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    Method of producing ceramic composite bodies
    11.
    发明授权
    Method of producing ceramic composite bodies 失效
    生产陶瓷复合体的方法

    公开(公告)号：US5299621A

    公开(公告)日：1994-04-05

    申请号：US762163

    申请日：1991-09-19

    Applicant: Terry D. Claar ,  Gerhard H. Schiroky ,  Donald P. Ripa ,  William B. Johnson

    Inventor： Terry D. Claar ,  Gerhard H. Schiroky ,  Donald P. Ripa ,  William B. Johnson

    IPC: C04B35/563 ,  C04B35/56 ,  C04B35/58 ,  C04B35/65 ,  C22C1/10 ,  B22D19/00

    CPC classification number: C04B35/563 ,  C04B35/5622 ,  C04B35/58071 ,  C04B35/58078 ,  C04B35/65 ,  C04B35/652

    Abstract: This invention relates generally to a novel method of preparing self-supporting bodies, and novel products made thereby. In its more specific aspects, this invention relates to a method for producing self-supporting bodies comprising one or more boron-containing compounds, e.g., a boride or a boride and a carbide, by reactive infiltration of molten parent metal into a preform comprising boron carbide or a boron donor material combined with a carbon donor material and, optionally, one or more inert fillers, to form the body. Specifically, a boron carbide material or combination of a boron donor material and a carbon donor material, and in either case, optionally, one or more inert fillers, are sedimentation cast, slip cast or pressed onto or into a body and into a particular desired shape.

    Abstract translation: 本发明一般涉及一种制备自支撑体的新方法，以及由此制成的新颖产品。 在其更具体的方面，本发明涉及通过将熔融母体金属反应性渗入包含硼的预成型体中来生产包含一种或多种含硼化合物（例如硼化物或硼化物）和碳化物的自支撑体的方法 碳化物或硼供体材料与碳供体材料和任选的一种或多种惰性填料组合以形成体。 具体地说，碳化硼材料或硼供体材料和碳供体材料的组合，并且在任一种情况下，任选地，一种或多种惰性填料中，是沉淀铸造，滑模浇注或压入或进入体内并进入特定期望的 形状。

    Method of modifying ceramic composite bodies by a post-treatment process and articles produced thereby
    12.
    发明授权
    Method of modifying ceramic composite bodies by a post-treatment process and articles produced thereby 失效
    通过后处理工艺改变陶瓷复合体的方法和由此制备的制品

    公开(公告)号：US5298051A

    公开(公告)日：1994-03-29

    申请号：US973449

    申请日：1992-11-09

    Applicant: Terry D. Claar ,  Gerhard H. Schiroky ,  William B. Johnson

    Inventor： Terry D. Claar ,  Gerhard H. Schiroky ,  William B. Johnson

    IPC: C04B35/65 ,  C04B41/50 ,  C04B41/87 ,  C22C29/00 ,  C22C29/04

    CPC classification number: C04B41/009 ,  C04B35/652 ,  C04B41/5062 ,  C04B41/87 ,  C22C29/00

    Abstract: This invention relates generally to a novel method of manufacturing a composite body, such as a ZrB.sub.2 -ZrC-Zr (optional) composite body, by utilizing a post-treatment process and to the novel products made thereby. More particularly, the invention relates to a method of modifying a composite body comprising one or more boron-containing compounds (e.g., a boride or a boride and a carbide) which has been made by the reactive infiltration of a molten parent metal into a bed or mass containing boron carbide, and optionally one or more inert fillers, to form the body.

    Abstract translation: 本发明一般涉及通过利用后处理工艺制造复合体，例如ZrB 2 -ZrC-Zr（任选的）复合体的新方法和由此制备的新颖产品。 更具体地说，本发明涉及一种修饰包括一种或多种含硼化合物（例如，硼化物或硼化物和碳化物）的复合体的方法，其通过将熔融母体金属的反应性渗入床形成 或含有碳化硼的物质，以及任选的一种或多种惰性填料以形成体。

    Process for preparing self-supporting bodies and products made thereby
    16.
    发明授权
    Process for preparing self-supporting bodies and products made thereby 失效
    制备自支撑体及其制品的方法

