摘要:
Silicon nitride materials with high strength, fracture toughness values, and Weibull moduli simultaneously, due to unique large grain reinforcing microstructures and well engineered grain boundary compositions. The invention demonstrates that, surprisingly and contrary to prior art, a silicon nitride material can be made which simultaneously has high strength above about 850-900 MPa, a Weibull above about 15 and high fracture toughness (above about 8 and 9 MPa·m1/2), and has reinforcing grains longer than 5 μm, typically longer than 10 μm in the microstructure without compromising its properties and reliability. The product of this invention can be processed using a variety of densification methods, including gas-pressure sintering, hot pressing, hot isostatic pressing, but is not limited to these, and does not require multiple heat treatments for all of these features to be achieved.
摘要:
An aspect of the present disclosure relates to a device for securing a helmet, such as a helmet holster. The device may include a pocket defined by a base and a pocket portion, wherein the pocket portion exhibits a width and a height. The width of the pocket portion may be equal to or greater than said height of the pocket portion. The device may also include an adjustable restraint, wherein the restraint includes a first portion affixed to the base, configured to at least partially retain at least a portion of the helmet in the pocket. The device may further include an adjustable strap affixed to the pocket.
摘要:
A dense silicon carbide (SiC) material with boron (B), nitrogen (N) and oxygen (O) as the only additives and with excellent insulting performance (electrical volume resistivity greater than 1×108 Ω·cm). The SiC ceramic material, made from a powder mix of, by weight, from 0.1 to 7% boron carbide, from 0.1 to 7% silicon nitride, from 0.1 to 6% silicon dioxide, and a balance of α-SiC, consists essentially of (1) at least 90% by weight of α-SiC, (2) about 0.3 to 4.0% by weight of boron, (3) about 0.1 to 6.0% by weight of nitrogen, (4) about 0.06 to 0.5% by weight of oxygen, and (5) no more than 0.07% by weight of metallic impurities; wherein the boron and nitrogen are present according to an B/N atomic ratio of 0.9 to 1.5. In particular, this material is suitable for applications in plasma etching chambers for semiconductor and integrated circuit manufacturing.
摘要:
High-volume, fully dense, multi-component monoliths with microstructurally indistinguishable joints that can be used as refractory, corrosion and wear resistant components in the non-ferrous metal industry. The Si3N4 monoliths according to the invention comprise at least 90% by weight β-type Si3N4 and up to 10% by weight of a predominantly amorphous binder phase, said binder phase being formed from compositions of the rare earth metal —Al—Si—O—N, rare earth metal —Mg—Si—O—N or Mg—Si—O—N systems. Preferably the rare earth metal is yttrium (Y). The monoliths have a volume of greater than 250 cm3. A method of making the multi-component monoliths is achieved by simultaneously joining and uniaxially hot pressing an assembly of reaction bonded silicon nitride bodies (RBSN bodies). RBSN bodies are placed in contact with each other in the substantial absence of any interlayer or ceramic paste in between.
摘要翻译:高容量,完全致密的多组分整料,具有微结构难以区分的接头,可用作有色金属工业中的耐火,耐腐蚀和耐磨部件。 根据本发明的Si 3 N 4整体包含至少90重量%的β型Si 3 N 4和至多10重量%的主要为无定形粘结相,所述粘结相由稀土金属-Al-Si-ON ,稀土金属-Mg-Si-ON或Mg-Si-ON系统。 稀土金属优选为钇(Y)。 整料具有大于250cm 3的体积。 通过同时接合和单轴热压反应接合的氮化硅体(RBSN体)的组件来实现制造多组分整料的方法。 基本上不存在任何中间层或陶瓷浆料,将RBSN体彼此接触。
摘要:
A method of making a silicon nitride comprising object by use of a low density reaction bonded body is disclosed. An uncompacted mixture of silicon powder and a fluxing agent is heated in a nitrogen atmosphere to react the mixture with the atmosphere to form a body consisting essentially of silicon nitride and having a dimension greater than and a density less than the finished product. The nitrided mixture is then hot pressed to produce a silicon nitride comprising object of desired dimension and density, which material is useful as a cutting tool material for machining metals.
