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11.发明授权High voltage battery formation protocols and control of charging and discharging for desirable long term cycling performance 有权高电压电池形成方案和充放电控制，达到理想的长期循环性能公开(公告)号：US08765306B2
公开(公告)日：2014-07-01
申请号：US12732520
申请日：2010-03-26
IPC分类号： H01M10/0525 , H01M4/525 , H01M4/583 , H01M10/44 , H02J7/00 , H01M4/505 , H01M4/587 , H01M4/04 , H01M4/131 , H01M10/058 , H01M10/0585
CPC分类号： H02J7/0075 , H01M4/0447 , H01M4/505 , H01M4/587 , H01M10/0525 , H01M10/44 , H01M10/446 , Y02E60/122
摘要： Improved cycling of high voltage lithium ion batteries is accomplished through the use of a formation step that seems to form a more stable structure for subsequent cycling and through the improved management of the charge-discharge cycling. In particular, the formation charge for the battery can be performed at a lower voltage prior to full activation of the battery through a charge to the specified operational voltage of the battery. With respect to management of the charging and discharging of the battery, it has been discovered that for the lithium rich high voltage compositions of interest that a deeper discharge can preserve the cycling capacity at a greater number of cycles. Battery management can be designed to exploit the improved cycling capacity obtained with deeper discharges of the battery.
摘要翻译： 高压锂离子电池的改进循环是通过使用似乎形成用于随后循环的更稳定结构并通过改进的充放电循环管理的形成步骤来实现的。 特别地，电池的形成电荷可以在电池完全激活之前以较低的电压进行，通过电荷到电池的指定工作电压。 关于电池的充电和放电的管理，已经发现，对于感兴趣的富锂高压组合物，更深的放电可以在更多的循环数量下保持循环容量。 电池管理可以设计成利用电池更深的放电获得的改进的循环容量。
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公开(公告)号：US20120107680A1
公开(公告)日：2012-05-03
申请号：US12938073
申请日：2010-11-02
CPC分类号： H01M4/1393 , C01G45/1228 , C01G45/1257 , C01G51/50 , C01G53/50 , C01P2004/82 , H01M4/0447 , H01M4/1395 , H01M4/386 , H01M4/505 , H01M4/587 , H01M6/5005 , H01M10/052 , H01M10/058 , H01M10/446 , Y02E60/122 , Y02T10/7011 , Y10T29/49108 , Y10T29/49115
摘要： Supplemental lithium can be used to stabilize lithium ion batteries with lithium rich metal oxides as the positive electrode active material. Dramatic improvements in the specific capacity at long cycling have been obtained. The supplemental lithium can be provided with the negative electrode, or alternatively as a sacrificial material that is subsequently driven into the negative electrode active material. The supplemental lithium can be provided to the negative electrode active material prior to assembly of the battery using electrochemical deposition. The positive electrode active materials can comprise a layered-layered structure comprising manganese as well as nickel and/or cobalt.
摘要翻译： 补充锂可用于稳定锂离子电池与富锂金属氧化物作为正极活性物质。 已经获得了长时间骑行的具体能力的显着改善。 补充的锂可以设置有负极，或者替代地作为随后被驱动到负极活性材料中的牺牲材料。 在使用电化学沉积的电池组装之前，可以将补充的锂提供给负极活性材料。 正极活性物质可以包括包含锰以及镍和/或钴的层状结构的结构。
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13.发明申请公开(公告)号：US20110236751A1
公开(公告)日：2011-09-29
申请号：US12732520
申请日：2010-03-26
CPC分类号： H02J7/0075 , H01M4/0447 , H01M4/505 , H01M4/587 , H01M10/0525 , H01M10/44 , H01M10/446 , Y02E60/122
摘要： Improved cycling of high voltage lithium ion batteries is accomplished through the use of a formation step that seems to form a more stable structure for subsequent cycling and through the improved management of the charge-discharge cycling. In particular, the formation charge for the battery can be performed at a lower voltage prior to full activation of the battery through a charge to the specified operational voltage of the battery. With respect to management of the charging and discharging of the battery, it has been discovered that for the lithium rich high voltage compositions of interest that a deeper discharge can preserve the cycling capacity at a greater number of cycles. Battery management can be designed to exploit the improved cycling capacity obtained with deeper discharges of the battery.
