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公开(公告)号：US20110180755A1
公开(公告)日：2011-07-28
申请号：US12678006
申请日：2008-09-26
申请人： Yoshifumi Adachi , Kazushi Torii , Yusuke Watanabe , Taishi Kobayashi , Toshimasa Kitayama , Seiichi Suzuki , Atsuro Yoneda
发明人： Yoshifumi Adachi , Kazushi Torii , Yusuke Watanabe , Taishi Kobayashi , Toshimasa Kitayama , Seiichi Suzuki , Atsuro Yoneda
IPC分类号： C09K3/00
CPC分类号： C08F8/32 , B01J20/262 , B01J20/267 , C08F220/06 , C08F222/1006 , C08G73/02 , C08K5/09 , C08L33/02 , C08L79/02
摘要： The present invention provides a water absorbing agent, including: water absorbent resin particles; and a modified cationic polymer compound containing a primary amino group and/or a secondary amino group, the modified cationic polymer compound being obtained by reacting, with a modifying agent, a cationic polymer compound containing the primary amino group and/or the secondary amino group, and the modifying agent containing two or more carbon atoms continuously linked, and one reactive group which reacts with the primary amino group and/or the secondary amino group. The present invention further provides a method for producing a water absorbing agent including water absorbent resin particles, the method including the step (i) of mixing the water absorbent resin particles with a modified cationic polymer compound.
摘要翻译： 本发明提供一种吸水剂，包括：吸水性树脂颗粒; 和含有伯氨基和/或仲氨基的改性阳离子聚合物化合物，所述改性阳离子聚合物化合物通过使改性剂与含有伯氨基和/或仲氨基的阳离子聚合物化合物 和包含连续连接的两个或更多个碳原子的改性剂，以及与伯氨基和/或仲氨基反应的一个反应性基团。 本发明还提供一种吸水性树脂粒子的吸水剂的制造方法，其特征在于，包括将吸水性树脂粒子与改性阳离子性高分子化合物混合的工序（i）。
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12.发明授权公开(公告)号：US07495056B2
公开(公告)日：2009-02-24
申请号：US11449656
申请日：2006-06-09
CPC分类号： A61F13/531 , A61F2013/530708 , A61F2013/530788 , A61L15/24 , A61L15/60 , B01J20/26 , B01J20/261 , B01J20/267 , B01J2220/68 , C08L33/02 , C08L3/02
摘要： The present invention provides: a novel water-absorbing agent, which exhibits an excellent absorption capacity under a load (AAP), gel layer liquid permeation rate under a load (FRUP), saline flow conductivity (SFC), and shape-maintaining property and ball burst strength (BBS) of a swollen water-absorbing agent aggregate, and excellent persistency of these effects for a long time. The water-absorbing agent, which comprises a polymer obtained by a process including the steps of polymerizing and then crosslinking a monomer including acrylic acid and/or a salt thereof, with the water-absorbing agent being characterized by: (1) exhibiting a free swelling capacity of not less than 23 g/g (GV), a gel deformation of not more than 12.5 cm under a short-time load (0.5 hrPT), and a gel deformation deterioration of not more than 3.5 cm under a load with the passage of time (ΔPT); (2) exhibiting a free swelling capacity of not less than 23 g/g (GV), a ball burst strength of not less than 80 gf (BBS), and a deterioration of ball burst strength of not more than 40% (DBBS); or (3) exhibiting a free swelling capacity of not less than 23 g/g (GV), an absorption capacity of not less than 20 g/g under a load of 4.9 kPa (AAP), and a gel deformation of not more than 12.5 cm under a load (16 hrPT).