    公开(公告)号：US4978644A

    公开(公告)日：1990-12-18

    申请号：US449521

    申请日：1989-12-12

    Applicant: Danny R. White ,  Terry D. Claar

    Inventor： Danny R. White ,  Terry D. Claar

    IPC: C04B35/58 ,  C04B35/65

    CPC classification number: C04B35/5805 ,  C04B35/58064 ,  C04B35/58071 ,  C04B35/58078 ,  C04B35/652 ,  C04B35/653

    Abstract: Self-supporting bodies are produced by reactive infiltration of a parent metal into a boron nitride material typically resulting in a body comprising a boron-containing compound, a nitrogen-containing compound and metal. The mass to be infiltrated may contain one or more inert fillers admixed with the boron nitride, to produce a composite by reactive infiltration, which composite comprises a matrix which embeds the filler material. The matrix, in a composite body containing filler material, comprises one or more of metal, a boron-containing compound and a nitrogen-containing compound. The relative amounts of reactants and process conditions may by altered or controlled to yield a body containing varying volume percents of ceramic, metal and/or porosity. The mass to be infiltrated can be contained within a refractory vessel having a venting means included therein.

    Abstract translation: 通过将母体金属反应性渗透到氮化硼材料中而产生自支撑体，通常产生包含含硼化合物，含氮化合物和金属的体。 待渗透的物质可以包含一种或多种与氮化硼混合的惰性填料，以通过反应性渗透产生复合材料，该复合材料包括嵌入填料的基质。 含有填料的复合体中的基体包含一种或多种金属，含硼化合物和含氮化合物。 反应物和工艺条件的相对量可以通过改变或控制以产生包含不同体积百分比的陶瓷，金属和/或孔隙率的主体。 待渗透的物质可以包含在其中包括排气装置的耐火容器中。

    Process for preparing self-supporting bodies and products made thereby
    17.
    发明授权
    Process for preparing self-supporting bodies and products made thereby 失效
    制备自支撑体及其制品的方法

    公开(公告)号：US4940679A

    公开(公告)日：1990-07-10

    申请号：US137044

    申请日：1987-12-23

    Applicant: Terry D. Claar ,  Steven M. Mason ,  Kevin P. Pochopien ,  Danny R. White

    Inventor： Terry D. Claar ,  Steven M. Mason ,  Kevin P. Pochopien ,  Danny R. White

    IPC: C04B35/58 ,  C04B35/56 ,  C04B35/563 ,  C04B35/622 ,  C04B35/65 ,  C04B41/50 ,  C04B41/87 ,  C22C29/00 ,  C22C29/14

    CPC classification number: C04B41/009 ,  C04B35/56 ,  C04B35/5607 ,  C04B35/5611 ,  C04B35/5622 ,  C04B35/5805 ,  C04B35/58064 ,  C04B35/58071 ,  C04B35/58078 ,  C04B35/652 ,  C04B35/653 ,  C04B41/5062 ,  C04B41/87 ,  C22C29/00

    Abstract: Self-supporting bodies are produced by reactive infiltration of a parent metal into boron carbide typically resulting in a composite comprising a boron-containing compound and metal. The mass to be infiltrated may contain one or more inert fillers admixed with the boron carbide, or at least one carbon donor material, to produce a composite by reactive infiltration, which composite comprises a matrix of metal and boron-containing compound embedding the filler. In one embodiment of the invention, a parent metal is reactively infiltrated into a mass comprising a boron carbide material mixed with a carbon-containing compound. In this embodiment, a self-supporting composite is formed typically comprising a boron-containing compound, a carbon-containing compound, and metal. The relative amounts of reactants and process conditions may be altered or controlled to yield a body containing varying volume percents of ceramic, metal and/or porosity. The mass to be infiltrated can be contained within a refractory vessel having a venting means included therein.

