Polyamic acid, polyimide, and method for manufacturing graphite sheet
    12.
    发明授权
    Polyamic acid, polyimide, and method for manufacturing graphite sheet 有权
    聚酰胺酸,聚酰亚胺和石墨片的制造方法

    公开(公告)号:US09593207B2

    公开(公告)日:2017-03-14

    申请号:US14172532

    申请日:2014-02-04

    Abstract: Disclosed is a method of fabricating a graphite sheet, including: polymerizing diamines and a dianhydride to form a polyamic acid. The polyamic acid is solvent casted on a substrate and hot baked to form a polyamic acid film or gel film. The polyamic acid film or gel film is biaxially stretched at a high temperature imidization or chemical imidization to form the polyimide film. The polyimide film is then carbonized and graphitized to form a graphite sheet. The diamines include a diamine of Formula 1 and a diamine of Formula 2, and the dianhydride includes a dianhydride of Formulae 3, Formula 4, Formula 5, Formula 6, Formula 7, Formula 8, Formula 9, or combinations thereof.

    Abstract translation: 公开了一种制造石墨片的方法,包括:聚合二胺和二酐以形成聚酰胺酸。 将聚酰胺酸溶剂浇铸在基材上并热烘烤以形成聚酰胺酸膜或凝胶膜。 聚酰胺酸膜或凝胶膜在高温酰亚胺化或化学酰亚胺化下双轴拉伸,形成聚酰亚胺膜。 然后将聚酰亚胺膜碳化并石墨化以形成石墨片。 二胺包括式1的二胺和式2的二胺,二酐包括式3,式4,式5,式6,式7,式8,式9或其组合的二酐。

    Aqueous-phase catalyst compositions and method for preparing polyphenylene ether
    14.
    发明授权
    Aqueous-phase catalyst compositions and method for preparing polyphenylene ether 有权
    水相催化剂组合物和聚苯醚的制备方法

    公开(公告)号:US09359475B1

    公开(公告)日:2016-06-07

    申请号:US14585906

    申请日:2014-12-30

    CPC classification number: C08G65/44

    Abstract: An aqueous-phase catalyst composition including a metal ion including copper, nickel, manganese or iron and a water-soluble linear polymer having a molecular weight ranging from 1,000 to 20,000 is provided. The metal ion and the water-soluble linear polymer have a weight ratio of 1:1 to 1:5. A method for preparing polyphenylene ether including providing the disclosed aqueous-phase catalyst composition and adding phenolic monomers to the aqueous-phase catalyst composition to proceed to a polymerization reaction to prepare polyphenylene ether is also provided.

    Abstract translation: 提供包含铜,镍,锰或铁的金属离子和分子量为1,000〜20,000的水溶性线性聚合物的水相催化剂组合物。 金属离子和水溶性线性聚合物的重量比为1:1至1:5。 还提供了一种制备聚苯醚的方法,其包括提供所公开的水相催化剂组合物并将酚单体加入到水相催化剂组合物中以进行聚合反应以制备聚苯醚。

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