摘要翻译： 本发明提供：在负荷（AAP），载荷下的凝胶层液体渗透速率（FRUP），盐水导电率（SFC）和形状维持性等方面表现出优异的吸收容量的新型吸水剂， 膨胀吸水剂聚集体的球破裂强度（BBS），长时间保持这些效果的持久性。 包含通过包括使包含丙烯酸和/或其盐在内的单体聚合然后将其与所述吸水剂交联的方法获得的聚合物的吸水剂的特征在于：（1） 溶胀能力不小于23g / g（GV），在短时间负荷（0.5hrPT）下凝胶变形不超过12.5cm，凝胶变形劣化不大于3.5cm， 时间流逝（DeltaPT）; （2）表现出不小于23g / g（GV）的游离膨胀能力，不高于80gf（BBS）的球破裂强度和不大于40％的球爆裂强度的劣化（DBBS） ; 或（3）在4.9kPa（AAP）的载荷下表现出不小于23g / g（GV）的游离溶胀能力，不低于20g / g的吸收能力，凝胶变形不大于 负荷为12.5厘米（16小时）。
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13.发明授权Pressure-resistant absorbent resin, disposable diaper using the resin, and absorbent resin, and method for production thereof 失效耐压吸收性树脂，使用树脂的一次性尿布和吸收性树脂，及其制造方法公开(公告)号：US06184433B2
公开(公告)日：2001-02-06
申请号：US09058023
申请日：1998-04-10
IPC分类号： A61F1315
CPC分类号： A61L15/60
摘要： This invention is directed to a disposable diaper using a pressure-resistant absorbent resin manifesting a ratio of water absorption capacity under pressure of 30 g/g or more to artificial urine under a load of 50 g/cm2, and a pressure-resistant absorption ratio of 0.6 or more, wherein the pressure resistant absorption ratio is defined as the ratio of the ratio of water absorption capacity under high pressure to artificial urine under a load of 100 g/cm2 to a ratio of water absorption capacity under pressure to artificial urine under a load of 50 g/cm2.
摘要翻译： 本发明涉及一种使用耐压吸收树脂的一次性尿布，其表现出在50g / cm 2负荷下人造尿液在30g / g以上的压力下的吸水倍率与耐压吸收率 为0.6以上，其中耐压吸收率定义为在负荷为100g / cm 2的情况下，高压下的人造尿与人造尿之间的吸水能力与人造尿下的吸水能力的比例 负荷为50g / cm 2。
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14.发明授权
公开(公告)号：US5853867A
公开(公告)日：1998-12-29
申请号：US713866
申请日：1996-09-13
CPC分类号： A61L15/60 , Y10S428/913 , Y10T428/249986 , Y10T442/277 , Y10T442/2885 , Y10T442/2893 , Y10T442/2918
摘要： This invention concerns an absorbent composite a supporting member and a cationic absorbent polymer and anionic absorbent polymer particles fixed to the supporting member. This absorbent composite excels in absorbing capacity under pressure, vertical aspiration power, and flexibility and suffers only sparing exfoliation of an absorbent polymer. This invention further concerns an absorbent composite which contains an absorbent polymer in an amount of at least 30% by weight based on the total weight of the absorbent composite and, after absorbing a liquid, shows a value of not less than 3 for the expansion anisotropy specified by the following formula. Expansion anisotropy=(Ez/Ex+Ez/Ey)/2 (wherein Ex, Ey, and Ez respectively represent coefficient of liner expansion in the directions of X axis, Y axis, and Z axis) and an absorbent article using the absorbent composite. This invention permits production of a novel absorbent composite which suffers no leakage and excels in water absorbing power, water retaining power, and flexibility and an absorbent article using the absorbent composite.
摘要翻译： 本发明涉及一种吸收性复合材料，其是支撑构件和阳离子吸收聚合物以及固定在支撑构件上的阴离子吸收性聚合物颗粒。 这种吸收性复合材料在压力，垂直抽吸力和柔韧性下的吸收能力优异，并且仅仅吸收聚合物的剥落。 本发明还涉及一种吸收性复合材料，其含有吸收性聚合物，该吸收性聚合物的量相对于吸收性复合材料的总重量为至少30重量％，并且在吸收液体之后，对于膨胀各向异性显示不小于3的值 由以下公式指定。 膨胀各向异性=（Ez / Ex + Ez / Ey）/ 2（其中，Ex，Ey和Ez分别表示在X轴，Y轴和Z轴方向上的衬垫膨胀系数）和使用吸收性复合材料 。 本发明允许生产不会发生泄漏并且吸水力，保水力和柔软性优异的吸收性复合材料，以及使用吸收性复合体的吸收性物品。
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15.发明申请公开(公告)号：US20060229413A1
公开(公告)日：2006-10-12
申请号：US11449656
申请日：2006-06-09
IPC分类号： C08L77/00
CPC分类号： A61F13/531 , A61F2013/530708 , A61F2013/530788 , A61L15/24 , A61L15/60 , B01J20/26 , B01J20/261 , B01J20/267 , B01J2220/68 , C08L33/02 , C08L3/02
摘要： The present invention provides: a novel water-absorbing agent, which exhibits an excellent absorption capacity under a load (AAP), gel layer liquid permeation rate under a load (FRUP), saline flow conductivity (SFC), and shape-maintaining property and ball burst strength (BBS) of a swollen water-absorbing agent aggregate, and excellent persistency of these effects for a long time. The water-absorbing agent, which comprises a polymer obtained by a process including the steps of polymerizing and then crosslinking a monomer including acrylic acid and/or a salt thereof, with the water-absorbing agent being characterized by: (1) exhibiting a free swelling capacity of not less than 23 g/g (GV), a gel deformation of not more than 12.5 cm under a short-time load (0.5 hrPT), and a gel deformation deterioration of not more than 3.5 cm under a load with the passage of time (ΔPT); (2) exhibiting a free swelling capacity of not less than 23 g/g (GV), a ball burst strength of not less than 80 gf (BBS), and a deterioration of ball burst strength of not more than 40% (DBBS); or (3) exhibiting a free swelling capacity of not less than 23 g/g (GV), an absorption capacity of not less than 20 g/g under a load of 4.9 kPa (AAP), and a gel deformation of not more than 12.5 cm under a load (16 hrPT).