摘要翻译： 高压锂离子电池的改进循环是通过使用似乎形成用于随后循环的更稳定结构并通过改进的充放电循环管理的形成步骤来实现的。 特别地，电池的形成电荷可以在电池完全激活之前以较低的电压进行，通过电荷到电池的指定工作电压。 关于电池的充电和放电的管理，已经发现，对于感兴趣的富锂高压组合物，更深的放电可以在更多的循环数量下保持循环容量。 电池管理可以设计成利用电池更深的放电获得的改进的循环容量。
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14.发明授权Metal halide coatings on lithium ion battery positive electrode materials and corresponding batteries 有权锂离子电池正极材料和相应电池上的金属卤化物涂层公开(公告)号：US08663849B2
公开(公告)日：2014-03-04
申请号：US12888131
申请日：2010-09-22
CPC分类号： H01M4/136 , H01M4/1315 , H01M4/13915 , H01M4/1397 , H01M4/366 , H01M4/485 , H01M4/505 , H01M4/525 , H01M4/582 , H01M10/052 , Y02T10/7011
摘要： Lithium ion battery positive electrode material are described that comprise an active composition comprising lithium metal oxide coated with an inorganic coating composition wherein the coating composition comprises a metal chloride, metal bromide, metal iodide, or combinations thereof. Desirable performance is observed for these coated materials. In particular, the non-fluoride metal halide coatings are useful for stabilizing lithium rich metal oxides.
摘要翻译： 描述了锂离子电池正极材料，其包含涂覆有无机涂料组合物的包含锂金属氧化物的活性组合物，其中涂料组合物包含金属氯化物，金属溴化物，金属碘化物或其组合。 对于这些涂覆材料观察到理想的性能。 特别地，非氟化物金属卤化物涂层可用于稳定富锂金属氧化物。
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公开(公告)号：US20120105007A1
公开(公告)日：2012-05-03
申请号：US13305981
申请日：2011-11-29
CPC分类号： H01M4/1393 , C01G45/1228 , C01G45/1257 , C01G51/50 , C01G53/50 , C01P2004/82 , H01M4/0447 , H01M4/1395 , H01M4/386 , H01M4/505 , H01M4/587 , H01M6/5005 , H01M10/052 , H01M10/058 , H01M10/446 , Y02E60/122 , Y02T10/7011 , Y10T29/49108 , Y10T29/49115
摘要： Supplemental lithium can be used to stabilize lithium ion batteries with lithium rich metal oxides as the positive electrode active material. Dramatic improvements in the specific capacity at long cycling have been obtained. The supplemental lithium can be provided with the negative electrode, or alternatively as a sacrificial material that is subsequently driven into the negative electrode active material. The supplemental lithium can be provided to the negative electrode active material prior to assembly of the battery using electrochemical deposition. The positive electrode active materials can comprise a layered-layered structure comprising manganese as well as nickel and/or cobalt.
摘要翻译： 补充锂可用于稳定锂离子电池与富锂金属氧化物作为正极活性物质。 已经获得了长时间骑行的具体能力的显着改善。 补充的锂可以设置有负极，或者替代地作为随后被驱动到负极活性材料中的牺牲材料。 在使用电化学沉积的电池组装之前，可以将补充的锂提供给负极活性材料。 正极活性物质可以包括包含锰以及镍和/或钴的层状结构的结构。
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16.发明申请METAL HALIDE COATINGS ON LITHIUM ION BATTERY POSITIVE ELECTRODE MATERIALS AND CORRESPONDING BATTERIES 有权锂离子电池正极电极材料和相应电池的金属卤化物涂层公开(公告)号：US20120070725A1
公开(公告)日：2012-03-22
申请号：US12888131
申请日：2010-09-22
CPC分类号： H01M4/136 , H01M4/1315 , H01M4/13915 , H01M4/1397 , H01M4/366 , H01M4/485 , H01M4/505 , H01M4/525 , H01M4/582 , H01M10/052 , Y02T10/7011
摘要： Lithium ion battery positive electrode material are described that comprise an active composition comprising lithium metal oxide coated with an inorganic coating composition wherein the coating composition comprises a metal chloride, metal bromide, metal iodide, or combinations thereof. Desirable performance is observed for these coated materials. In particular, the non-fluoride metal halide coatings are useful for stabilizing lithium rich metal oxides.
