公开(公告)号：US08092609B2

公开(公告)日：2012-01-10

申请号：US12025153

申请日：2008-02-04

申请人： Robert Jansen ,  John Kerr ,  Anthony Baiada

发明人： Robert Jansen ,  John Kerr ,  Anthony Baiada

IPC分类号： C13K1/08

CPC分类号： C13K3/00 ,  C13B20/14

摘要： We disclose a method of inverting sucrose, including (i) determining an initial solids concentration of an aqueous sucrose solution (solidsi), an initial bed volume (BVi) of a sucrose inversion resin system, a minimum target inversion percentage (invert %min), a maximum target inversion percentage (invert %max), a target maximum hydroxymethylfuran (HMF) concentration (HMFmax), a minimum target pH (pHmin), or a maximum target pH (pHmax); (ii) contacting the sucrose inversion resin system with the aqueous sucrose solution under conditions of aqueous solution flow rate in BVi/hr (ratep) and aqueous solution temperature in ° C. (temperaturep) to produce an inverted sucrose solution having an inversion percentage (invert %product), an HMF concentration (HMFproduct), and a pH (pHproduct); (iii) observing an instantaneous inversion percentage (invert %inst), an instantaneous HMF concentration (HMFinst), or an instantaneous pH (pHinst) of the inverted sucrose solution; and, if invert %inst invert %max, HMFinst>HMFmax, pHinst pHmax; (iv) changing at least one of the aqueous solution flow rate or the aqueous solution temperature such that invert %min≦invert %product≦invert %max, HMFproduct≦HMFmax, or pHmin≦pHproduct≦pHmax. We also disclose a computing apparatus capable of use in performing a method of inverting sucrose.

摘要翻译： 我们公开了一种蔗糖翻转方法，包括（i）测定蔗糖反应树脂体系的初始固体浓度，蔗糖反转树脂体系的初始床体积（BVi），最小目标反转百分比（反转百分比） ，最大目标反转百分比（反转百分比最大值），目标最大羟甲基呋喃（HMF）浓度（HMFmax），最小目标pH（pHmin）或最大目标pH（pHmax））; （ii）在水溶液流速（BVi / hr（速率））和水溶液温度（℃）（℃）下的条件下，将蔗糖反转树脂体系与蔗糖溶液的蔗糖溶液接触，得到反转百分比的倒转蔗糖溶液 转化％产物），HMF浓度（HMF产物）和pH（pH值产物）; （iii）观察反转蔗糖溶液的瞬时反转百分率（反转％inst），瞬时HMF浓度（HMFinst）或瞬时pH（pHinst）; 并且，如果反转％inst invert％max，HMFinst> HMFmax，pHinst pHmax; （iv）改变水溶液流速或水溶液温度中的至少一个，使得反相％min和nlE反相％max，HMFproduct＆NlE; HMFmax或pHmin＆amp; NlE; pH值＆amp; NlE; pHmax。 我们还公开了一种能够用于执行蔗糖翻转方法的计算装置。

公开(公告)号：US20090299054A1

公开(公告)日：2009-12-03

申请号：US12413955

申请日：2009-03-30

申请人： Robert Jansen ,  Gordon Walker ,  John Kerr ,  Anthony Baiada

发明人： Robert Jansen ,  Gordon Walker ,  John Kerr ,  Anthony Baiada

IPC分类号： C13K13/00

CPC分类号： C07H5/02

摘要： A process for the extraction of sucralose from an aqueous solution containing at least sucralose, other chlorinated saccharides, sodium chloride and dimethylammonium chloride into an organic solvent for sucralose by contacting said organic solvent with said solution to extract sucralose into the organic solvent. The ratio of sodium chloride to dimethylammonium chloride in the aqueous solution is increased prior to or during contact so as to increase the partition coefficient of sucralose into said organic solvent.

