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    HYBRID SEALING COMPOSITE FOR FLAT SOLID OXIDE FUEL CELL STACK
    22.
    发明申请
    HYBRID SEALING COMPOSITE FOR FLAT SOLID OXIDE FUEL CELL STACK 有权
    用于平板固体氧化物燃料电池堆的混合密封复合材料

    公开(公告)号：US20100285394A1

    公开(公告)日：2010-11-11

    申请号：US12438619

    申请日：2006-12-08

    Applicant: Jong-Ho Lee ,  Hae-Weon Lee ,  Joo-Sun Kim ,  Hue-Sup Song ,  Ji-Won Son ,  Hae-Ryoung Kim ,  Sung-Moon Kim ,  Hyoung-Chul Kim ,  Hwa-Young Jung

    Inventor： Jong-Ho Lee ,  Hae-Weon Lee ,  Joo-Sun Kim ,  Hue-Sup Song ,  Ji-Won Son ,  Hae-Ryoung Kim ,  Sung-Moon Kim ,  Hyoung-Chul Kim ,  Hwa-Young Jung

    IPC: H01M2/08

    CPC classification number: H01M8/0282

    Abstract: The present invention provides a hybrid composite sealant, as a sealing material for a planar type solid oxide fuel cell stack, having a matrix of a glass composition, wherein a surface layer reinforced with platelet reinforcement particles is laminated on either one or both surfaces of an inner layer reinforced with fibrous reinforcement particles. Accordingly, by applying the composite sealant of the present invention to the solid oxide fuel cell stack, excellent gas-tightness of the stack can be obtained even under low coupling pressure, thermal cycling durability can be enhanced due to low coupling strength with a contact surface of an object to be sealed, stack disassembly and maintenance can be facilitated when parts within the stack are disabled, and stack stability as well as stack performance can be maintained under a pressurized operation condition where pressure differentials between the inside and outside of the stack reach to 5 atmospheric pressures (0.5 MPa).

    Abstract translation: 本发明提供一种作为平面型固体氧化物燃料电池堆的密封材料的混合复合密封剂，其具有玻璃组合物的基体，其中用片状增强颗粒增强的表面层层叠在一个或两个表面上 内层用纤维增强颗粒增强。 因此，通过将本发明的复合密封剂应用于固体氧化物型燃料电池组，即使在低耦合压力下也能获得优异的气密性，因为与接触面的低耦合强度可以提高热循环耐久性 当堆中的部件被禁用时，可以方便地进行堆封拆卸和维护，堆叠的稳定性以及堆叠性能可以在叠层内外的压差达到的加压运行状态下保持 至5个大气压（0.5MPa）。

    Paste for solid oxide fuel cells, anode-supported solid oxide fuel cells using the same, and fabricating method thereof
    24.
    发明申请
    Paste for solid oxide fuel cells, anode-supported solid oxide fuel cells using the same, and fabricating method thereof 有权
    用于固体氧化物燃料电池的浆料，使用其的负极固体氧化物燃料电池及其制造方法

    公开(公告)号：US20070077476A1

    公开(公告)日：2007-04-05

    申请号：US11529212

    申请日：2006-09-29

    Applicant: Hae-Weon Lee ,  Jong-Ho Lee ,  Joo-Sun Kim ,  Ji-Won Son ,  Hue-Sup Song ,  Hyoung-Chul Kim ,  Hwa-Young Jung

    Inventor： Hae-Weon Lee ,  Jong-Ho Lee ,  Joo-Sun Kim ,  Ji-Won Son ,  Hue-Sup Song ,  Hyoung-Chul Kim ,  Hwa-Young Jung

    IPC: H01M8/12 ,  C04B35/64

    CPC classification number: H01M4/9066 ,  H01M4/8621 ,  H01M4/8885 ,  H01M8/1213 ,  H01M8/1226 ,  H01M8/124 ,  Y02P70/56

    Abstract: The present invention discloses a paste for screen printing which is used in a process of fabricating an anode functional layer, an electrolyte layer and a cathode layer of an anode-supported solid oxide fuel cell. The paste for the solid oxide fuel cell contains raw material powder of each layer, ethyl cellulose which is a binder, alpha terpineol which is a solvent, and an alcoholic solvent which has solubility to a thermosetting binder contained in an anode support and which is added by 0.5 to 20 wt % of alpha terpineol as an additional solvent. The present invention also discloses a fabricating method of an anode-supported solid oxide fuel cell which forms each layer of the fuel cell by screen printing by using the paste. According to the present invention, in the highly efficient pore structure anode support fabricated by thermosetting molding, the composition of the paste for screen printing is controlled to improve weftability, and the movement of the elements is restricted by curing, thereby reducing surface defects of the layers and interfacial defects between the layers in fabrication and improving the interface strength. As a result, the high performance large area solid oxide fuel cell can be economically and efficiently fabricated, and reliability of the product can be remarkably improved.