摘要翻译： 描述了锂离子电池正极材料，其包含涂覆有无机涂料组合物的包含锂金属氧化物的活性组合物，其中涂料组合物包含金属氯化物，金属溴化物，金属碘化物或其组合。 对于这些涂覆材料观察到理想的性能。 特别地，非氟化物金属卤化物涂层可用于稳定富锂金属氧化物。
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17.发明授权Lithium ion batteries with high energy density, excellent cycling capability and low internal impedance 有权具有高能量密度，优异的循环能力和低内部阻抗的锂离子电池公开(公告)号：US09552901B2
公开(公告)日：2017-01-24
申请号：US13588783
申请日：2012-08-17
申请人： Shabab Amiruddin , Subramanian Venkatachalam , Bing Li , Charles Bowling , Yezi Bei , Deepak Kumaar Karthikeyan , Herman Lopez , Sujeet Kumar
发明人： Shabab Amiruddin , Subramanian Venkatachalam , Bing Li , Charles Bowling , Yezi Bei , Deepak Kumaar Karthikeyan , Herman Lopez , Sujeet Kumar
IPC分类号： H01M4/13 , H01M4/58 , H01M6/12 , H01M6/46 , H01M4/00 , H01B1/08 , H01M4/505 , H01M4/131 , H01M10/0525 , C01G53/00 , H01M2/02
CPC分类号： H01B1/08 , C01G53/50 , C01P2002/52 , C01P2006/40 , H01M2/021 , H01M4/131 , H01M4/505 , H01M10/0525 , Y02E60/122 , Y02T10/7011
摘要： Batteries with particularly high energy capacity and low internal impedance have been described herein. The batteries can exhibit extraordinary long cycling with acceptable low amounts of fade. Pouch batteries using high specific capacity lithium rich metal oxide as positive electrode material combined with graphitic carbon anode can reach an energy density of at least about 180 Wh/kg at a rate of C/3 from 4.35V to 2V at room temperature while having a room temperature areas specific DC resistance of no more than about 75 ohms-cm2 at 20% SOC based on a full charge to 4.35V. High specific capacity lithium rich metal oxide with specific stoichiometry ranges used in these batteries are disclosed.
摘要翻译： 这里描述了具有特别高的能量容量和低内部阻抗的电池。 电池可以显示非凡的长时间循环，可接受的低褪色量。 使用高比容量的富锂金属氧化物作为与石墨碳阳极结合的正极材料的袋电池可以在室温下从4.35V至2V的C / 3速率达到至少约180Wh / kg的能量密度，同时具有 室温区域的特定直流电阻不超过约75欧姆 - 厘米2，基于充电至4.35V的20％SOC。 公开了在这些电池中使用的具有特定化学计量范围的高比容量的富锂金属氧化物。
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18.发明申请LITHIUM ION BATTERIES WITH HIGH ENERGY DENSITY, EXCELLENT CYCLING CAPABILITY AND LOW INTERNAL IMPEDANCE 有权具有高能量密度，卓越循环能力和低内部阻抗的锂离子电池公开(公告)号：US20140050972A1
公开(公告)日：2014-02-20
申请号：US13588783
申请日：2012-08-17
申请人： Shabab Amiruddin , Subramanian Venkatachalam , Bing Li , Charles Bowling , Yezi Bei , Deepak Kumaar Karthikeyan , Herman Lopez , Sujeet Kumar
发明人： Shabab Amiruddin , Subramanian Venkatachalam , Bing Li , Charles Bowling , Yezi Bei , Deepak Kumaar Karthikeyan , Herman Lopez , Sujeet Kumar
IPC分类号： H01M4/505 , H01B1/08 , H01M4/54 , H01M4/525 , H01M10/052 , H01M10/056
CPC分类号： H01B1/08 , C01G53/50 , C01P2002/52 , C01P2006/40 , H01M2/021 , H01M4/131 , H01M4/505 , H01M10/0525 , Y02E60/122 , Y02T10/7011
摘要： Batteries with particularly high energy capacity and low internal impedance have been described herein. The batteries can exhibit extraordinary long cycling with acceptable low amounts of fade. Pouch batteries using high specific capacity lithium rich metal oxide as positive electrode material combined with graphitic carbon anode can reach an energy density of at least about 180 Wh/kg at a rate of C/3 from 4.35V to 2V at room temperature while having a room temperature areas specific DC resistance of no more than about 75 ohms-cm2 at 20% SOC based on a full charge to 4.35V. High specific capacity lithium rich metal oxide with specific stoichiometry ranges used in these batteries are disclosed.