摘要翻译： 通过使所述有机溶剂与所述溶液接触将三氯半乳蔗糖，其它氯化糖，氯化钠和二甲基氯化铵的水溶液提取到三氯半乳蔗糖的有机溶剂中以将三氯蔗糖萃取到有机溶剂中的方法。 在接触之前或接触期间，水溶液中氯化钠与二甲基氯化铵的比例增加，从而增加三氯蔗糖分配成所述有机溶剂的分配系数。

公开(公告)号：US20090247792A1

公开(公告)日：2009-10-01

申请号：US12390608

申请日：2009-02-23

申请人： Robert P. Jansen ,  Anthony Baiada ,  John Kerr

发明人： Robert P. Jansen ,  Anthony Baiada ,  John Kerr

IPC分类号： C07C31/22

CPC分类号： C07C29/86 ,  C07C31/225

摘要： A process for the recovery of glycerol comprises contacting an aqueous feed composition that comprises water, glycerol, and at least one contaminant with a solvent extractant comprising at least one C5-C8 alkanol, optionally in admixture with at least one alkane, to form a first mixture, and separating the first mixture into a first solvent phase and a first aqueous phase. The first solvent phase comprises a majority (more than 50 wt %) of the solvent extractant and a majority of the glycerol that was present in the aqueous feed composition. The weight ratio in the first solvent phase of glycerol to a contaminant present is greater than the weight ratio of glycerol to the contaminant in the aqueous feed composition. The first aqueous phase comprises a majority of the water from the aqueous feed composition and at least some of the contaminant from the aqueous feed composition.

摘要翻译： 用于回收甘油的方法包括使包含水，甘油和至少一种污染物的含水进料组合物与包含至少一种C5-C8链烷醇的溶剂萃取剂接触，任选与至少一种烷烃混合形成第一 混合物，并将第一混合物分离成第一溶剂相和第一水相。 第一溶剂相包含大部分（超过50重量％）的溶剂萃取剂和存在于含水进料组合物中的大部分甘油。 丙三醇与污染物的第一溶剂相中的重量比大于水性进料组合物中甘油与污染物的重量比。 第一水相包含来自含水进料组合物的大部分水和来自含水进料组合物的至少一些污染物。

公开(公告)号：US20120138048A1

公开(公告)日：2012-06-07

申请号：US13316278

申请日：2011-12-09

申请人： Robert Jansen ,  John Kerr ,  Anthony Baiada

发明人： Robert Jansen ,  John Kerr ,  Anthony Baiada

IPC分类号： C13B99/00

CPC分类号： C13K3/00 ,  C13B20/14

摘要： A method of inverting sucrose, including (i) determining an initial solids concentration of an aqueous sucrose solution, an initial bed volume of a sucrose inversion resin system, a minimum target inversion percentage, a maximum target inversion percentage, a target maximum hydroxymethylfuran (HMF) concentration, a minimum target pH, or a maximum target pH; (ii) contacting the sucrose inversion resin system with the aqueous sucrose solution under conditions of aqueous solution flow rate and aqueous solution temperature to produce an inverted sucrose solution having an inversion percentage, an HMF concentration, and a pH; (iii) observing an instantaneous inversion percentage, an instantaneous HMF concentration, or an instantaneous pH of the inverted sucrose solution; and, if appropriate; (iv) changing at least one of the aqueous solution flow rate or the aqueous solution temperature to yield a product having a desired inversion percentage, HMF concentration, and/or pH. An apparatus capable of performing the method.

摘要翻译： 一种反相蔗糖的方法，包括（i）测定蔗糖水溶液的初始固体浓度，蔗糖反转树脂体系的初始床体积，最小目标反转百分比，最大目标反转百分比，目标最大羟甲基呋喃（HMF ）浓度，最小目标pH或最大目标pH; （ii）在水溶液流动速率和水溶液温度条件下使蔗糖反转树脂体系与蔗糖溶液水溶液接触，以产生具有倒置百分数，HMF浓度和pH值的倒置蔗糖溶液; （iii）观察反转蔗糖溶液的瞬时反转百分比，瞬时HMF浓度或瞬时pH值; 并酌情; （iv）改变水溶液流速或水溶液温度中的至少一个，得到具有所需转化百分比，HMF浓度和/或pH值的产物。 一种能够执行该方法的装置。

公开(公告)号：US08497367B2

公开(公告)日：2013-07-30

申请号：US12413955

申请日：2009-03-30

申请人： Robert Jansen ,  Gordon Walker ,  John Kerr ,  Anthony Baiada

发明人： Robert Jansen ,  Gordon Walker ,  John Kerr ,  Anthony Baiada

IPC分类号： C07H5/02

CPC分类号： C07H5/02

摘要： A process for the extraction of sucralose from an aqueous solution containing at least sucralose, other chlorinated saccharides, sodium chloride and dimethylammonium chloride into an organic solvent for sucralose by contacting said organic solvent with said solution to extract sucralose into the organic solvent. The ratio of sodium chloride to dimethylammonium chloride in the aqueous solution is increased prior to or during contact so as to increase the partition coefficient of sucralose into said organic solvent.

