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    Process for Purification of Oligoanilines and Oligoanilines
    12.
    发明申请
    Process for Purification of Oligoanilines and Oligoanilines 审中-公开
    寡聚苯胺和低聚苯胺的纯化方法

    公开(公告)号：US20080042557A1

    公开(公告)日：2008-02-21

    申请号：US11631034

    申请日：2005-07-06

    申请人： Taku Kato ,  Takuji Yoshimoto

    发明人： Taku Kato ,  Takuji Yoshimoto

    IPC分类号： H01J1/62 ,  C07C209/82

    CPC分类号： C08G73/0266 ,  C07C209/84 ,  C07C211/54 ,  H01L51/0025 ,  H01L51/0035 ,  H01L51/5048 ,  H01L51/5088

    摘要： Oligoanilines of the general formula (1) exhibiting absorption coefficient (ε) of 30 or below at 560 nm are obtained by dissolving a crude oligoaniline which contains an oligoaniline of the general formula (1) and oxides thereof and exhibits an absorption coefficient (ε) of 80 to 1000 at 560 nm in a solvent to form an oligoaniline solution, treating the solution with 4 to 20% by mass of activated carbon based on the crude oligoaniline, and subjecting the resulting solution to recrystallization. According to the process, oligoanilines which little contain impurities and can exert electroluminescent characteristics with high reproducibility can be obtained. [wherein R1 to R3 are each independently hydrogen, hydroxyl, or the like; A and B are each independently a divalent group represented by the general formula (2) or (3), R4 to R11 are each independently hydrogen, hydroxyl, or the like; and m and n are each independently an integer of 1 or above and satisfy the relationship: m+n≦20.]

    摘要翻译： 通过溶解含有通式（1）的低聚苯胺及其氧化物并显示吸收系数（ε）的粗寡苯胺，得到在560nm下显示吸收系数（ε）为30以下的通式（1）的聚苯胺， 在溶剂中在560nm下进行80〜1000的反应，形成低聚苯胺溶液，用粗寡胺以4〜20质量％的活性炭处理该溶液，使所得溶液重结晶。 根据该方法，可以获得少量含有杂质且能够以高再现性发挥电致发光特性的低聚苯胺。 [其中R 1至R 3各自独立地为氢，羟基等; A和B各自独立地为由通式（2）或（3）表示的二价基团，R 4至R 11各自独立地为氢，羟基或 喜欢; m和n各自独立地为1以上的整数，并且满足关系：m + n <= 20]

    Process for preparing sertraline hydrochloride polymorphic form II
    15.
    发明授权
    Process for preparing sertraline hydrochloride polymorphic form II 失效
    舍曲林盐酸多晶型II的制备方法

    公开(公告)号：US07067700B2

    公开(公告)日：2006-06-27

    申请号：US10479155

    申请日：2002-05-30

    申请人： Ilpo Laitinen

    发明人： Ilpo Laitinen

    IPC分类号： C07C209/82 ,  C07C209/86

    CPC分类号： C07C209/82 ,  C07C211/42 ,  C07C2602/10

    摘要： Sertraline hydrochloride, (1Scis)-4-(3,4-dichlorophenyl)-1,2,3,4-tetrahydro-N-methyl-1-naphtalenaminehydrochloride, polymorph II is prepared by extracting or dissolving the sertraline base into ethyl acetate, adding isopropanol as a solvent, adding hydrogen chloride dissolved in ethyl acetate or in gaseous form, and finally isolating and drying sertraline hydrochloride polymorphic form II.

    摘要翻译： 盐酸舍曲林（1Scis）-4-（3,4-二氯苯基）-1,2,3,4-四氢-N-甲基-1-萘胺盐酸盐，通过将舍曲林碱提取或溶解于乙酸乙酯中制备多晶型II， 加入异丙醇作为溶剂，加入溶于乙酸乙酯或气态的氯化氢，最后分离和干燥盐酸舍曲林多晶型II。