    Abstract translation: 通过将母体金属反应性浸渗到碳化硼中而产生自支撑体，通常产生包含含硼化合物和金属的复合材料。 待渗透的物质可以含有一种或多种与碳化硼或至少一种碳供体材料混合的惰性填料，以通过反应性渗透产生复合材料，该复合材料包含嵌入填料的金属和含硼化合物的基质。 在本发明的一个实施方案中，母体金属被反应地渗透到包含与含碳化合物混合的碳化硼材料的组合物中。 在该实施方案中，通常包含含硼化合物，含碳化合物和金属的自支撑复合材料。 可以改变或控制反应物和工艺条件的相对量，以产生包含不同体积百分比的陶瓷，金属和/或孔隙的体。 待渗透的物质可以包含在其中包括排气装置的耐火容器中。

    High-temperature direct-contact thermal energy storage using phase-change media
    18.
    发明授权
    High-temperature direct-contact thermal energy storage using phase-change media 失效
    使用相变介质的高温直接接触式热能储存

    公开(公告)号：US4421661A

    公开(公告)日：1983-12-20

    申请号：US275380

    申请日：1981-06-19

    Applicant: Terry D. Claar ,  Randy J. Petri

    Inventor： Terry D. Claar ,  Randy J. Petri

    IPC: C09K5/06 ,  F28D20/02 ,  F24H7/04 ,  F28F23/00

    CPC classification number: F28D20/023 ,  C09K5/063 ,  Y02E60/145 ,  Y02E70/30 ,  Y10T428/2982 ,  Y10T428/2991 ,  Y10T428/2993

    Abstract: A high-temperature direct-contact thermal energy storage element for use in a system for storage and retrieval of thermal energy in the range of about 400.degree. to about 2000.degree. F. The thermal energy is directly stored, without heat exchange tubes in composite latent/sensible heat thermal energy storage media utilizing the heat of fusion and high-temperature stability of alkaline metal and alkaline earth carbonates, chlorides, nitrates, nitrites, fluorides, hydroxides, sulfates, and mixtures thereof maintained within a porous support-structure material which itself is capable of storage as sensible heat. The thermal energy storage according to the invention may be effectively utilized for storage of thermal energy derived from solar, industrial waste, process heat, and high-temperature gas reactor energy sources and retrieved for a wide variety of uses such as combustion air preheating, drying, space heating, heating of process gases, and the like.

    Abstract translation: 一种高温直接接触式热能储存元件，用于在约400°至约2000°F范围内储存和回收热能的系统中。热能直接储存在复合潜热中的热交换管 /显热热存储介质，其利用本身的多孔载体结构材料中的碱金属和碱土金属碳酸盐，氯化物，硝酸盐，亚硝酸盐，氟化物，氢氧化物，硫酸盐及其混合物的融合热和高温稳定性 能够作为显热储存。 根据本发明的热能储存可以有效地用于储存源自太阳能，工业废物，工艺热和高温气体反应堆能源的热能，并且可用于多种用途，如燃烧空气预热，干燥 ，空间加热，工艺气体的加热等。

    Method of making metal matrix composite with the use of a barrier
    19.
    发明授权
    Method of making metal matrix composite with the use of a barrier 失效
    使用屏障制作金属基复合材料的方法

    公开(公告)号：US5482778A

    公开(公告)日：1996-01-09

    申请号：US179463

    申请日：1994-01-10

    Applicant: Michael K. Aghajanian ,  Terry D. Claar

    Inventor： Michael K. Aghajanian ,  Terry D. Claar

    IPC: C04B35/65 ,  C04B41/51 ,  C04B41/88 ,  C22C1/10 ,  C04B35/00

    CPC classification number: C04B35/652 ,  C04B41/5155 ,  C04B41/88 ,  C22C1/1036 ,  C22C2001/1063 ,  Y10T428/12007 ,  Y10T428/12486 ,  Y10T428/12576 ,  Y10T428/12583 ,  Y10T428/12736 ,  Y10T428/30

    Abstract: A net shaped ceramic-reinforced aluminum matrix composite is provided by forming a permeable mass of ceramic material with a defined surface boundary having a barrier, and contacting a molten aluminum-magnesium alloy with the permeable mass of ceramic material in the presence of a gas comprising from about 10 to 100% nitrogen, by volume, balance nonoxidizing gas, e.g. hydrogen or argon. Under these conditions, the molten alloy spontaneously infiltrates the ceramic mass under normal atmospheric pressures until it reaches the barrier. A solid body of the alloy can be placed adjacent to a permeable bedding of ceramic material having a barrier, and brought to the molten state, preferably to at least about 700.degree. C., in order to form the net shape aluminum matrix composite by spontaneous infiltration. In addition to magnesium, auxiliary alloying elements may be employed with aluminum. The resulting composite products may contain a discontinuous aluminum nitride phase in the aluminum matrix.