摘要翻译： 通过使所述有机溶剂与所述溶液接触将三氯半乳蔗糖，其它氯化糖，氯化钠和二甲基氯化铵的水溶液提取到三氯半乳蔗糖的有机溶剂中以将三氯蔗糖萃取到有机溶剂中的方法。 在接触之前或接触期间，水溶液中氯化钠与二甲基氯化铵的比例增加，从而增加三氯蔗糖分配成所述有机溶剂的分配系数。

公开(公告)号：US08084651B2

公开(公告)日：2011-12-27

申请号：US12390608

申请日：2009-02-23

申请人： Robert P. Jansen ,  Anthony Baiada ,  John Kerr

发明人： Robert P. Jansen ,  Anthony Baiada ,  John Kerr

IPC分类号： C07C31/22

CPC分类号： C07C29/86 ,  C07C31/225

摘要： A process for the recovery of glycerol comprises contacting an aqueous feed composition that comprises water, glycerol, and at least one contaminant with a solvent extractant comprising at least one C5-C8 alkanol, optionally in admixture with at least one alkane, to form a first mixture, and separating the first mixture into a first solvent phase and a first aqueous phase. The first solvent phase comprises a majority (more than 50 wt %) of the solvent extractant and a majority of the glycerol that was present in the aqueous feed composition. The weight ratio in the first solvent phase of glycerol to a contaminant present is greater than the weight ratio of glycerol to the contaminant in the aqueous feed composition. The first aqueous phase comprises a majority of the water from the aqueous feed composition and at least some of the contaminant from the aqueous feed composition.

摘要翻译： 用于回收甘油的方法包括使包含水，甘油和至少一种污染物的含水进料组合物与包含至少一种C5-C8链烷醇的溶剂萃取剂接触，任选与至少一种烷烃混合形成第一 混合物，并将第一混合物分离成第一溶剂相和第一水相。 第一溶剂相包含大部分（超过50重量％）的溶剂萃取剂和存在于含水进料组合物中的大部分甘油。 丙三醇与污染物的第一溶剂相中的重量比大于水性进料组合物中甘油与污染物的重量比。 第一水相包含来自含水进料组合物的大部分水和来自含水进料组合物的至少一些污染物。

公开(公告)号：US20080276931A1

公开(公告)日：2008-11-13

申请号：US12025153

申请日：2008-02-04

申请人： Robert Jansen ,  John Kerr ,  Anthony Baiada

发明人： Robert Jansen ,  John Kerr ,  Anthony Baiada

IPC分类号： C13J1/06 ,  G05B21/00

CPC分类号： C13K3/00 ,  C13B20/14

摘要： We disclose a method of inverting sucrose, including (i) determining an initial solids concentration of an aqueous sucrose solution (solidsi), an initial bed volume (BVi) of a sucrose inversion resin system, a minimum target inversion percentage (invert %min), a maximum target inversion percentage (invert %max), a target maximum hydroxymethylfuran (HMF) concentration (HMFmax), a minimum target pH (pHmin), or a maximum target pH (pHmax); (ii) contacting the sucrose inversion resin system with the aqueous sucrose solution under conditions of aqueous solution flow rate in BVi/hr (ratep) and aqueous solution temperature in ° C. (temperaturep) to produce an inverted sucrose solution having an inversion percentage (invert %product), an HMF concentration (HMFproduct), and a pH (pHproduct); (iii) observing an instantaneous inversion percentage (invert %inst), an instantaneous HMF concentration (HMFinst), or an instantaneous pH (pHinst) of the inverted sucrose solution; and, if invert %inst invert %max, HMFinst>HMFmax, pHinst pHmax; (iv) changing at least one of the aqueous solution flow rate or the aqueous solution temperature such that invert %min≦invert %product≦invert %max, HMFproduct≦HMFmax, or pHmin≦pHproduct≦pHmax. We also disclose a computing apparatus capable of use in performing a method of inverting sucrose.