摘要翻译： 本发明提供：在负荷（AAP），载荷下的凝胶层液体渗透速率（FRUP），盐水导电率（SFC）和形状维持性等方面表现出优异的吸收容量的新型吸水剂， 膨胀吸水剂聚集体的球破裂强度（BBS），长时间保持这些效果的持久性。 包含通过包括使包含丙烯酸和/或其盐在内的单体聚合然后将其与所述吸水剂交联的方法获得的聚合物的吸水剂的特征在于：（1） 溶胀能力不小于23g / g（GV），在短时间负荷（0.5hrPT）下凝胶变形不超过12.5cm，凝胶变形劣化不大于3.5cm， 时间流逝（DeltaPT）; （2）表现出不小于23g / g（GV）的游离膨胀能力，不高于80gf（BBS）的球破裂强度和不大于40％的球爆裂强度的劣化（DBBS） ; 或（3）在4.9kPa（AAP）的载荷下表现出不小于23g / g（GV）的游离溶胀能力，不低于20g / g的吸收能力，凝胶变形不大于 负荷为12.5厘米（16小时）。
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公开(公告)号：US07098284B2
公开(公告)日：2006-08-29
申请号：US10053659
申请日：2002-01-24
IPC分类号： C08F2/10
CPC分类号： A61F13/531 , A61F2013/530708 , A61F2013/530788 , A61L15/24 , A61L15/60 , B01J20/26 , B01J20/261 , B01J20/267 , B01J2220/68 , C08L33/02 , C08L3/02
摘要： The present invention provides: a novel water-absorbing agent, which exhibits an excellent absorption capacity under a load (AAP), gel layer liquid permeation rate under a load (FRUP), saline flow conductivity (SFC), and shape-maintaining property and ball burst strength (BBS) of a swollen water-absorbing agent aggregate, and excellent persistency of these effects for a long time. The water-absorbing agent, which comprises a polymer obtained by a process including the steps of polymerizing and then crosslinking a monomer including acrylic acid and/or a salt thereof, with the water-absorbing agent being characterized by: (1) exhibiting a free swelling capacity of not less than 23 g/g (GV), a gel deformation of not more than 12.5 cm under a short-time load (0.5 hrPT), and a gel deformation deterioration of not more than 3.5 cm under a load with the passage of time (ΔPT); (2) exhibiting a free swelling capacity of not less than 23 g/g (GV), a ball burst strength of not less than 80 gf (BBS), and a deterioration of ball burst strength of not more than 40% (DBBS); or (3) exhibiting a free swelling capacity of not less than 23 g/g (GV), an absorption capacity of not less than 20 g/g under a load of 4.9 kPa (AAP), and a gel deformation of not more than 12.5 cm under a load (16 hrPT).
