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公开(公告)号：US20080033164A1
公开(公告)日：2008-02-07
申请号：US11484374
申请日：2006-07-10
IPC分类号： C07D487/22 , C07C309/00
CPC分类号： C01B21/086 , C01D15/00 , C07C211/63 , C07C381/12
摘要： Novel compositions are provided containing a compound represented by the formula YOSF5 or ZOSF5, where: (a) Y is: (i) an organic cation other than (Me2N)3S+ or (ii) an inorganic cation, provided that when Y is the inorganic cation, the composition further includes a complexing agent; and (b) Z is C1-20 alkyl, aryl, cycloalkyl, combinations thereof, or analogues thereof containing at least one heteroatom, provided that the compound represented by the formula ZOSF5 is a molecular compound. Processes of making the cationic compounds are disclosed as are processes for using the compositions containing cationic compounds in nucleophilic replacement reactions to prepare the compositions containing molecular compounds including the OSF5 group.
摘要翻译： 提供含有由式YOSF 5或ZOSF 5 N表示的化合物的新型组合物，其中：（a）Y为：（i）除（Me < 或（ii）无机阳离子，条件是当Y是无机阳离子时，该组合物还包含络合剂（例如，N，N-二甲基氨基乙基） ; 和（b）Z为含有至少一个杂原子的C 1-20烷基，芳基，环烷基，其组合或其类似物，条件是由式ZOSF 5表示的化合物， SUB>是分子化合物。 公开了制备阳离子化合物的方法，就是使用含有阳离子化合物的组合物在亲核置换反应中制备含有分子化合物的组合物的方法，包括OSF 5组。
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公开(公告)号：US06455744B1
公开(公告)日：2002-09-24
申请号：US09985786
申请日：2001-11-06
IPC分类号： C07C2522
CPC分类号： C07C49/697 , C07B39/00 , C07C17/18 , C07C17/23 , C07C25/22 , C07C45/512 , C07C23/18
摘要： A method of preparing vicinal difluoro aromatic compounds in high yield from hydroxy aromatic compounds and a method of preparing intermediates thereof. The hydroxy aromatic compound can be a mono-, bi- or tricyclic aromatic in which the rings are separate or fused. One or more of the rings can contain heteroatoms, such as oxygen, nitrogen, or sulfur, and can contain one or more substitutions, in addition to the hydroxy substitution.
摘要翻译： 由羟基芳香族化合物高产率制备邻位二氟芳族化合物的方法及其制备中间体的方法。 羟基芳族化合物可以是单环，双环或三环芳族，其中环是分开的或稠合的。 除了羟基取代之外，一个或多个环可以含有杂原子，例如氧，氮或硫，并且可以包含一个或多个取代。
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公开(公告)号：US06207860B1
公开(公告)日：2001-03-27
申请号：US08939635
申请日：1997-09-29
IPC分类号： C07C31300
CPC分类号： C07C381/00 , C07D207/48 , C07D223/30
摘要： Diaryl-, dialkoxyalkyl-, alkylalkoxyalkyl-, arylalkoxyalkyl- and cyclic aminosulfur trifluorides fluorinating agents are disclosed.
摘要翻译： 公开了二芳基 - ，二烷氧基烷基 - ，烷基烷氧基烷基 - ，芳基烷氧基烷基 - 和环状氨基三氟化硫氟化剂。
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公开(公告)号：US09321881B2
公开(公告)日：2016-04-26
申请号：US13208449
申请日：2011-08-12
申请人： Gauri Sankar Lal , Kristen Elaine Minnich , Pritesh G. Patel , Gamini Ananda Vedage , Garret C. Lau
发明人： Gauri Sankar Lal , Kristen Elaine Minnich , Pritesh G. Patel , Gamini Ananda Vedage , Garret C. Lau
IPC分类号： C08G59/50 , C07C211/46 , C07C211/55 , C09K3/00 , B05D3/00
CPC分类号： C08G59/5033 , C07C211/46 , C07C211/55 , C09K3/00
摘要： A liquid methylenedianiline product is disclosed. The product is produced by reacting aniline and ethylaniline with formaldehyde with an amine to formaldehyde ratio greater than about 2:1. The resulting reaction product is a liquid mixture of methylenedianiline, monoethyl methylenedianiline, and diethyl methylenedianiline having a viscosity of less than about 1000 cps at 40° C.