    Abstract translation: 本发明公开了一种丝网印刷用糊剂，其用于制造阳极支撑固体氧化物型燃料电池的阳极功能层，电解质层和阴极层的工序。 固体氧化物型燃料电池用糊剂含有各层的原料粉末，作为粘合剂的乙基纤维素，作为溶剂的α-萜品醇和对阳极载体中含有的热固性粘合剂具有溶解性的醇溶剂， 作为另外的溶剂使用0.5〜20重量％的萜品醇。 本发明还公开了一种阳极支撑的固体氧化物燃料电池的制造方法，其通过使用该糊状物的丝网印刷形成燃料电池的各层。 根据本发明，在通过热固性成型制造的高效率孔结构阳极支撑体中，控制用于丝网印刷的糊剂的组成以改善纬向性，并且元件的移动受到固化的限制，从而减少了 层和界面缺陷在制造和提高界面强度。 结果，可以经济高效地制造高性能大面积固体氧化物燃料电池，可以显着提高产品的可靠性。

    Shape anisotropic metal oxide nanoparticles and synthetic method thereof
    25.
    发明授权
    Shape anisotropic metal oxide nanoparticles and synthetic method thereof 失效
    形状各向异性金属氧化物纳米粒子及其合成方法

    公开(公告)号：US07122168B2

    公开(公告)日：2006-10-17

    申请号：US10678047

    申请日：2003-10-01

    Applicant: Kyoungja Woo ,  Jae-Pyoung Ahn ,  Hae-Weon Lee

    Inventor： Kyoungja Woo ,  Jae-Pyoung Ahn ,  Hae-Weon Lee

    IPC: C01G1/00 ,  C01G49/00

    CPC classification number: B82Y30/00 ,  C01G49/06 ,  C01P2002/72 ,  C01P2004/04 ,  C01P2004/64 ,  C01P2006/42 ,  Y10S977/773 ,  Y10S977/775 ,  Y10S977/777 ,  Y10S977/811

    Abstract: In a metal oxide nanoparticle and a synthetic method thereof, and in particular to maghemite (γ-Fe2O3) nanoparticles usable as a superhigh density magnetic recording substance by having good shape anisotropy and magnetic characteristics, hematite (α-Fe2O3) nanoparticles usable as a precursor to the maghemite or a catalyst, maghemite and hematite-mixed nanoparticles and a synthetic method thereof, the method for synthesizing metal oxide nanoparticles includes forming a reverse micelle solution by adding distilled water, a surfactant and a solvent to metallic salt not less than trivalent, precipitating and separating gel type amorphous metal oxide particles by adding proton scavenger to the reverse micelle solution; adjusting a molar ratio of metal oxide to the surfactant by washing the gel type amorphous metal oxide particles with a polar solvent; and crystallizing metal oxide nanoparticles through heating or reflux after dispersing the gel type amorphous metal oxide particles in a non-polar solvent having a high boiling point.

    Abstract translation: 在金属氧化物纳米颗粒及其合成方法中，特别涉及可用作超高密度磁记录物质的磁赤铁矿（γ-Fe 2 O 3 O 3）纳米颗粒，其具有良好的 形状各向异性和磁特性，可用作磁赤铁矿或催化剂的前体的赤铁矿（α-Fe 2 O 3 O 3）纳米颗粒和合成的赤铁矿 方法，合成金属氧化物纳米粒子的方法包括：通过向不同于三价的金属盐中加入蒸馏水，表面活性剂和溶剂形成反胶束溶液，通过向反相中加入质子清除剂沉淀和分离凝胶型无定形金属氧化物颗粒 胶束溶液; 通过用极性溶剂洗涤凝胶型无定形金属氧化物颗粒来调节金属氧化物与表面活性剂的摩尔比; 以及在将凝胶型无定形金属氧化物颗粒分散在具有高沸点的非极性溶剂中之后通过加热或回流结晶金属氧化物纳米颗粒。

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