摘要:
A dampening system roll which may be used in an offset printing press, is made of porous rebonded, fused silica, the pores of which are impregnated and sealed by a silicone resin. In a typical embodiment of the invention disclosed herein, a dampening system roll is fabricated by providing a 3 3/4 inch diameter 42 1/2 inch long fused silica cylinder infiltrated with a silicone resin and ground and polished to a 30 microinch Ra exterior smoothness. The ends of the cylinder are drilled out to provide a 1 3/4 inch diameter by 4 inch deep hollow core on each side which is adapted to receive a pair of shafts or end caps typically made of stainless steel or other low expansion metal alloy material and the end shafts or caps are bonded into the drilled ends of the fused silica cylinder for interfacing the printing press system. In an additional embodiment, the ends of the cylinder are core drilled to provide a pair of axial sockets each about 2 inches in diameter and about 2 inches deep. A threaded, low expansion metal alloy insert is then bonded to the interior of each such socket and mating threaded shafts are screwed into the inserts for connecting the cylinder to the remainder of the dampening system.
摘要:
A method of making a reaction bonded/hot pressed silicon nitride comprising object is disclosed. Second phase crystallites are formed prior to hot pressing. A mixture of silicon, SiO.sub.2, and 0.4-2.3 molar percent (by weight of the silicon) of oxygen carrying agents, i.e., Y.sub.2 O.sub.3 and Al.sub.2 O.sub.3, is performed and reaction nitrided to form discs or billets having at least 60% alpha Si.sub.3 N.sub.4 and a high proportion of second phase crystallites which displace substantially all silicate glass except for a controlled small quantity. The reactive amounts of Y.sub.2 O.sub.3, Al.sub.2 O.sub.3 and SiO.sub.2 are controlled to assure formation of substantially Y.sub.1 SiO.sub.2 N as the second phase crystallite. Al.sub.2 O.sub.3 is controlled in an amount of 0.4-4% by weight to ensure that the small proportion of glass serves to protect the oxynitrides against linear oxidation kinetics. The hot pressed material has no visual mottle porosity associated therewith.
摘要翻译:公开了制造包含反应结合/热压氮化硅的物体的方法。 在热压之前形成第二相微晶。 执行硅,SiO 2和0.4-2.3摩尔%(重量比的硅)氧气载体(即Y 2 O 3和Al 2 O 3)的混合物,并将其反应氮化以形成具有至少60%的α3 Si 3 N 4和 高比例的第二相微晶,除了受控的少量之外基本上置换所有的硅酸盐玻璃。 控制Y 2 O 3,Al 2 O 3和SiO 2的反应量,以确保形成基本上作为第二相微晶的Y1SiO2N。 控制Al2O3的量为0.4-4重量%,以确保玻璃的小比例用于保护氮氧化物免受线性氧化动力学的影响。 热压材料没有与之相关的视觉斑点孔隙。
摘要:
A method of cooling a nuclear reactor core is disclosed. The method includes contacting the nuclear reactor core with an aqueous solution comprising at least one of polyhedral boron hydride anions or carborane anions. Nuclear reactors are also disclosed. The nuclear reactor has a neutron moderator that is an aqueous solution comprising at least one of polyhedral boron hydride anions or carborane anions, or the nuclear reactor has an emergency core cooling system including a vessel containing a volume of an aqueous solution comprising at least one of polyhedral boron hydride anions or carborane anions. The nuclear reactor can also have both an aqueous solution comprising at least one of polyhedral boron hydride anions or carborane anions as a neutron moderator and an emergency core cooling system that includes an aqueous solution comprising at least one of polyhedral boron hydride anions or carborane anions.
摘要:
An armor blast shield for use on the bottom of a vehicle to protect occupants of the vehicle from improvised explosive devices. A preferred embodiment is configured in a V-shaped configuration formed by at least two planar blast resistant panels and an I-beam having channels with inclined walls which receive the panels at an obtuse angle. The panels are adhesively adhered to the I-beam channel walls and at least one bolt is secured through the I-beam and a panel to provide superior blast resistant performance as compared to welded panels.
摘要:
Silicon nitride materials with high strength, fracture toughness values, and Weibull moduli simultaneously, due to unique large grain reinforcing microstructures and well engineered grain boundary compositions. The invention demonstrates that, surprisingly and contrary to prior art, a silicon nitride material can be made which simultaneously has high strength above about 850-900 MPa, a Weibull above about 15 and high fracture toughness (above about 8 and 9 MPa·m1/2), and has reinforcing grains longer than 5 μm, typically longer than 10 μm in the microstructure without compromising its properties and reliability. The product of this invention can be processed using a variety of densification methods, including gas-pressure sintering, hot pressing, hot isostatic pressing, but is not limited to these, and does not require multiple heat treatments for all of these features to be achieved.