锂离子电池阴极的过渡金属羟基 - 阴离子电极材料

    公开(公告)号：US09590247B2

    公开(公告)日：2017-03-07

    申请号：US14408870

    申请日：2013-06-20

    申请人： Candace Chan

    发明人： Candace Chan

    IPC分类号： H01M4/13 ,  H01M4/58 ,  H01M4/00 ,  H01M4/42 ,  H01M4/136 ,  C01B25/37 ,  C01G3/10 ,  H01M4/1391 ,  H01M10/052 ,  H01M4/02

    CPC分类号： H01M4/5825 ,  C01B25/37 ,  C01G3/10 ,  H01M4/136 ,  H01M4/1391 ,  H01M10/052 ,  H01M2004/028 ,  Y02E60/122

    摘要： A transition metal hydroxy-anion electrode material for lithium-ion battery cathodes includes the charge-neutral structure Mx(OH)n(XO4)m, where M is one or more transition metals, x is the total number of transition metal atoms, X is sulfur or phosphorus, and x, n, and m are integers. (OH)n(XO4)m is a hydroxysulfate or hydroxyphosphate, and M can be one or more (e.g., a solid solution of) transition metals selected from the group consisting of copper, iron, manganese, nickel, vanadium, cobalt, zinc, chromium, and molybdenum. A lithium-ion battery may have a cathode including Mx(OH)n(XO4)m as a cathode material, and an electronic device may include a lithium-ion battery having a cathode including Mx(OH)n(XO4)m as a cathode material.

    摘要翻译： 用于锂离子电池阴极的过渡金属羟基 - 阴离子电极材料包括电荷中性结构Mx（OH）n（XO4）m，其中M是一种或多种过渡金属，x是过渡金属原子的总数X 是硫或磷，x，n和m是整数。 （OH）n（XO4）m是羟基硫酸盐或羟基磷酸盐，M可以是选自铜，铁，锰，镍，钒，钴，锌中的一种或多种（例如，固溶体）过渡金属 ，铬和钼。 锂离子电池可以具有包括M x（OH）n（XO 4）m作为阴极材料的阴极，并且电子器件可以包括具有包含M x（OH）n（XO 4）m的阴极的锂离子电池作为 阴极材料。

    Lithium lanthanum zirconate thin films
    13.
    发明授权
    Lithium lanthanum zirconate thin films 有权

    公开(公告)号：US11268196B2

    公开(公告)日：2022-03-08

    申请号：US16669767

    申请日：2019-10-31

    申请人： Candace Chan ,  Jon Mark Weller

    发明人： Candace Chan ,  Jon Mark Weller

    IPC分类号： C23C16/40 ,  C23C16/455 ,  C23C18/12 ,  C23C22/05 ,  C23C22/70 ,  C23C28/04 ,  H01M10/0562 ,  C23C16/56 ,  H01M10/0525

    摘要： Forming a lithium lanthanum zirconate thin film includes disposing zirconium oxide on a substrate to yield a zirconium oxide coating, contacting the zirconium oxide coating with a solution including a lithium salt and a lanthanum salt, heating the substrate to yield a dried salt coating on the zirconium oxide coating, melting the dried salt coating to yield a molten salt mixture, reacting the molten salt mixture with the zirconium oxide coating to yield lithium lanthanum zirconate, and cooling the lithium lanthanum zirconate to yield a lithium lanthanum zirconate coating on the substrate. In some cases, the zirconium oxide coating is contacted with an aqueous molten salt mixture including a lithium salt and a lanthanum salt, the molten salt mixture is reacted with the zirconium oxide coating to yield lithium lanthanum zirconate, and the lithium lanthanum zirconate is cooled to yield a lithium lanthanum zirconate coating on the substrate.

    SYNTHESIS OF LITHIUM LANTHANUM ZIRCONATE FROM NANOCRYSTALLINE LANTHANUM ZIRCONATE
    15.
    发明申请
    SYNTHESIS OF LITHIUM LANTHANUM ZIRCONATE FROM NANOCRYSTALLINE LANTHANUM ZIRCONATE 有权

    公开(公告)号：US20210371296A1

    公开(公告)日：2021-12-02

    申请号：US17396967

    申请日：2021-08-09

    申请人： Jon Weller ,  Candace Chan

    发明人： Jon Weller ,  Candace Chan

    IPC分类号： C01G25/00 ,  C08L33/08 ,  C08L33/10 ,  C08L29/14 ,  C08K5/053 ,  C08K5/09

    摘要： Fabricating a layer including lithium lanthanum zirconate (Li7La3Zr2O12) layer includes forming a slurry including lanthanum zirconate (La2Zr2O7) nanocrystals, a lithium precursor, and a lanthanum precursor in stoichiometric amounts to yield a dispersion including lithium, lanthanum, and zirconium. In some cases, the dispersion includes lithium, lanthanum, and zirconium in a molar ratio of 7:3:2. In certain cases, the slurry includes excess lithium. The slurry is dispensed onto a substrate and dried. The dried slurry is calcined to yield the layer including lithium lanthanum zirconate.

    Oxidation-reduction assisted exfoliation and reassembly of transition metal oxide lithium intercalation compounds
    19.
    发明授权
    Oxidation-reduction assisted exfoliation and reassembly of transition metal oxide lithium intercalation compounds 有权

    公开(公告)号：US10720642B2

    公开(公告)日：2020-07-21

    申请号：US15661080

    申请日：2017-07-27

    申请人： Candace Chan ,  Qian Cheng

    发明人： Candace Chan ,  Qian Cheng

    IPC分类号： H01M4/525 ,  H01M4/505 ,  H01M10/0525 ,  C25B1/14 ,  B01J2/18 ,  H01M4/02

    摘要： Exfoliating transition metal oxide lithium intercalation particles having lithium ions intercalated between transition metal oxide nanosheets includes electrochemically oxidizing a transition metal in first transition metal oxide lithium intercalation particles from a first oxidation state to a second oxidation state, inserting first cations having a radius exceeding the radius of a lithium ion into the vacancies, reducing the transition metal from the second oxidation state to the first oxidation state, and exfoliating the transition metal oxide nanosheets from the second transition metal oxide lithium intercalation particles to yield dispersed transition metal oxide nanosheets comprising the transition metal in the first oxidation state and oxygen. The dispersed transition metal oxide nanosheets can be reassembled to yield a material suitable for a lithium-ion battery cathode. Metal oxide sodium intercalation particles can be similarly exfoliated and reassembled to yield a material suitable for a sodium-ion battery cathode.