摘要翻译： 公开了一种液体亚甲基二苯胺产物。 该产物通过苯胺和乙基苯胺与甲醛反应制得，胺与甲醛的比例大于约2:1。 所得反应产物是在40℃下具有小于约1000cps的亚甲基二苯胺，单乙基亚甲基二苯胺和二乙基亚甲基二苯胺的液体混合物。
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公开(公告)号：US20080312464A1
公开(公告)日：2008-12-18
申请号：US11761447
申请日：2007-06-12
IPC分类号： C07C313/10
CPC分类号： C07C381/00 , C07C2601/14 , C07C2601/16
摘要： A compound comprising at least one alicyclic or heteroalicyclic ring structure, the ring structure comprising a ring of about four to about eight atoms, wherein at least two adjacent atoms of the ring are carbon atoms and at least one of said carbon atoms is covalently bonded to an —OSF5 functional group and either is bonded to a moiety selected from hydrogen; halogen; C1-C6 substituted or unsubstituted, branched or straight alkyl; C5-C7 substituted or unsubstituted aryl or heteroaryl; C3-C8 aliphatic cyclic; OSF5; or is a member of a fused, bridged, fused-bridged, or spirocyclic ring system; provided that if the moiety is fluorine, then at least one of the other ring atoms are bonded to an atom or functional group other than fluorine; as well as methods for making the same.
摘要翻译： 包含至少一个脂环族或杂脂环结构的化合物，所述环结构包含约4至约8个原子的环，其中所述环的至少两个相邻原子是碳原子，并且所述碳原子中的至少一个共价键合到 一个-OSF 5官能团并且可以键合到选自氢的部分; 卤素; C1-C6取代或未取代的，支链或直链烷基; C5-C7取代或未取代的芳基或杂芳基; C3-C8脂肪族环状; OSF5; 或是稠合，桥连，稠合桥连或螺环体系的成员; 条件是如果该部分是氟，则其它环原子中的至少一个键合到除氟以外的原子或官能团; 以及制作相同的方法。
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![Fluorinated alkyl substituted-thieno[3,4-]thiophene monomers and polymers therefrom](/abs-image/US/2008/10/07/US07432340B2/abs.jpg.150x150.jpg)
16.发明授权Fluorinated alkyl substituted-thieno[3,4-]thiophene monomers and polymers therefrom 有权氟化烷基取代噻吩并[3,4-b]噻吩单体及其聚合物公开(公告)号：US07432340B2
公开(公告)日：2008-10-07
申请号：US11128538
申请日：2005-05-13
申请人： Steffen Zahn , Gauri Sankar Lal , William Franklin Burgoyne, Jr. , Kristen Elaine Minnich , Andrew Francis Nordquist , Lloyd Mahlon Robeson , Francis Joseph Waller
发明人： Steffen Zahn , Gauri Sankar Lal , William Franklin Burgoyne, Jr. , Kristen Elaine Minnich , Andrew Francis Nordquist , Lloyd Mahlon Robeson , Francis Joseph Waller
CPC分类号： C08G61/123 , C08G61/126
摘要： Partially and fully fluorinated alkyl substituted thienothiophene monomers (and polymers thereof) wherein the monomers are represented by the formula: wherein R is a partially or fully fluorinated primary, secondary or tertiary alkyl having from 1 to 8 carbon atoms; and X and X′ are independently selected from the group consisting of H, F, Cl, Br, I, MgCl, MgBr, Mgl, Sn(R′)3, CH═CHR″, —OR″, —COOR″, —S—COR″, —B(OR″)2, —COR″, —C≡CH, and a polymerizable cyclic pi-conjugated carbon-ring structure optionally comprising S, N or O heteroatoms; wherein R′ is a primary, secondary or tertiary alkyl having from 1 to 6 carbon atoms, and R″ is H or a primary, secondary or tertiary alkyl having from 1 to 6 carbon atoms.
摘要翻译： 部分和完全氟化的烷基取代的噻吩并噻吩单体（及其聚合物），其中单体由下式表示：其中R是具有1至8个碳原子的部分或完全氟化的伯，仲或叔烷基; 并且X和X'独立地选自H，F，Cl，Br，I，MgCl，MgBr，MgI，Sn（R'）3，CH-CHR“， - OR“，-COOR”，-S-COR“，-B（OR”）2，-COR“，-C≡CH和可聚合的环状π-共轭碳 任选地包含S，N或O杂原子的环结构; 其中R'是具有1至6个碳原子的伯，仲或叔烷基，R“是H或具有1至6个碳原子的伯，仲或叔烷基。
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公开(公告)号：US07166755B2
公开(公告)日：2007-01-23
申请号：US10954719
申请日：2004-09-30
IPC分类号： C07C19/08
CPC分类号： C07C381/00 , C07C2601/14 , C07F5/027 , C07F7/081
摘要： This invention relates to 2-pentafluorosulfanylnapthalene, substituted derivatives thereof and to a process for producing naphthalene carrying an SF5 group. A 3-step process is employed wherein 1,4-dihydronaphthalene is reacted with pentafluorosulfanyl halide. Next the resulting 3-halo-2-pentafluorosulfanylnaphthalene or derivative is converted to 2-pentafluorosulfanyl-1,4-dihydronaphthalene or derivative by treatment with a base and subsequently transformed into pentafluorosulfanylnaphthalene by removing hydrogen atoms.
