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58 条记录 (耗时 0.021 秒)

    Production and use of octafluoropropane
    11.
    发明申请
    Production and use of octafluoropropane 有权
    生产和使用八氟丙烷

    公开(公告)号：US20040158109A1

    公开(公告)日：2004-08-12

    申请号：US10770438

    申请日：2004-02-04

    申请人： SHOWA DENKO K.K.

    发明人： Hiromoto Ohno ,  Toshio Ohi

    IPC分类号： C07C019/08

    CPC分类号： C07C19/08 ,  C07C17/087 ,  C07C17/10 ,  C07C17/206 ,  C07C17/21 ,  C07C17/38 ,  C07C17/383

    摘要： Octafluoropropane is produced by a process including a step (1) of reacting hexafluoropropene with hydrogen fluoride in a gas phase at a temperature of from 150 to 450null C. in the presence of a fluorination catalyst to obtain 2H-heptafluoropropane and a step (2) of reacting 2H-heptafluoropropane obtained in step (1) with fluorine gas in a gas phase at a temperature of from 250 to 500null C. in the absence of a catalyst to obtain octafluoropropane. High-purity octafluoropropane is obtained which can be used in a process for producing a semiconductor device.

    摘要翻译： 通过在氟化催化剂的存在下，在150〜450℃的温度下，使六氟丙烯与氟化氢反应的工序（1）来制造八氟丙烷，得到2H-七氟丙烷和工序（2 ）在步骤（1）中获得的2H-七氟丙烷与氟气在气相中在250-500℃的温度下在不存在催化剂的情况下反应，得到八氟丙烷。 得到高纯度八氟丙烷，可用于制造半导体器件的方法。

    Processes for purifying chlorofluorinated compounds and processes for purifying CF3CFHCF3
    14.
    发明申请
    Processes for purifying chlorofluorinated compounds and processes for purifying CF3CFHCF3 失效
    纯化氟氯化合物的方法和纯化CF3CFHCF3的方法

    公开(公告)号：US20040102661A1

    公开(公告)日：2004-05-27

    申请号：US10698579

    申请日：2003-10-31

    发明人： Yuichi Iikubo ,  Stephen Owens ,  Mitchel Cohn ,  Stephan M. Brandstadter ,  Vicki E. Hedrick ,  Janet K. Boggs ,  John Qian ,  Julie Sacarias

    IPC分类号： C07C017/08 ,  C07C019/08

    CPC分类号： C07C17/383 ,  B01J23/44 ,  B01J23/8926 ,  B01J27/128 ,  B01J27/132 ,  C07C17/10 ,  C07C17/206 ,  C07C17/23 ,  C07C17/38 ,  C07C17/395 ,  Y02P20/582 ,  C07C19/10 ,  C07C19/08

    摘要： Methods and materials are provided for the production of essentially isomerically pure perhalogenated and partially halogenated compounds. One embodiment of the present invention provides a process for the production of essentially isomerically pure CFC-216aa. Other embodiments include processes for the production of CFC-217ba and HFC-227ea. Particular embodiments of the present invention provide separation techniques for the separation of chlorofluorocarbons from HF, from other chlorofluorocarbons, and the separation of isomers of halogenated compounds. Still other embodiments of the present invention provide catalytic synthetic techniques that demonstrate extended catalyst lifetime. In other embodiments, the present invention provides catalytic techniques for the purification of isomeric mixtures.

    摘要翻译： 提供了用于生产基本上异构纯的全卤代和部分卤代化合物的方法和材料。 本发明的一个实施方案提供了生产基本上异构纯的CFC-216aa的方法。 其它实施方案包括生产CFC-217ba和HFC-227ea的方法。 本发明的具体实施方案提供了将氯氟烃与其它氯氟烃分开的分离技术以及卤代化合物异构体的分离。 本发明的其它实施方案提供催化合成技术，其显示延长的催化剂寿命。 在其它实施方案中，本发明提供用于纯化异构体混合物的催化技术。