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17.发明授权
公开(公告)号：US6001911A
公开(公告)日：1999-12-14
申请号：US860445
申请日：1997-06-26
CPC分类号： A61F13/531 , A61L15/60 , C08J3/075 , A61F2013/15357 , A61F2013/15463 , A61F2013/530583 , A61F2013/530708 , A61F2013/530715 , A61F2013/530744
摘要： A water content of a water-containing gel of a hydrophilic cross-linked polymer is reduced by pressuring (calendaring) it. Then, a gel composition including, for example, a water-containing gel including cross-linked poly(meth)acrylic acid (salt), glycerol (polyhydric alcohol) and polyester fibers (auxiliary forming material), etc., is fed to a drum dryer on an upstream side of a pressurizing roller. Then, the resulting gel composition is pressurized (calendared) heated by a pressurizing roller to be formed into a sheet. As a result, a sheet-like absorbent material having at least one smooth surface can be obtained. The absorbent material resulting from the described method shows excellent properties and especially absorbing properties such as absorbing rate, absorbency under load, and shape retaining properties.
摘要翻译： PCT No.PCT / JP96 / 03191 Sec。 371日期：1997年6月26日 102（e）日期1996年6月26日PCT提交1996年10月31日PCT公布。 公开号WO97 / 16492 日期1997年5月9日亲水性交联聚合物的含水凝胶的含水量通过加压（压延）而降低。 然后，将包含交联聚（甲基）丙烯酸（盐），甘油（多元醇）和聚酯纤维（辅助成形材料）等的含水凝胶等的凝胶组合物供给到 滚筒式干燥机在加压辊的上游侧。 然后，将所得凝胶组合物加压（压延），由加压辊加热以形成片材。 结果，可以获得具有至少一个平滑表面的片状吸收材料。 由所述方法得到的吸收材料显示出优异的性能，特别是吸收速率，负载下的吸收性和形状保持性等吸收性能。
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公开(公告)号：US08247491B2
公开(公告)日：2012-08-21
申请号：US10544348
申请日：2004-02-06
申请人： Kazushi Torii , Yoshiro Mitsukami , Motohiro Imura , Taku Iwamura , Toshimasa Kitayama , Kenji Kadonaga , Hiroki Inoue , Koji Miyake , Kozo Nogi , Masatoshi Nakamura , Shigeru Sakamoto , Sayaka Machida
发明人： Kazushi Torii , Yoshiro Mitsukami , Motohiro Imura , Taku Iwamura , Toshimasa Kitayama , Kenji Kadonaga , Hiroki Inoue , Koji Miyake , Kozo Nogi , Masatoshi Nakamura , Shigeru Sakamoto , Sayaka Machida
CPC分类号： A61L15/60
摘要： There are disclosed a water-absorbent resin composition and its production process, wherein the water-absorbent resin composition causes little gel-blocking and is excellent in the liquid permeability and liquid diffusibility and is high also in the absorption performances and further is strong also against the physical damage; and there are further disclosed a water-absorbent resin composition and its production process, wherein the water-absorbent resin composition has the following further advantages, in addition to the above, of involving little segregation of the metal compound and further having a dust prevention effect. One of water-absorbent resin compositions according to the present invention is a water-absorbent resin composition comprising water-absorbent resin particles obtained by polymerizing a monomer including acrylic acid and/or its salt, with the composition having a mass-average particle diameter of 100 to 600 μm and comprising water-soluble polyvalent metal salt particles and the water-absorbent resin particles that have been surface-crosslinked.