摘要翻译： 这里描述了具有特别高的能量容量和低内部阻抗的电池。 电池可以显示非凡的长时间循环，可接受的低褪色量。 使用高比容量的富锂金属氧化物作为与石墨碳阳极结合的正极材料的袋电池可以在室温下从4.35V至2V的C / 3速率达到至少约180Wh / kg的能量密度，同时具有 室温区域的特定直流电阻不超过约75欧姆 - 厘米2，基于充电至4.35V的20％SOC。 公开了在这些电池中使用的具有特定化学计量范围的高比容量的富锂金属氧化物。
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公开(公告)号：US09139441B2
公开(公告)日：2015-09-22
申请号：US13354096
申请日：2012-01-19
申请人： Yogesh Kumar Anguchamy , Charan Masarapu , Haixia Deng , Yongbong Han , Subramanian Venkatachalam , Sujeet Kumar , Herman A. Lopez
发明人： Yogesh Kumar Anguchamy , Charan Masarapu , Haixia Deng , Yongbong Han , Subramanian Venkatachalam , Sujeet Kumar , Herman A. Lopez
IPC分类号： H01M4/525 , C01B33/023 , H01M4/134 , H01M4/38 , B82Y30/00 , H01M4/36 , H01M4/505 , H01M4/62 , H01M10/052 , H01M4/02 , H01M10/42
CPC分类号： C01B33/023 , B82Y30/00 , H01M4/134 , H01M4/362 , H01M4/366 , H01M4/386 , H01M4/505 , H01M4/525 , H01M4/622 , H01M4/625 , H01M10/052 , H01M2004/021 , H01M2010/4292 , Y02E60/122 , Y02T10/7011
摘要： A porous silicon based material comprising porous crystalline elemental silicon formed by reducing silicon dioxide with a reducing metal in a heating process followed by acid etching is used to construct negative electrode used in lithium ion batteries. Gradual temperature heating ramp(s) with optional temperature steps can be used to perform the heating process. The porous silicon formed has a high surface area from about 10 m2/g to about 200 m2/g and is substantially free of carbon. The negative electrode formed can have a discharge specific capacity of at least 1800 mAh/g at rate of C/3 discharged from 1.5V to 0.005V against lithium with in some embodiments loading levels ranging from about 1.4 mg/cm2 to about 3.5 mg/cm2. In some embodiments, the porous silicon can be coated with a carbon coating or blended with carbon nanofibers or other conductive carbon material.
摘要翻译： 使用包含在加热过程中随后用酸蚀刻还原二氧化硅形成的多孔结晶元素硅的多孔硅基材料来构造用于锂离子电池的负极。 可以使用温度逐渐升温的温度梯度来进行加热过程。 形成的多孔硅具有约10m 2 / g至约200m 2 / g的高表面积，并且基本上不含碳。 形成的负极可以具有至少1800mAh / g的放电比容量，其相对于锂从1.5V至0.005V释放的C / 3的速率，在一些实施方案中负载水平为约1.4mg / cm 2至约3.5mg / cm2。 在一些实施例中，多孔硅可以涂覆有碳涂层或与碳纳米纤维或其它导电碳材料混合。
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公开(公告)号：US09190694B2
公开(公告)日：2015-11-17
申请号：US12938951
申请日：2010-11-03
申请人： Herman A. Lopez , Yogesh Kumar Anguchamy , Haixia Deng , Yongbong Han , Charan Masarapu , Subramanian Venkatachalam , Sujeet Kumar
发明人： Herman A. Lopez , Yogesh Kumar Anguchamy , Haixia Deng , Yongbong Han , Charan Masarapu , Subramanian Venkatachalam , Sujeet Kumar
CPC分类号： H01M4/134 , C25F3/12 , H01M4/131 , H01M4/133 , H01M4/364 , H01M4/38 , H01M4/386 , H01M4/505 , H01M4/525 , H01M4/587 , H01M4/621 , H01M4/622 , H01M10/0525 , H01M2004/027 , H01M2004/028 , H01M2220/30 , Y02E60/122
摘要： High capacity silicon based anode active materials are described for lithium ion batteries. These materials are shown to be effective in combination with high capacity lithium rich cathode active materials. Supplemental lithium is shown to improve the cycling performance and reduce irreversible capacity loss for at least certain silicon based active materials. In particular silicon based active materials can be formed in composites with electrically conductive coatings, such as pyrolytic carbon coatings or metal coatings, and composites can also be formed with other electrically conductive carbon components, such as carbon nanofibers and carbon nanoparticles. Additional alloys with silicon are explored.
摘要翻译： 锂离子电池描述了大容量硅基阳极活性材料。 这些材料显示与高容量富锂正极活性材料组合有效。 补充锂显示出改善循环性能并减少至少某些基于硅的活性材料的不可逆容量损失。 特别地，硅基活性材料可以与导电涂层（例如热解碳涂层或金属涂层）的复合材料形成，并且复合材料也可以与其它导电碳组分如碳纳米纤维和碳纳米颗粒一起形成。 探索了具有硅的附加合金。
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