公开(公告)号：US20090238918A1

公开(公告)日：2009-09-24

申请号：US12357555

申请日：2009-01-22

申请人： Robert Jansen ,  John Kerr ,  Peter Lloyd-Jones ,  Richard Tanner

发明人： Robert Jansen ,  John Kerr ,  Peter Lloyd-Jones ,  Richard Tanner

IPC分类号： C12C11/07 ,  C12C1/16

CPC分类号： C13K1/06 ,  C08B30/044 ,  C12P7/06 ,  C12P19/14 ,  Y02E50/17

摘要： A corn wet-milling process comprises steeping corn kernels in an aqueous liquid, which produces softened corn; milling the softened corn in a first mill, which produces a first milled corn; separating germ from the first milled corn, thereby producing a germ-depleted first milled corn; milling the germ-depleted first milled corn in a second mill, producing a second milled corn; separating the second milled corn into a first starch/protein portion that comprises starch and protein and a first fiber portion that comprises fiber, starch, and protein; milling the first fiber portion in a third mill, which produces a milled fiber material that comprises fiber, starch, and protein; separating at least some of the starch and protein in the milled fiber material from the fiber therein, producing a second fiber portion that comprises fiber and starch and a second starch/protein portion that comprises starch and protein; and contacting the second fiber portion with at least one enzyme to convert at least some of the starch therein to dextrose. The converted material is screened using one or more screens to separate the fiber from the liquor. The liquor can be fermented to ethanol, or refined to dextrose. The fiber can be pressed and dried as an animal feed.

摘要翻译： 玉米湿法研磨方法包括在含水液体中浸泡玉米粒，产生软化的玉米; 在第一磨机中研磨软化的玉米，其生产第一研磨的玉米; 将胚芽与第一磨碎的玉米分离，从而产生一种无菌的第一磨碎的玉米; 在第二磨机中研磨灭菌的第一批玉米，生产第二批玉米; 将第二研磨的玉米分离成包含淀粉和蛋白质的第一淀粉/蛋白质部分和包含纤维，淀粉和蛋白质的第一纤维部分; 在第三磨机中研磨第一纤维部分，其产生包含纤维，淀粉和蛋白质的研磨纤维材料; 将磨碎的纤维材料中的至少一些淀粉和蛋白质与其中的纤维分离，产生包含纤维和淀粉的第二纤维部分和包含淀粉和蛋白质的第二淀粉/蛋白质部分; 以及使所述第二纤维部分与至少一种酶接触以将其中的至少一些淀粉转化成葡萄糖。 使用一个或多个筛网筛选转化的材料以将纤维与液体分离。 酒可以发酵成乙醇，或精制成葡萄糖。 纤维可以作为动物饲料被压制和干燥。

公开(公告)号：US20090095286A1

公开(公告)日：2009-04-16

申请号：US12173257

申请日：2008-07-15

申请人： John Kerr ,  Robert Jansen ,  Loren Luppes ,  Peter Lloyd-Jones ,  Richard Tanner

发明人： John Kerr ,  Robert Jansen ,  Loren Luppes ,  Peter Lloyd-Jones ,  Richard Tanner

IPC分类号： C08B30/00

CPC分类号： C12M43/04 ,  A23J1/12 ,  A23L7/152 ,  A23L7/197 ,  C12M21/04 ,  C12M21/12 ,  C12P5/023 ,  C12P7/06 ,  F23G2900/50208 ,  Y02E50/17 ,  Y02E50/343