    Abstract translation: 通过形成具有限定的具有阻挡层的表面边界的陶瓷材料的可渗透物质，并且在熔融的铝 - 镁合金与可渗透的陶瓷材料的物质的存在下，在气体存在下接触，形成网状陶瓷增强的铝基复合材料，所述气体包括 约10至100％的氮气（体积），平衡非氧化气体，例如 氢或氩。 在这些条件下，熔融合金在正常大气压力下自发渗透到陶瓷块中直至达到屏障。 合金的固体可以邻近具有阻挡层的陶瓷材料的可渗透层，并且进入熔融状态，优选至少约700℃，以便通过自发形成网状铝基复合材料 浸润。 除了镁之外，辅助合金元素可以与铝一起使用。 所得到的复合产品可能在铝基体中含有不连续的氮化铝相。

    Methods of making composite aluminum nitride ceramic articles having embedded filler
    20.
    发明授权
    Methods of making composite aluminum nitride ceramic articles having embedded filler 失效
    制备具有嵌入填料的复合氮化铝陶瓷制品的方法

    公开(公告)号：US5420085A

    公开(公告)日：1995-05-30

    申请号：US7387

    申请日：1993-01-21

    Applicant: Marc S. Newkirk ,  Harry R. Zwicker ,  Andrew W. Urquhart ,  Harold D. Lesher ,  Terry D. Claar ,  Michael K. Aghajanian ,  John P. Biel, Jr.

    Inventor： Marc S. Newkirk ,  Harry R. Zwicker ,  Andrew W. Urquhart ,  Harold D. Lesher ,  Terry D. Claar ,  Michael K. Aghajanian ,  John P. Biel, Jr.

    IPC: C04B35/65 ,  C04B35/76 ,  C04B35/80 ,  C04B41/50 ,  C04B41/87 ,  C04B35/58

    CPC classification number: C04B41/5025 ,  C04B35/652 ,  C04B35/76 ,  C04B35/80 ,  C04B41/87

    Abstract: A method of making self-supporting ceramic composite structures having filler embedded therein includes infiltrating a permeable mass of filler with polycrystalline material comprising an oxidation reaction product obtained by oxidation of a parent metal such as aluminum and optionally, containing therein non-oxidized constituents of the parent metal. The structure is formed by placing a parent metal adjacent to a permeable filler and heating the assembly to melt the parent metal and provide a molten body of parent metal which is contacted with a suitable vapor-phase oxidant. Within a certain temperature region and optionally, aided by one or more dopants in or on the parent metal, molten parent metal will migrate through previously formed oxidation reaction product into contact with the oxidant, causing the oxidation reaction product to grow so as to embed the adjacent filler and provide the composite structure. In a preferred embodiment, a parent metal comprising aluminum is oxidized by a vapor-phase oxidant comprising nitrogen to form a ceramic matrix comprising an aluminum nitride oxidation reaction product. In a particularly preferred embodiment, one or more protective coatings are applied to the filler prior to formation of the aluminum nitride oxidation reaction product matrix.

    Abstract translation: 制造具有嵌入其中的填料的自支撑陶瓷复合结构的方法包括用多晶材料渗透可渗透的填料，所述多晶材料包含通过氧化母体金属如铝而获得的氧化反应产物，并且任选地含有其中的非氧化成分 母金属。 通过将母体金属放置在可渗透填料附近并加热该组件以熔化母体金属并提供与合适的气相氧化剂接触的母体金属的熔融体来形成结构。 在一定温度范围内，任选地，由母体金属中或母体金属上的一种或多种掺杂剂辅助，熔融母体金属将迁移通过预先形成的氧化反应产物与氧化剂接触，使氧化反应产物生长，从而嵌入 相邻填料并提供复合结构。 在优选的实施方案中，包含铝的母体金属被包含氮的气相氧化剂氧化以形成包含氮化铝氧化反应产物的陶瓷基体。 在特别优选的实施方案中，在形成氮化铝氧化反应产物基质之前，将一种或多种保护性涂料施加到填料上。

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