Method of making a cellulose acetate low density microcellular foam
    11.
    发明授权
    Method of making a cellulose acetate low density microcellular foam 失效
    制造醋酸纤维素低密度微孔泡沫的方法

    公开(公告)号:US4118449A

    公开(公告)日:1978-10-03

    申请号:US749205

    申请日:1976-12-09

    Applicant: James A. Rinde

    Inventor: James A. Rinde

    Abstract: Low-density microcellular foam having a cell size of not greater than 2 .mu.m and method of making by dissolving cellulose acetate in an acetone-based solvent, gelling the solution in a water bath maintained at 0-10.degree. C for a selected period of time to allow impurities to diffuse out, freezing the gel, and then freeze-drying wherein water and solvents sublime and the gel structure solidifies into low-density microcellular foam. The foam has a density of 0.065 to 0.6.times.10.sup.3 kg/m.sup.3 and cell size of about 0.3 to 2 .mu.m. The small cell size foam is particularly adaptable for encapsulation of laser targets.

    Abstract translation: 细胞尺寸不大于2μm的低密度微孔泡沫体和通过将乙酸纤维素溶解在丙酮溶剂中制备的方法,将溶液凝胶保持在0-10℃的水浴中一段选定时间 时间允许杂质扩散出来,冷冻凝胶,然后冷冻干燥,其中水和溶剂升华,凝胶结构固化成低密度微孔泡沫。 泡沫体的密度为0.065〜0.6×10 3 kg / m 3,电池尺寸为0.3〜2μm左右。 小泡沫泡沫特别适用于激光靶的封装。

    Method of making metal-doped organic foam products
    15.
    发明授权
    Method of making metal-doped organic foam products 失效
    制造金属掺杂有机泡沫产品的方法

    公开(公告)号:US4261937A

    公开(公告)日:1981-04-14

    申请号:US26505

    申请日:1979-04-03

    Applicant: James A. Rinde

    Inventor: James A. Rinde

    CPC classification number: C08J9/28 C08J2201/0546

    Abstract: Organic foams having a low density and very small cell size and method forroducing same in either a metal-loaded or unloaded (nonmetal loaded) form are described. Metal-doped foams are produced by soaking a polymer gel in an aqueous solution of desired metal salt, soaking the gel successively in a solvent series of decreasing polarity to remove water from the gel and replace it with a solvent of lower polarity with each successive solvent in the series being miscible with the solvents on each side and being saturated with the desired metal salt, and removing the last of the solvents from the gel to produce the desired metal-doped foam having desired density cell size, and metal loading. The unloaded or metal-doped foams can be utilized in a variety of applications requiring low density, small cell size foam. For example, rubidium-doped foam made in accordance with the invention has utility in special applications, such as in x-ray lasers.

    Abstract translation: 描述了具有低密度和非常小的泡孔尺寸的有机泡沫体以及用于以金属加载或卸载(非金属加载)形式生产的有机泡沫体。 通过将聚合物凝胶浸渍在所需金属盐的水溶液中来制备金属掺杂的泡沫,将凝胶依次以极性降低的溶剂系列浸泡以从凝胶中除去水,并用每个相继的溶剂代替低极性的溶剂 该系列与每一侧上的溶剂混溶并被所需的金属盐饱和,并从凝胶中除去最后的溶剂以产生具有所需密度单元尺寸和金属负载的所需金属掺杂泡沫。 无负载或金属掺杂的泡沫可用于需要低密度,小泡孔泡沫的各种应用中。 例如,根据本发明制成的掺杂铷的泡沫可用于特殊应用中,例如在x射线激光器中。

    Use of 2,5-dimethyl-2,5-hexane diamine as a curing agent for epoxy resins
    16.
    发明授权
    Use of 2,5-dimethyl-2,5-hexane diamine as a curing agent for epoxy resins 失效
    使用2,5-二甲基-2,5-己二胺作为环氧树脂的固化剂

    公开(公告)号:US4252936A

    公开(公告)日:1981-02-24

    申请号:US5940

    申请日:1979-01-24

    CPC classification number: C08G59/5033 C08G59/5006

    Abstract: Primary diamines of the formula ##STR1## wherein R is a straight chain saturated hydrocarbon of 2 to 4 carbons, a disubstituted benzene ring, or disubstituted dibenzo methane for use as a curing agent for epoxy resins. These curing agents can be used to form epoxy resin mixtures useful in filament winding and pre-impregnated fiber molding and in formulating film adhesives, powder coatings and molding powders. The epoxy mixtures form for such uses as room temperature non-reacting, intermediate stable state which has a latent cross-linking capability.

    Abstract translation: 其中R是2至4个碳原子的直链饱和烃,二取代苯环,或用作环氧树脂固化剂的二取代二苯甲烷的伯胺二胺。 这些固化剂可用于形成用于纤维缠绕和预浸纤维成型以及配制膜粘合剂,粉末涂料和模塑粉末的环氧树脂混合物。 环氧混合物形成用于室温非反应,具有潜在交联能力的中间稳定状态的用途。

    Low-density microcellular foam and method of making same
    17.
    发明授权
    Low-density microcellular foam and method of making same 失效
    低密度微孔泡沫及其制备方法

    公开(公告)号:US4012265A

    公开(公告)日:1977-03-15

    申请号:US609641

    申请日:1975-09-02

    Applicant: James A. Rinde

    Inventor: James A. Rinde

    Abstract: Low-density microcellular foam having a cell size of not greater than 2 .mu.m and method of making by dissolving cellulose acetate in an acetone-based solvent, gelling the solution in a water bath maintained at 0.degree.-10.degree. C for a selected period of time to allow impurities to diffuse out, freezing the gel, and then freeze-drying wherein water and solvents sublime and the gel structure solidifies into low-density microcellular foam. The foam has a density of 0.065 to 0.6.times.10.sup.3 kg/m.sup.3 and cell size of about 0.3 to 2 .mu.m. The small cell size foam is particularly applicable for encapsulation of laser targets.

    Abstract translation: 细胞尺寸不大于2μm的低密度微孔泡沫体和通过将乙酸纤维素溶解在丙酮类溶剂中制备的方法,将溶液凝胶保持在0-10℃的水浴中选定的时间 的时间以允许杂质扩散出来,冷凝凝胶,然后冷冻干燥,其中水和溶剂升华,凝胶结构固化成低密度微孔泡沫。 泡沫体的密度为0.065〜0.6×10 3 kg / m 3,电池尺寸为0.3〜2μm左右。 小泡沫泡沫特别适用于激光靶材的封装。

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