摘要： A process including steeping cereal kernels in an aqueous liquid, producing softened cereal; milling the softened cereal, producing a milled cereal comprising germ, protein, starch, and fiber; separating at least some of at least one material selected from the group consisting of germ, starch, and protein from the milled cereal, producing at least one of germ, starch, and a first protein portion, and also producing a first fiber portion that comprises fiber and starch, and a light steep water that comprises protein; separating at least some protein from the light steep water, producing a second protein portion and a process water that comprises protein; converting at least some of the starch in the first fiber portion to saccharides; separating at least some of the saccharides from the first fiber portion, producing saccharides and a second fiber portion that comprises fiber; and burning at least some of the fiber from the second fiber portion, producing a flue gas and a first quantity of energy; wherein the process further comprises at least one step selected from the group consisting of least partially powering at least one previous step with the first quantity of energy; and drying at least one separated material selected from the group consisting of the germ, the starch, the first protein portion, the second protein portion, and the saccharides with the flue gas, producing a dried separated material and a dryer exhaust. In one further embodiment, the process further includes digesting anaerobically the biologically available organic residues from the process water, producing a biogas and a final waste water. In a still further embodiment, the process further includes burning the biogas to produce a second quantity of energy and at least partially powering at least one previous step with the second quantity of energy.

摘要翻译： 一种包括在水性液体中浸泡谷粒的方法，产生软化谷物; 研磨软化谷物，生产包含胚芽，蛋白质，淀粉和纤维的碾磨谷物; 从磨碎的谷物中分离至少一种选自细菌，淀粉和蛋白质的至少一种材料，产生胚芽，淀粉和第一蛋白质部分中的至少一种，并且还产生第一纤维部分，其包含 纤维和淀粉，以及包含蛋白质的轻陡的水; 从轻水中分离出至少一些蛋白质，产生第二蛋白质部分和包含蛋白质的工艺水; 将第一纤维部分中的至少一些淀粉转化为糖; 从第一纤维部分分离出至少一些糖类，生成糖类和包含纤维的第二纤维部分; 并且从第二纤维部分燃烧至少一些纤维，产生烟道气和第一量的能量; 其中所述方法还包括至少一个步骤，所述步骤选自由对所述第一能量的至少一个先前步骤进行的至少部分供电; 并用烟道气干燥选自由胚芽，淀粉，第一蛋白质部分，第二蛋白质部分和糖类组成的组中的至少一种分离的材料，产生干燥的分离的材料和干燥器排气。 在一个另外的实施方案中，该方法还包括厌氧地从工艺水中消化生物可获得的有机残余物，产生沼气和最终的废水。 在又一个实施例中，该方法还包括燃烧沼气以产生第二数量的能量，并且至少部分地为第二数量的能量提供至少一个先前步骤。

公开(公告)号：US08422998B2

公开(公告)日：2013-04-16

申请号：US11814523

申请日：2005-01-31

申请人： Christian Herrero Verón ,  Patrice Hédé ,  John Kerr

发明人： Christian Herrero Verón ,  Patrice Hédé ,  John Kerr

IPC分类号： H04M3/42 ,  H04W4/00 ,  H04L29/08 ,  H04L12/66 ,  H04N7/14

CPC分类号： H04W4/16

摘要： A technique is provided for use by a user terminal or mobile services switching center (MSC) for responding to a request to switch an on-going call from speech mode to multimedia mode within a wireless communication network conFig.d to automatically disconnect a call if a requested mode switch is not confirmed within a predetermined period of time specified by a call drop timer. In one example, the terminal or MSC activities an automatic response timer upon receipt of a request from a user to switch an on-going call from speech to multimedia, with the timer set shorter than the call drop timer. The user receiving the request is then prompted to accept or decline the request. If no response is received before expiration of the automatic response timer, the terminal or MSC automatically declines the request on behalf of the user so that the call drop timer does not expire.

摘要翻译： 提供了一种技术，用于由用户终端或移动业务交换中心（MSC）用于响应在无线通信网络conFig.d中将正在进行的呼叫从语音模式切换到多媒体模式的请求，以自动断开呼叫，如果 在由呼叫丢弃定时器指定的预定时间段内未确认所请求的模式切换。 在一个示例中，终端或MSC在接收到来自用户的请求时将活动自动响应定时器，以将正在进行的呼叫从语音切换到多媒体，其中定时器设置短于呼叫丢弃定时器。 然后，接收请求的用户被提示接受或拒绝该请求。 如果在自动响应定时器到期之前没有收到响应，则终端或MSC代表用户自动拒绝该请求，使得呼叫丢弃定时器不会过期。