    Fluorine compound and fluorinating agent comprising the compound
    15.
    发明申请
    Fluorine compound and fluorinating agent comprising the compound 失效
    氟化合物和包含该化合物的氟化剂

    公开(公告)号：US20040073065A1

    公开(公告)日：2004-04-15

    申请号：US10433412

    申请日：2003-06-04

    发明人： Toshio Hidaka ,  Norio Fushimi ,  Takafumi Yoshimura ,  Takeshi Kawai

    IPC分类号： C07C019/08 ,  C07F009/02

    CPC分类号： C07F9/54 ,  C07B39/00 ,  C07C17/16 ,  C07C17/18 ,  C07C211/29 ,  C07C251/30 ,  C07C271/20 ,  C07F9/5004 ,  Y02P20/582

    摘要： A fluorine compound represented by Formula (1) is provided. The above fluorine compound is effective for introducing a fluorine atom into a compound having an active group such as an oxygen-containing functional group, and it can be used for uses of surface treatment, cleaning and coating. Further, after the fluorination reaction, the above compound is recovered and can be reused as a starting material for producing the above fluorine compound, and it is useful for various fluorination processes. 1 (wherein X represents a nitrogen or phosphorus atom; R0, R1, and R2 represent hydrogen, an alkyl group or aryl group which may have a substituent, and they each may be the same or different; and R0, R1, and R2 may be combined with each other to form a ring).

    摘要翻译： 提供由式（1）表示的氟化合物。 上述氟化合物有效地将氟原子引入具有活性基团的化合物如含氧官能团，并且其可用于表面处理，清洁和涂覆的用途。 此外，在氟化反应之后，回收上述化合物，可以重复使用作为制备上述氟化合物的原料，可用于各种氟化处理。 （其中X表示氮或磷原子; R 0，R 1和R 2表示氢，可以具有取代基的烷基或芳基，它们各自可以相同或不同; R 0，R 1和R 2可以是 结合起来形成一个戒指）。

    Process for the manufacture of halocarbons and selected compounds and azeotropes with HF
    16.
    发明申请
    Process for the manufacture of halocarbons and selected compounds and azeotropes with HF 有权
    用于制造卤代烃和所选化合物以及与HF共沸的方法

    公开(公告)号：US20030208090A1

    公开(公告)日：2003-11-06

    申请号：US10460270

    申请日：2003-06-12

    发明人： Ralph Thomas Baker ,  Ralph Newton Miller ,  Viacheslav Alexandrovich Petrov ,  Velliyur Nott Mallikarjuna Rao ,  Allen Capron Sievert

    IPC分类号： C07C253/30 ,  C07C019/08

    CPC分类号： C07C19/10 ,  C01B7/191 ,  C07C17/206 ,  C07C17/275 ,  C07C17/278 ,  C07C17/38 ,  C07C17/386 ,  C07C19/08 ,  Y02P20/582 ,  C07C19/01 ,  C07C19/16

    摘要： A liquid phase process is disclosed for producing halogenated alkane adducts of the formula CAR1R2CBR3R4 (where A, B, R1, R2, R3, and R4 are as defined in the specification) which involves contacting a corresponding halogenated alkane, AB, with a corresponding olefin, CR1R2nullCR3R4 in a dinitrile or cyclic carbonate ester solvent which divides the reaction mixture into two liquid phases and in the presence of a catalyst system containing (i) at least one catalyst selected from monovalent and divalent copper; and optionally (ii) a promoter selected from aromatic or aliphatic heterocyclic compounds which contain at least one carbon-nitrogen double bond in the heterocyclic ring. When hydrochlorofluorocarbons are formed, the chlorine content may be reduced by reacting the hydrochlorofluorocarbons with HF. New compounds disclosed include CF3CF2CCl2CH2CCl3, CF3CCl2CH2CH2Cl and CF3CCl2CH2CHClF. These compounds are useful as intermediates for producing hydrofluorocarbons. Azeotropes of CClF2CH2CF3 with HF and azeotropes of CF3CH2CHF2 with HF are also disclosed; as are process for producing such azeotropes. A process for purification of certain hydrofluorocarbons and/or chloro-precursors thereof from mixtures of such compounds with HF is also disclosed.