摘要翻译： 公开了吸水性树脂组合物及其制造方法，其中吸水性树脂组合物几乎没有凝胶阻塞，并且液体渗透性和液体扩散性优异，并且吸收性能也高，并且还强 物理伤害; 并且还公开了一种吸水性树脂组合物及其制造方法，其中除了上述之外，吸水性树脂组合物具有以下进一步的优点，即涉及金属化合物几乎不偏析并且还具有防尘效果 。 根据本发明的吸水性树脂组合物之一是吸收性树脂组合物，其包含通过使包含丙烯酸和/或其盐的单体聚合而获得的吸水性树脂颗粒，其组成物的质量平均粒径为 100〜600μm，并且包含水溶性多价金属盐颗粒和表面交联的吸水性树脂颗粒。
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公开(公告)号：US20060073969A1
公开(公告)日：2006-04-06
申请号：US10544348
申请日：2004-02-06
申请人： Kazushi Torii , Yoshiro Mitsukami , Motohiro Imura , Taku Iwamura , Toshimasa Kitayama , Kenji Kadonaga , Hiroki Inoue , Koji Miyake , Kozo Nogi , Masatoshi Nakamura , Shigeru Sakamoto
发明人： Kazushi Torii , Yoshiro Mitsukami , Motohiro Imura , Taku Iwamura , Toshimasa Kitayama , Kenji Kadonaga , Hiroki Inoue , Koji Miyake , Kozo Nogi , Masatoshi Nakamura , Shigeru Sakamoto
IPC分类号： B01J20/00
CPC分类号： A61L15/60
摘要： There are disclosed a water-absorbent resin composition and its production process, wherein the water-absorbent resin composition causes little gel-blocking and is excellent in the liquid permeability and liquid diffusibility and is high also in the absorption performances and further is strong also against the physical damage; and there are further disclosed a water-absorbent resin composition and its production process, wherein the water-absorbent resin composition has the following further advantages, in addition to the above, of involving little segregation of the metal compound and further having a dust prevention effect. One of water-absorbent resin compositions according to the present invention is a water-absorbent resin composition comprising water-absorbent resin particles obtained by polymerizing a monomer including acrylic acid and/or its salt, with the composition having a mass-average particle diameter of 100 to 600 μm and comprising water-soluble polyvalent metal salt particles and the water-absorbent resin particles that have been surface-crosslinked.
摘要翻译： 公开了吸水性树脂组合物及其制造方法，其中吸水性树脂组合物几乎没有凝胶阻塞，并且液体渗透性和液体扩散性优异，并且吸收性能也高，并且还强 物理伤害; 并且还公开了一种吸水性树脂组合物及其制造方法，其中除了上述之外，吸水性树脂组合物具有以下进一步的优点，即涉及金属化合物几乎不偏析并且还具有防尘效果 。 根据本发明的吸水性树脂组合物之一是吸收性树脂组合物，其包含通过使包含丙烯酸和/或其盐的单体聚合而获得的吸水性树脂颗粒，其组成物的质量平均粒径为 100〜600μm，含有水溶性多价金属盐粒子和表面交联的吸水性树脂粒子。
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20.发明授权公开(公告)号：US07312278B2
公开(公告)日：2007-12-25
申请号：US10333614
申请日：2002-06-07
申请人： Yasuhisa Nakashima , Hiroyuki Ikeuchi , Yasuhiro Fujita , Makoto Nagasawa , Shigeru Sakamoto , Yorimichi Dairoku , Katsuyuki Wada , Shinichi Fujino , Toshimasa Kitayama , Kazuhisa Hitomi
发明人： Yasuhisa Nakashima , Hiroyuki Ikeuchi , Yasuhiro Fujita , Makoto Nagasawa , Shigeru Sakamoto , Yorimichi Dairoku , Katsuyuki Wada , Shinichi Fujino , Toshimasa Kitayama , Kazuhisa Hitomi
CPC分类号： A61L15/60
摘要： There is provided: a production process for a water-absorbing agent having stable properties in a short time; and a water-absorbing agent. The production process comprises the step of blending an acid-group-containing water-absorbent resin powder with a noncrosslinkable water-soluble inorganic base and/or an irreducible alkaline-metal-salt pH buffer and further with a dehydratable crosslinking agent reactable with the acid group, thereby subjecting the resin powder to crosslinking treatment, or comprises the step of blending an acid-group-containing water-absorbent resin powder with the above base and/or pH buffer and further with a crosslinking agent reactable with the acid group, thereby subjecting the resin powder to crosslinking treatment, wherein the resin powder has a weight-average particle diameter of 300 to 600 μm wherein the ratio of fine powders having particle diameters of not larger than 150 μm in the resin powder is not more than 10 weight %.
摘要翻译： 提供了一种在短时间内具有稳定性能的吸水剂的生产方法; 和吸水剂。 生产方法包括将含酸基的吸水性树脂粉末与不可交联的水溶性无机碱和/或不可还原的碱金属盐pH缓冲剂以及可与酸反应的可脱水交联剂 从而使树脂粉末进行交联处理，或者包括将含酸基的吸水性树脂粉末与上述碱和/或pH缓冲剂以及与酸基反应的交联剂进一步混合的步骤，由此 使树脂粉末进行交联处理，其中树脂粉末的重均粒径为300〜600μm，其中树脂粉末中粒径不大于150μm的细粉末的比率不大于10重量％ 。
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