摘要翻译： 本发明涉及2-五氟硫烷基萘及其取代衍生物，以及一种生产含有SF 5 H 5基团的萘的方法。 使用其中1,4-二氢萘与五氟硫烷基卤化物反应的三步法。 接下来，通过用碱处理将所得3-卤代-2-五氟硫烷基萘或其衍生物转化为2-五氟硫烷基-1,4-二氢萘或衍生物，随后通过除去氢原子转化成五氟硫烷基萘。
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公开(公告)号：US06706933B2
公开(公告)日：2004-03-16
申请号：US10334183
申请日：2002-12-30
IPC分类号： C07C2522
CPC分类号： C07C49/697 , C07B39/00 , C07C17/18 , C07C17/23 , C07C25/22 , C07C45/512 , C07C23/18
摘要： A method of preparing vicinal difluoro aromatic compounds in high yield from hydroxy aromatic compounds and a method of preparing intermediates thereof. The hydroxy aromatic compound can be a mono-, bi- or tricyclic aromatic in which the rings are separate or fused. One or more of the rings can contain heteroatoms, such as oxygen, nitrogen, or sulfur, and can contain one or more substitutions, in addition to the hydroxy substitution.
摘要翻译： 由羟基芳香族化合物高产率制备邻位二氟芳族化合物的方法及其制备中间体的方法。 羟基芳族化合物可以是单环，双环或三环芳族，其中环是分开的或稠合的。 除了羟基取代之外，一个或多个环可以含有杂原子，例如氧，氮或硫，并且可以包含一个或多个取代。
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公开(公告)号：US06222064B1
公开(公告)日：2001-04-24
申请号：US09483751
申请日：2000-01-14
申请人： Gauri Sankar Lal , Guido Peter Pez
发明人： Gauri Sankar Lal , Guido Peter Pez
IPC分类号： C07C17013
CPC分类号： C07C319/14 , C07B39/00 , C07C17/093 , C07C17/16 , C07C17/18 , C07C17/38 , C07C45/63 , C07C51/60 , C07C67/307 , C07C253/30 , C07C2601/14 , C07C2601/16 , C07C2601/18 , C07C23/10 , C07C22/08 , C07C23/16 , C07C49/457 , C07C69/63 , C07C323/03 , C07C255/10
摘要： A fluorination method of oxygen and halogen sites with diaryl-, dialkoxyalkyl-, alkylalkoxyalkyl-, arylalkoxyalkyl- and cyclic aminosulfur trifluorides fluorinating reagents is disclosed.
摘要翻译： 公开了具有二芳基 - ，二烷氧基烷基 - 烷基烷氧基烷基 - ，芳基烷氧基烷基 - 和环状氨基三氟化硫氟化试剂的氧和卤素位点的氟化方法。
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公开(公告)号：US09233063B2
公开(公告)日：2016-01-12
申请号：US12967752
申请日：2010-12-14
摘要： A polymeric composition is disclosed for use in personal care products. The composition is, at room temperature, a solid solution of a long-chain alcohol having ten to fifty carbon atoms and a polyalkyl[meth]acrylate polymer having some alkyl side chains pendant the ester group having ten to thirty carbon atoms and other alkyl side chains pendant the ester group having one to eight carbon atoms. The polymer can be formed by a transesterification reaction of a polyalkyl[meth]acrylate and the long chain alcohol in the presence of a catalyst.
摘要翻译： 公开了用于个人护理产品的聚合物组合物。 该组合物在室温下为具有10至50个碳原子的长链醇的固体溶液和具有一些烷基侧链的聚（甲基）丙烯酸烷基酯聚合物侧链，其具有10至30个碳原子的酯基和其它烷基侧 链侧链具有1-8个碳原子的酯基。 聚合物可以通过在催化剂存在下由[甲基]丙烯酸聚烷基酯和长链醇进行酯交换反应形成。
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