    摘要翻译： 公开了用于制备式CAR 1 R 2 CBR 3 R 4的卤代烷烃加成物的液相方法（其中A，B，R 1，R 2，R 3， 和R 4如说明书中所定义），其包括将相应的卤代烷烃AB与相应的烯烃CR 1 R 2 = CR 3 R 4在二腈或环状 碳酸酯溶剂，其将反应混合物分成两个液相，并且在含有（i）至少一种选自一价和二价铜的催化剂的催化剂体系的存在下， 和任选地（ii）选自在杂环中含有至少一个碳 - 氮双键的芳族或脂族杂环化合物的促进剂。 当形成氢氯氟烃时，可以通过氢氯氟烃与HF反应来降低氯含量。 所公开的新化合物包括CF 3 CF 2 CCl 2 CH 2 ClCl 3，CF 3 CCl 2 CH 2 CH 2 Cl和CF 3 CCl 2 CH 2 CHClF。 这些化合物可用作生产氢氟烃的中间体。 还公开了CClF 2 CH 2 CF 3与HF的共沸物和CF 3 CH 2 CHF 2与HF的共沸物质; 生产这种共沸物的方法也是如此。 还公开了从这种化合物与HF的混合物中纯化某些氢氟烃和/或其氯前体的方法。

    Ortho substituted benzaldehydes, preparation thereof and use thereof
    18.
    发明申请
    Ortho substituted benzaldehydes, preparation thereof and use thereof 失效
    正取代的苯甲醛，其制备及其用途

    公开(公告)号：US20010050352A1

    公开(公告)日：2001-12-13

    申请号：US09852552

    申请日：2001-05-10

    申请人： Clariant GmbH

    发明人： Rainer Wingen ,  Wolfgang Schmidt

    IPC分类号： C09K019/54 ,  C07C025/13 ,  C09K019/52 ,  C07C019/08

    CPC分类号： C07C47/55 ,  C07C45/00 ,  C07C45/68 ,  Y10T428/10

    摘要： Compounds of the formula (I) 1 in which X1nullH or F, X2nullH or F, and YnullCl, Br or I, are prepared by reacting, in a solvent or solvent mixture at a temperature below null60null C., a halobenzene of the formula (II) with an organic lithium compound and then with a formyl equivalent of the formula (III) 2 and may be used as starting materials for preparing agrochemicals, electronic materials and pharmaceuticals.

    摘要翻译： 其中X1 = H或F，X2 = H或F，以及Y = Cl，Br或I的式（I）化合物通过在低于-60℃的温度下在溶剂或溶剂混合物中反应来制备 ，式（II）的卤代苯与有机锂化合物反应，然后与式（III）的甲酰当量反应，可用作制备农药，电子材料和药物的原料。

    Process for preparation of dihalogenoadamantanes
    19.
    发明申请
    Process for preparation of dihalogenoadamantanes 失效
    二卤代金刚烷的制备方法

    公开(公告)号：US20040260127A1

    公开(公告)日：2004-12-23

    申请号：US10493892

    申请日：2004-04-26

    发明人： Norihiro Tanaka ,  Masao Yamaguchi

    IPC分类号： C07C019/08

    CPC分类号： C07C23/38 ,  C07C17/10

    摘要： This invention discloses a process for preparing a dihalogenated adamantane by reacting an adamantane optionally substituted with alkyl at 1-position with a halosulfonic acid, comprising the first stage of monohalogenation conducted at null5 to 15null C. and then the second stage of dihalogenation conducted at 17 to 35null C., preferably in the absence of an organic solvent.

    摘要翻译： 本发明公开了一种制备二卤代金刚烷的方法，该方法是将任选被1位烷基取代的金刚烷与卤代磺酸反应，该方法包括在-5至15℃下进行一卤化的第一阶段，然后进行第二阶段的二卤化反应 在17至35℃，优选在不存在有机溶剂的情况下。